After several failures had occurred in the HRT leak detector system, several lengths of this tubing were removed for metallurgical examination. The tubing was of type 304 stainless steel and was 1/4" in diameter with a 0.065 wall. The tubing had been purchased as three different lots, the first in 45 ft. lengths and the other two as standards lengths. Tubing from the first lot was used primarily for the shield penetration and, therefore, sections of it are present in all lines of the system. It appears that chloride contamination entered the system in a portion of the first lot of tubing used for the shield penetration. The exact source of the chloride cannot be determined, but after considering the results and visiting the manufacturer's plant, it appears most likely the contamination was during the manufacturing process.

A system for concentrating uranyl nitrate solutions was designed and installed in the Thorex Pilot Plant. A total of 16,060 g of uranium was concentrated in the system in 68 batch runs. A total of 14,400 g total uranium (14.180 g U/sup 233/) was recovered as product suitable for shipment. Uranium loss to the evaporator condensate was 0.03% of the total uranium processed. The material balance across the system was 98.4%. The average concentration of uranium in the evaporator feed solution was 29 g/liter; the average concentration in the evaporated solution was 298 g U/liter and in the product solution was 199 g/liter. Radiation readings of bottles containing product solutions were taken with a hard-shell cutie pie immediately after each run, and these readings ranged from 35 to 1100 mr/hr. The radiation levels of the bottles of product solution shipped averaged 78 mr/hr. Bottles of product solution reading in excess of 300 mr/hr, maximum allowable for shipment. were reprocessed in the second-cycle solvent extraction system (Thorex) and reconcentrated. The products from seven runs had radiation levels in excess of 300 mr/hr at the time of concentration, or the activities had grown to that level by the time of shipment. The …

The Eyewash program, written by James H. Alexander and Nancy D. Given, provides solutions of reactor criticality problems in spherical geometry by means of the group diffusion method. It employs thirty lethargy groups (plus one thermal group) in nine regions. The input consists principally of specifying the geometrical scaling factor, boundaries and compositions of the various regions, and temperature level. The output includes the value of vc that would render the system critical, the relative fission density distribution, fissions, absorptions, and leakages in each lethargy group in each region, and, if desired, an edit of the flux at each space point, each lethargy, and an edit of the macroscopic cross sections for each lethargy, each region. OCUSOL-A is a minor modification and extension of Eyewash. It provides for the computation and editing, on the supervisory control typewriter, of the total absorptions in selected nuclides in the various regions. This information is useful in the computation of breeding ratios and the preparation of detailed neutron balances, and in the estimation of flux-averaged cross sections for use in estimating the rate of change of concentration of the various nuclides with burn-up. The program also provides for saving and transferring the final fission …

From abstract: "Four plates of uranium that were fabricated by powder metallurgy techniques and clad with 1100 aluminum by hot pressing were irradiated in the Materials Testing Reactor. Increases of about one-half per cent in length and one per cent in thickness were observed after exposure of 1600 megawatt days per ton. The surfaces of the plates remained smooth."

The in-plie slurry loop work is now being considered as a joint program between the PAR project and ORNL. It is proposed that PAR design, fabricate and test the in-pile loops and that ORNL operate the loops in-pile, dismantle the loops after irradiation and made the appropriate measurements to determine the radiation effects. This report gives the objects of the slurry in-pile program and outlines the facilities and operations required to execute ORNL's part of this program.

Abstract: "A radioactive tracer, Fe^59, was used to determine the disposition of iron as a result of the excitation of a U3O8 matrix in a d - c arc. Two different spectrographic procedures, both using carrier distillation excitation techniques, were compared as to the percent of iron volatilized, the percent of iron diffused into the electrode and the percent of iron remaining in the residual charge."

A monthly report summarizing work perform by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. In this monthly report information on the reactor design No. 10 had been selected as the LMFRE preliminary reference design, various shielding designs have bee studied, various calculations on multiregion code and reactivity have been continued, and other related to the LMFRE

A monthly report summarizing work performed by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. In this monthly report the R&D budget was reviewed, two-dimensional calculations were performed, analysis work was started on control rods and their housing, as well as continued work on the development of the LMFRE reactor.

A monthly report summarizing work perform by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. Included in this report was a study made regarding the possible use of beryllium as a core moderating material, calculations made regarding temperature distribution for various channel sizes and power levels, design parameters for initial operation of the LMFRE, and other work in the design and operation of the reactor.

