The cyclotron is the only practical source of many carrier-free radioisotopes. The preparation and radiochemical isolation of a number of these activities, produced in the 60-inch cyclotron of Crocker Laboratory, will be presented in this paper and in subsequent papers of this series. In most cases the carrier-free radioisotopes were prepared for use in biological systems and the final preparations were in the form of isotonic saline solutions at a range of pH from 5 to 8. The present paper reports the radiochemical isolation of carrier-free Sn{sup 113} and In{sup 114} produced by bombarding cadmium with 38 Mev alpha-particles. At this energy, Sn{sup 113} and In{sup 114} are produced in a thick target by the nuclear reactions; Cd{sup 110}({alpha},n)Sn{sup 113}, Cd{sup 111}({alpha},2n)Sn{sup 113}, Cd{sup 112}({alpha},3n)Sn{sup 113}, Cd{sup 111}({alpha},p)In{sup 114}, Cd{sup 112}({alpha},pn) In{sup 114}. The shorter-lived tin and indium activities together with the possible radioisotopes of silver produced by (n,p) reactions, were allowed to decay out prior to the chemical separations.

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The progress report discusses activities of the P Division for the month of July, 1949. The B and F piles operated at 275 megawatts and the D pile at 305 megawatts throughout the month except for outages listed under Area Activities. A total of 57.5 tons of metal, at an average concentration of 363 megawatt days/ton (MWD/ton) was discharged from the piles during the month. This included 41.9 tons of Class V (alpha-rolled, triple-dipped, completely transformed) metal at an average concentration of 397 MWD/ton which was discharged without difficulty. A portion of this material was inspected and appears to be satisfactory for exposures at this concentration.

This progress report discusses activities at Hanford Engineer Works for the month of July, 1944. The organization size increased rapidly in July, jumping from 1384 to 1886, an increase of 502 employees. Shortages existed on special lines such as electricians, instrument mechanics, and power operators. The opportunities to interview and employ Construction personnel improved as the Construction, organization moved past its peak employment figure. 269 houses were completed in Richland and 370 occupancies were reported, reducing the backlog of empty houses due to slow furniture movements. A total of 1530 houses or 35.6% of the village is now occupied. The overall canning yield increased from 63% to 75% while production leveled off at approximately two-thirds of design capacity. The metal machining operation and the test pile operated on a one shift-six day per week basis. The portion of the 100-B Area from the pump house through the filter plant and including the Power House was taken over by Operations on July 25. The Power House in the 200-W Area was started and flushing of process lines with water and steam got under way in the canyon. A new department was formed to control the Protection activities of the plant.

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Tests made prior to beginning operation of the 100 Areas showed that the cooling water had a tendency to deposit a film upon the slug and tubs surfaces. This film would manifest itself as an increase in the pressure drop through the tubes and its most serious affect would be the resultant decrease in the slug to water host transfer coefficient which would increase the slug surface temperature, causing greatly accelerated corrosion rates. It was thus proposed to study film formation an a production test. This report discusses this test.

This technical progress report details 100 Area activities for the time period of August 13 through August 19, 1946.

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This report discusses the use of coal tar to extinguish potential magnesium fires in stored metal turnings at the Hanford Engineer Works. The report is dated August 11, 1943. (JL)

This memorandum provides results of spectroscopic analysis of pile gas which were completed on August 4, 1945.

The pile physics group reports on reactivity power coefficients from the production test No. 105-248-P, the water leak in B pile, graphite properties, xenon equations from the B pile shutdown of March 1946, and reactivity balance. The experimental physics group headed by J.M. West reports on graphite testing, the P-11 project, and shielding. The experimental physics group headed by E.B. Montgomery reports on diffusion length measurements in the DR and H piles. (GHH)

The uranium slugs were used as the charge into the pile for the manufacture of minute quantities of plutonium. So little was known of uranium`s commercially adaptable physical properties that it was relegated almost to the category of a laboratory curiosity. A series of experimental and developmental programs were inaugurated to determine not only the extrudability, machinability and other physical properties, but also the influence on these of microscopic quantities of impurities present in the uranium. This historical document describes these early studies in the following sections: exceptional characteristics of the slug program; extrusion; drawing, waging and rolling; outgassing and straightening; Project 1030 (procurement of an additional sixty tons of finished slugs over and above that quantity originally supplied to the Clinton Laboratories) Machining, grinding and grooving; development of canning methods; production of canned slugs; and The Dummy Slug program.

