The cyclotron is the only practical source of many carrier-free radioisotopes. The preparation and radiochemical isolation of a number of these activities, produced in the 60-inch cyclotron of Crocker Laboratory, will be presented in this paper and in subsequent papers of this series. In most cases the carrier-free radioisotopes were prepared for use in biological systems and the final preparations were in the form of isotonic saline solutions at a range of pH from 5 to 8. The present paper reports the radiochemical isolation of carrier-free Sn{sup 113} and In{sup 114} produced by bombarding cadmium with 38 Mev alpha-particles. At this energy, Sn{sup 113} and In{sup 114} are produced in a thick target by the nuclear reactions; Cd{sup 110}({alpha},n)Sn{sup 113}, Cd{sup 111}({alpha},2n)Sn{sup 113}, Cd{sup 112}({alpha},3n)Sn{sup 113}, Cd{sup 111}({alpha},p)In{sup 114}, Cd{sup 112}({alpha},pn) In{sup 114}. The shorter-lived tin and indium activities together with the possible radioisotopes of silver produced by (n,p) reactions, were allowed to decay out prior to the chemical separations.

On June 29th and July 13th, 1949, the Industrial Hygiene Group of the Health Instrument Divisions at HAPO conducted a study of the health aspects of the degreaser operations carried on in the Airlock adjoining the 105 Building in the 100 H Area. This was done at the request of the Medical Division. The results of the study, together with certain pertinent information concerning degreaser operation, are reported in this report.

Experimental use of sodium radiophosphate (P32)in treatment of polycythemia is described. Treatment history is 66 patients treated with P32 alone, 32 patients treated with P32 followed within 4 months by venesections, 21 patients treated with P32 followed more than 4 months later by venesections, 6 patients treated exclusively by venesections, and 9 patients treated and followed elsewhere.

The redox and pile operations are reported on. Construction in 100 (Pile), 200 (Separation), and 300 (Metal Fabrication) areas is described. General work in the Richland commercial areas and on the Southern Railroad connection is also described. Personnel information is disclosed.

The progress report discusses activities of the P Division for the month of July, 1949. The B and F piles operated at 275 megawatts and the D pile at 305 megawatts throughout the month except for outages listed under Area Activities. A total of 57.5 tons of metal, at an average concentration of 363 megawatt days/ton (MWD/ton) was discharged from the piles during the month. This included 41.9 tons of Class V (alpha-rolled, triple-dipped, completely transformed) metal at an average concentration of 397 MWD/ton which was discharged without difficulty. A portion of this material was inspected and appears to be satisfactory for exposures at this concentration.

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The general principles of a liquid-liquid solvent extraction method for the separation of metallic elements are outlined.

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This paper describes a means of determining tritium oxides in urine relying upon the production of acetylene from the active water with subsequent measurement of the ionization caused by the tritium beta particle.

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The relationship of respiration to photosynthesis in barley seedling leaves and the algae, Chlorella and Scenedesmus, has been investigated using radioactive carbon dioxide and the techniques of paper chromatography and radioautography. The plants are allowed to photosynthesize normally for thirty seconds in c{sup 14}O{sub 2} after which they are allowed to respire in air or helium in the light or dark. Respiration of photosynthetic intermediates as evidenced by the appearance of labeled glutomic, isocitric, fumaric and succinic acids is slower in the light than in the dark. Labeled glycolic acid is observed in barley and algae. It disappears rapidly in the dark and is maintained and increased in quantity in the light in C0{sub 2}-free air.

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A program was initiated to determine the thermal rupture characteristics of KS graphite under steady-state operating conditions simulating the thermal conditions of an uninhibited rocket reactor. The maximum thermal stress calculated using room-temperature properties was 3090 psi. The maximum net specific power obtained was 5.2 Btu/cu in.-sec. (B.O.G.)

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This report details events of importance reported by the Hanford Operations Office for the week ending July 13, 1949.

On July 14, 1949, and office memorandum was written about operations of a reprocessing building on the Hanford Site being suspended due to the mishandling of some plutonium powder. The letter describes the process of decontamination of the building surfaces, and the ventilation of the rooms of that building. It also describes the problem with the ventilation fans due to increased temperature and pressures.

As authorized by purchase order No. 11-2532 dated March 11, 1949 of the Kellex Corp., the first sample of a 4 inch three jaw type connector for Job 11 was fabricated. The design of the connector was per Crane Co. drawing DR-25126-D except vertical mounting. The materials were per Crane Co. drawing A-24491-C. As instructed in verbal conversation with Dr. D.D. Jacobus and as requested in Mr. J.J. Cuniffe`s letter of May 6, 1949, and Ingersoll-Rand Company`s 1 1/4 inch 534 impact wrench with suitable socket to fit the hexagon head of the operating screw of the 4 inch connector was procured on loan to make some preliminary tests. Engineering drawings are listed in a second report on the data base.

This report details events of importance reported by the Hanford Operations Office for the week ending July 6, 1949.

This is a progress report from Brookhaven National Laboratory for the period July 1 through December 31, 1949.

The following items of equipment have been completed: Two Scaler Multipliers, EO-18 and EO-338, undergoing test and adjustment. One Thyratron Heater Control for Scioto Laboratory. One Pilot model switch box for Group 16 hoods at Scioto Laboratory. One Pilot model patch box used as auxiliary to the present switch boxes. Installation of electronic equipment and sorting and cataloguing of stock at Scioto Laboratory has been started. The Y Section induction heaters have been installed electrically. With the present setup in the WD Building, it has been necessary to recycle all the solution which passes through the pH chamber on the clariflocculators. Sufficient tests have been run on the Berkeley Decimal scaler to indicate that, by using a pre-emplifier, it will be a satisfactory replacement for the scaler multiplier. Reworking of B-wall tubes has been held up pending the delivery of neon gas. Further investigations have been made on the frequency compensated constant voltage Sola transformers. Three automatic potential controllers have been modified in accordance with investigations of Group 10. The program of preventative maintenance on automatic potential controllers has resulted in a marked reduction of service calls and down-time for the operating group.

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