A monthly report summarizing work perform by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. Initial contacts were made at National Reactor Testing Station and Hanford Works, design conditions for the proposed reactor vessels were reviewed, estimates of heating rates caused by radiation and the pluggage of fuel passages were computed, and design parameters for the LMFRE were established.

A monthly report summarizing work perform by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. In this months report includes specifications a utility loop, further calculations for fuel rods, drawings were reviewed and specifications for the core reactor were reviewed.

A monthly report summarizing work perform by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. This month's report includes information on various factors entering into the estimate of reference design core which has been analyzed for sources of error, further design and testing procedures on the nuclear core, and other work focused on construction and design elements.

A monthly report summarizing work perform by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. In this monthly report work was reported on a completed study of the change in critical concentration and critical diameter with small changes in the physical and nuclear parameters of the reference design, reactor design #8 which incorporates an integral graphite core and core tank has been completed and distributed, and other work required for the design and construction of a LMFRE.

A monthly report summarizing work perform by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. This month's report includes the Research and Development program was completed, a study of shielding requirements indicated the necessity for test data, more information on studies regarding reactor startup, and other developments related to develop the LMFRE.

A monthly report summarizing work performed by Babcock & Wilcox personnel for the U.S. Atomic Energy Commission. In this month's report comparison of second two-dimensional calculation with the equivalent one-dimensional calculations was performed, reference design core modifications were completed, along with continued work on the design of the core and containment vessel for a LMRFE.

Report containing research and development undertaken regarding the Liquid Metal Fuel Reactor Experiment.

The radiolytic decomposition of tributyl phosphate has been show by burr to product gases, acids, and polymers. the acids that are formed can limit the usefulness of tributyl phosphate for the processing of radioactive materials. The study of acid formation on radiolysis therefor becomes important to us for the understanding of the mechanism of acid formation, the influence of added materials and the effect of the structure of organo- phosphorous compounds. Samples of purified esters have been irradiated in the ORNL cobalt source. Conclusions: (1) The formation of acid from tributyl phosphate during irradiation with cobalt gamma rays involves a mechanism that is not a primary step. Evidence has been obtained for a secondary reaction that is minimized by the presence of certain compounds. (2) Toluene acting as an inhibitor for radiolytic formation of acid may indicate the usefulness of an aromatic hydrocarbon diluent in processing. (3) The aromatic hydrocarbon, when phenyl, was not effective when it was part of the molecule. (4) First tests revealed that dibutyl butyl-phosphonate produced less acid the TBP and may warrant further consideration for process application.

The following report studies the interactions of K-mesons in nuclear track emulsions and measures range-energy.

The compositions of the compounds and fused salt mixtures referred to in the ANP project by numbers are given.

The feasibility of determining particle sizes in the submicron range by employing an activation analysis - centrifugation method has been demonstrated. It is believed that this method is now applicable to the analysis of thorium oxide for submicron particles. The same techniques are, in most instance, usable in determining particle sized in other sample materials.

"The pulsed source technique consists of introducing repeated short bursts of neutrons into a subcritical assembly, and following the decay of the leakage flux as a function of time...It is noted that plotting the decay constant as a function of buckling gives an apparently accurate way to extrapolate to prompt critical. The pulsed source technique can also be used to calibrate control rod and poison worth, and will give some estimate of the prompt neutron lifetime."

"A convenient summary is given of useful formulas on the kinematics of high energy electron scattering together with a derivation of the relevant formulas for transforming from the center of mass to the laboratory system such parameters as scattering cross sections. The formulas derived hold for any two- body collision: the approximation (m = 0) employed for the electron scattering calculations is rigorously true for the elastic scattering of photons."

To supply information about the several letdown valves which have been in HRT service, a typical valve plug examined by the Metallurgy Section confirms the belief that chemical attack on the Stellite #6 was occurring. It appears that most of the corrosion was due to rinse solutions, since this phenomenon has not been noted on letdown valves in the HRT Mockup where over 90% of the operating time has been with UO2SO4 solutions.

Abstract: "Theoretical differential cross-sections computed from the optical model for 7 Mev neutrons are presented for a large number of nuclei. The parameters used for the calculations were selected on the basis of best fit to existing experimental data."