From introduction: "Discussion of alternate processes for manufacture of perfluoroxylene as insurance against any eventuality, e.g. disaster, poor quality, required amount of elemental fluorine not obtainable, necessity for further expansion at some future date, or decreasing cost."

Development of certain liquid and solid fluorocarbon compounds with special properties.

From foreword: "Construction of some typical ionization detectors and their operation, with most developed at the Los Alamos Laboratory and a few at other projects connected with the development of the atomic bomb." This report includes chapters 8-16 and an appendix to the second part.

This report discusses the multi-channel pulse analyser including its components and operation.

From cover page: This document has been assigned the above MDDC (Manhattan District Declassification) number, as given in the List of Declassified Documents issued semi-monthly by the Research Division, Manhattan District. In the case of Los Alapnos reports, LADC (Los Alamos Declassification) numbers are listed on the title page if known. This declassified document may differ materially from the original classified document by reason of deletions necessary to accomplish declassification. Hence, this copy of a declassified document does not constitute authority for declassification of classified copies of a similar document which may bear the same title and authors. Reference is made to District Circular Letter (Research Control 47-3) dated 31 October 1946, subject: "Instructions for Use of List of Declassified Documents," which outlines the procedure by means of which declassification of classified copies may be effected. Every effort has been made to reproduce with accuracy of detail the declassified document as certified for declassification. No corrections or changes have been made in the content of the document.

This is a technical drawing of an oscilloscope camera.

This report contains drawings of the dry box.

The following report is a collection of drawings depicting the general structure of the Los Alamos oscilloscope cameras.

Abstract: Since the viscosity-temperature relationships of fluorocarbons are somewhat unusual, when compared to hydrocarbons, for example, it was decided to measure the viscosities, at several temperatures, of various fluorolube oils. The calculation of the viscosity of a blend of oils is at best an uncertain operation, varying considerably with the method used. A comparison of various methods was indicated, in order that reasonably accurate values might be assumed for theoretical composites. The densities were measured at corresponding temperatures for use in converting viscosities, and for their value, per se.

Abstract: This technical report consists of series of drawings of the instrument with the following explanation. The modification of the Simpson Methane flow proportional counter consists of a means for inserting and replacing samples into the chamber through an air-lock device which avoids the introduction of even a small quantity of air into the active volume of the chamber. This is accompanied by sweeping out the small volume of the air-lock containing the sample with methane gas before the sample is introduced into the chamber -- this sweeping out requiring only a few seconds. The mechanical construction is somewhat simplified over that employed in the Simpson counter design, although the electrical and counting characteristics are essentially duplicates of those employed in the Simpson version. Voltage plateaus about 400 volts long, flat within 1% per 100 volts are obtained with the counter, with the operating point at about 2500 volts for methane at one atmosphere pressure. A plateau extending over a range of about 40% variation in amplification factor is obtained. Standard samples have been checked to standard deviation of +/-0.3% over a period of one year. The counter is rather gas-tight and is ready for use within about ten minutes …

This technical report consists of day by day experimental data reported in Engineer's Log book, Electro-Chemistry Department, supporting Report No. EC-11 dated November 15, 1944, by W. L. Grube, Research Laboratories Division, General Motors Corporation.

This technical report contains day by day experimental data reported in Engineer's Log Book, Electro-Chemistry Department, supporting Report No. EC-11 dated November 15, 1944, by W. L. Grube, Research Laboratories Division, General Motors Corporation.

Technical report describing a procedure for the determination of lead in pitchblende. The procedure was determined as needed in the course of an investigation of the processing of pitchblende for the production of uranium. Summary: The volumetric dichromate method for the determination of lead was selected from among several methods investigated as being best suited for a rapid determination of lead in pitchblende. The method as described is accurate to within 1% and it does not require the application of an empirical factor as suggested by Willard and Diehl for this determination.