The redox and pile operations are reported on. Construction in 100 (Pile), 200 (Separation), and 300 (Metal Fabrication) areas is described. General work in the Richland commercial areas and on the Southern Railroad connection is also described. Personnel information is disclosed.

It was agreed during a meeting on July 10, 1945, investigation should be made to determine how fast and in what fashion the temperature of the effluent water from the 100 Areas is dissipated in the Columbia River. A preliminary report on these investigation was issued March 1, 1946: it discussed the testing techniques developed and the results of a survey made at the 100-B Area. Following a review of the data and tentative conclusions resented therein, it was agreed to extend the survey using similar technique: to the D and F Areas, and to determine if the tentative conclusions were substantiated.

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The weekly progress for D and F piles is given. Status of the test to determine the cause of white deposits on the horizontal control rods of the F pile is given. Also discussed are studies of process water control and pressure drop, corrosion, and graphite expansion. Test results indicate that graphite expansion has not seriously limited discharge of process tubes.

This monthly report covers activities for the production reactors. The 100 Area activities include: corrosion and blistering studies of slugs and flanges; study of the process tube leak at 105-D; graphite expansion studies which include galling of process tubes and stresses in biological shields; and irradiation studies.

The available information on the ionic and radiochemical composition of current and aged bismuth phosphate process wastes is tabulated here for the convenience of those concerned with metal recovery. In addition to its application in the design of research and development experiments, the compilation may serve to suggest specific needs for additional analytical data. For convenience in chemical calculation, molar compositions have been calculated for the ionic constituents based on the g/1 values usually reported. The dates of radiochemical analyses required for decay calculations should be available from the Analytical Sections at ORNL and HW.

This report details 100 Area reactor operation for the time period of August 6 through August 12, 1946.

This is a reference made to a memorandum about the cooperation between the Hanford Site and the US Geological Survey. The US Geological Survey was at the site to work with Hanford on geological problems the site was having. They worked together to locate the water supply wells of the site which would be coordinated with the drilling program. They also worked together on the possible contamination to the 300 and 3000 area wells. (MB)

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Information required by operators exposed to radiation hazards is discussed. All areas of the plant are subjected to radiation hazards similar to those in the radium industry. Personnel in these areas are required to wear pencil meters and special badges that are evidently not solely for identification. They are required to submit to medical examinations more stringent and frequent than usual. They are required to wear heavy gloves in one location, thin gloves in another, disposable hats or rubbers in another. They are required to stay away from familiar objects that they could handle a few days before. They observe health instrument men making readings at points not tangibly influenced by the operations. Under these circumstances, operators cannot perform their duties intelligently without being advised of the general nature of the risks involved. Since the general beta and gamma hazard occurs at nearly all points and cannot reasonably be concealed, this is the feature selected for general information. The special hazard of 105 Building can then be concealed, and the origin, but not the nature of the hazard in 231 likewise concealed.

Hood Worthington reports that slug testing in autoclaves shows improvement to substantiate a meeting on the initial loading of pile B and production for B.F. Babcock report examining five drafts of Operating Standards for the 100 Area. C.W.J. Wende are considering alternative loading schemes due to the observation that lead dummy slugs at the inlet end of a tube may mushroom when subjected to the stress of discharging. J.A. Wheeler reports on heavy metal content of reclaimed slugs compared to normal slugs. Also, temperature measurements on slugs in 105-B and corrosion rates of heavy metals are given. P.F. Gast reports on safety rod control calculations. T.B. Drew report on volume estimations of the B pile and analysis of data from leakage tests. Lastly, W.K. Woods reports on testing of solid aluminium dummies in the W-tube using an electric needle technique to detect motion of the pieces. Water flow considerations are discussed.

On June 29th and July 13th, 1949, the Industrial Hygiene Group of the Health Instrument Divisions at HAPO conducted a study of the health aspects of the degreaser operations carried on in the Airlock adjoining the 105 Building in the 100 H Area. This was done at the request of the Medical Division. The results of the study, together with certain pertinent information concerning degreaser operation, are reported in this report.