The Extraction Method of Purification of Uranyl Nitrate (open access)

The Extraction Method of Purification of Uranyl Nitrate

Technical report. Three extractions of a diethyl ether solution of uranyl nitrate with small portions of water are effective in removing rare earths, as is shown by radio-gadolinium and radio-europium tracer experiments. A study of representative ethers, alcohols, ketones, and esters showed that diethyl ether and a mixture of 85% ethyl methyl ketone with 15% xylene are the best solvents for the extraction.
Date: August 28, 1942
Creator: Myers, L. S., Jr.; Anderson, K. C.; Wexler, Sol & Boyd, G. E.
System: The UNT Digital Library
Examples for Pressure Drop Calculations in Parallel Flow Helium Cooling (open access)

Examples for Pressure Drop Calculations in Parallel Flow Helium Cooling

Pressure drop calculations are shown for He cooled power plants ranging from 400,000 kw to 30,000 kw.
Date: June 18, 1942
Creator: Feld, Bernard T. (Bernard Taub), 1919-1993 & Szilard, Leo
System: The UNT Digital Library
On Certain Phase Equilibria in the Ternary System Uranyl Nitrate--Ether--Water at 25° and at 1°C (open access)

On Certain Phase Equilibria in the Ternary System Uranyl Nitrate--Ether--Water at 25° and at 1°C

This report follows a study that deals with a portion of the ternary diagram previously analyzed, namely the boundary curves which separate the central area of two coexistent liquid phases from the two border stripe representing one-phase liquid systems.
Date: October 22, 1942
Creator: Van Name, Ralph Gibbs
System: The UNT Digital Library
Radiation Problems of the Chemical Plant (open access)

Radiation Problems of the Chemical Plant

"Absorption measurements have been made in a large body of water to evaluate the contribution to the radiation intensity produced by the degradation of radiation without absorption. Radiation intensities three times those expected from a simple exponential absorption were found. Scattering from the air of gamma radiation has been measured and has been found to agree satisfactorily with theoretical predictions. The penetration of radiation through curved pipes in shielding has been measured and been found to be a flat topped function. A 2" pipe bent in the arc of a circle of 7' chord and a 10' radius gives a reduction intensity over the intensity in air at the same distance of 2.5X10⁴."
Date: December 12, 1942
Creator: Borst, Lyle B. & Wollan, Ernest Omar
System: The UNT Digital Library
Capture Cross Section of Si for Thermal Neutrons (open access)

Capture Cross Section of Si for Thermal Neutrons

The following report analyzes different values and measurements that give the same results for the captured cross section of thermal neutrons for Si.
Date: May 6, 1942
Creator: Coon, J. H.
System: The UNT Digital Library
The Use of Sodium Diethyl Dithiocarbamate as a Reagent for the Determination of T (open access)

The Use of Sodium Diethyl Dithiocarbamate as a Reagent for the Determination of T

This report investigates the use of sodium diethyl dithiocarbonate as a reagent for the determination of T.
Date: 1942
Creator: Jones, A. G.
System: The UNT Digital Library
An Attempted Separation of Mercury Isotopes (open access)

An Attempted Separation of Mercury Isotopes

The following document describes the analysis on an attempt at separating mercury isotopes by making their environments as widely different as possible.
Date: April 30, 1942
Creator: Kauzmann, Walter, 1916-
System: The UNT Digital Library
The Preparation of Tungsten Hexafluoride (open access)

The Preparation of Tungsten Hexafluoride

From introductory paragraph: "Because of the possibility that tungsten hexafluoride might occur as an impurity in uranium hexafluoride it seemed worthwhile to prepare some of the material in order to become familiar with its mode of preparation, reactions, etc."
Date: June 1942
Creator: Priest, Homer F. & Colton, R.
System: The UNT Digital Library
Report on Determination of Densities of Several Uranium Compounds (open access)

Report on Determination of Densities of Several Uranium Compounds

This technical report details a process in order to determine the densities of several uranium compounds.
Date: August 10, 1942
Creator: Priest, Homer F. & Priest, G. L.
System: The UNT Digital Library
Measurement of Density of Liquid UF6 (open access)

Measurement of Density of Liquid UF6

This report describes a method and apparatus used to determine the density of liquid sodium hexafluoride. The report includes a drawing of the density cell used in the experiment.
Date: March 29, 1942
Creator: Priest, Homer F.
System: The UNT Digital Library
Effect of Temperature on the Surface of Cast Uranium Metal (open access)

Effect of Temperature on the Surface of Cast Uranium Metal

Technical report. Photomicrographs showing the effect of heating polished uranium surface at 600, 700, 850, and 1000 degrees C, and sandblasted and cut surface at 1000 degrees C are included.
Date: December 3, 1942
Creator: Johns, I. B; Newton, A. S. & Gladrow, E. M.
System: The UNT Digital Library
Interaction of Be with Fission Neutrons (open access)

Interaction of Be with Fission Neutrons

To determine whether or not the (n,2n) reaction in Be would produce a net increase in fission neutrons in a power plant, the distribution of In resonance neutrons slowed down from fission energies in a graphite block was measured with and without a 2" of Be in front of a U3O8 slab undergoing fission. The thermal neutrons producing the fissions were obtained by slowing down neutrons from a cyclotron source. The observed distribution without Be was well represented by a Gaussian source range 36 cm. (corresponding to an initial fission energy of 3 MeV) and a similar sink of range 7.8 cm. The total In resonance intensity with Be was 5% less than without Be. On the assumption that the effect of the Be is entirely due to its different mean free path and moderating power, the In distribution with Be was calculated. Since the m.f.p. as a function of energy is not known for Be, two separate calculations were made using the highest (2.9 cm.) and the lowest (1.80 cm.) possible values for the effective Be m.f.p. Both calculated curves were found to be higher than the observed Be distribution, indicating that at least 10% of the fission neutrons …
Date: April 29, 1942
Creator: Borst, L.; Allison, S. K.; Wheeler, John Archibald, 1911-2008 & Weinberg, Alvin Martin, 1915-2006
System: The UNT Digital Library
Poisoning and Production in a Power Plant (open access)

Poisoning and Production in a Power Plant

The yield of 49, the efficiency of production of 49, and poisoning in a power plant are discussed. Only the crudest of estimates of the poisoning are possible: these indicated that production will probably not be hampered by poisoning. In this case the yield of 49 could be as high as 3 kg/ton but only about 2 kg/ton is compatible with a fairly high efficiency. In the case that production is stopped by poisoning, smaller yields, proportional to the tolerable loss in k, are obtained. In this case the yield will be improved by a factor of 2 or 3 if only the most poisoned parts are extracted and replaced by new uranium.
Date: December 15, 1942
Creator: Ashkin, J.; Christy, Robert F., 1916-2012 & Feld, Bernard T. (Bernard Taub), 1919-1993
System: The UNT Digital Library