Introduction. The main objective of the Metallurgical Project was the preparation of large quantities of plutonium 239, an isotope of element 94, by the interaction of neutrons and uranium. At the beginning, only predictions of its chemical and biological properties could be made since it is a new element. It was predicted that it would be toxic to tissue by virtue of its high atomic weight, and in addition, that it would be toxic by virtue of its radioactivity. Thus, the preparation and use of the element on a large scale meant the manipulation of, and possible exposure to, toxic quantities. It was, therefore, of practical importance to obtain data which would elaborate on the predicted toxicity. The objectives of the work reported here were to establish the acute toxicity of plutonium in experimental animals and to study the distribution of the element in the body after the administration of a wide range of doses. In the interest of economy of what was, at that time, a rare substance, and of animals and facilities, these two objectives were frequently pursued in the same experiment. The information obtained from the separate experiments is therefore frequently incomplete in one or another respect. …

Technical report regarding he purpose of the investigation was to evaluate the Chicago mass spectrograph as an analytical instrument for solids.

Abstract: In the NaF-UF4 system the following intermediate phases have been found: NaUF5, -Na2UF6, -Na2UF6 and NacUF7. NaLaF4 is the only intermediate phase observed in the system NaF-LaF3. In the course of an incomplete study of the system NaF-ThF4 the phases NaTh2F9, -Na2ThF6, -Na2ThF6 and Na4ThF8 have been observed. Crystal structure data are given for all the phases.

Redux is a thermosetting synthetic resin manufactured by the Resinous Products & Chemical Co., Washington Square, Philadelphia 5, Pa. According to the manufacturer, it is intended for bonding metal to metal and metal to wood. It was apparently intended to replace rivets in aircraft structural parts and recent information indicates that a British airplane, the DeHaviland Dove, is in production using this resin. The adhesive was originally developed in England by Aero research Ltd. Experience at this laboratory has been confined to use of the resin for bonding electrical grade silicon steel laminations. Very strong bonds have been obtained under properly controlled conditions. The bond strength is sufficient to tear 29 gauge (.014") steel when attempting to peel off individual laminations. The bond is sufficiently homogeneous to prevent leaks parallel to the plane of the laminations into a high vacuum system. Experiments at the laboratory have been designed to test the adhesive for use in bonding the laminations which form the pole tips and vacuum chamber lids for the synchrontron magnet.

The emf of galvanic cells at high temperatures was measured using uranium metal in equilibrium with its chloride as one half of the cell, the other half of the cell being some reference electrode such as silver - silver chloride. Several designs of cells tried are described. A value of 2.83 volts/eq. at 1170[degree]K and also at 990[degree]K is considered as the most probably value for the potential of the uranium halide couple.

Abstract: Exposure of Sprague Dawley white rats to single doses of 900 kvp X radiation demonstrated a medium lethal dose of 600 r which was not markedly dependent upon sex, weight, or, in the case of females, stage of the estrous cycle at the time of irradiation. Deaths within 30 days were most frequent between the fourth and eighth, and between the tenth and fifteenth post- irradiation days, indicating the existence of at least two processes leading to death in the "acute" period.

Report describing results of experiments that involved injecting radioactive yttrium into animals: "The excretion, retention, and distribution of the yttrium was measured, and its effect on survival and growth was observed. The average total excretion of Y91 to the time of death (from 76 hours to 24 days) was a little less than 30 per cent of the injected dose" (p. 2).

Abstract: In the Biology Division, the maintenance of animals containing radioactive materials posed many problems. In addition to routine care of the animals, protection had to be provided for the personnel who worked with the contaminated animals. Frequent air changed in the room in which the animals were caged were necessary: farm workers were required to wear masks; animal cages were checked regularly for radiation; acid was used on the sawdust in the excrete pens; and a new, more efficient type of cage was designed. The most import feature of the new cage was that the support for the screen floor was outside the confines of the cage. Stainless steel was the preferred metal for case construction. Photographs and working drawings of cages for mice, rats, guinea pigs, rabbits, and goats, and several types of metabolism cases are included in this paper. Cage decontamination was accomplished with the aid of complexing agents such as citric acid or sodium tartrate. Under certain conditions, nitric acid was used.

This report describes observations of a sample of Carbon-14, or radiocarbon, made using the method of mass spectrometry.

This two page report discusses the processes followed and findings of an effort to estimate the minimum amount of hydrogen peroxide concentrations required for the formation of a precipitate in 50 percent solutions of uranyl nitrate and uranyl sulfate containing various concentrations of excess anion as acid. The report contains a table detailing the results.

This report details an experiment undergone to determine the amount of radioactive strontium, barium-lanthanum, fission mixture, and sodium accumulated by and distributed within non-feeding goldfish. The report includes tables detailing the findings.