The Chelate Process:  [Part] 5.  Investigation in Horizontal Extractors (open access)

The Chelate Process: [Part] 5. Investigation in Horizontal Extractors

The recovery of plutonium has been demonstrated in a laboratory countercurrent horizontal extractor using the TTA process. Using three extractive stages and two washing stages in each step, a recovery of 91 percent has been obtained in the chelation step and a recovery of 99.9+ percent in the de-chelation step. With five extractive stages, recoveries of 94-98 percent have been found for the chelation step.
Date: July 29, 1949
Creator: Hicks, T. E.; Rubin, B. & Vermeulen, T.
System: The UNT Digital Library
Urine Analysis for Tritium Oxide (open access)

Urine Analysis for Tritium Oxide

This report analyzes a procedure based on the production of acetylene from the active water, with subsequent measurement of the ionization caused by the tritium beta particle. This eliminates the troublesome absorption on the chamber walls when hydrogen is used, and provides a rapid method for the preparation of the urine samples.
Date: July 27, 1949
Creator: Healy, J. W.
System: The UNT Digital Library
Progress Report: June 1949: Preparation of Ductile Zirconium (open access)

Progress Report: June 1949: Preparation of Ductile Zirconium

Report discussing progress made in testing methods for preparation of ductile zirconium by the National Research Corporation for the month of June, 1949.
Date: July 26, 1949
Creator: DiPietro, W. O.; Findlay, G. R. & Mellen, G. L.
System: The UNT Digital Library
Rate of Burnout of Absorbers (open access)

Rate of Burnout of Absorbers

Report discussing change in absorptivity of some rare earth elements over time.
Date: July 19, 1949
Creator: Gillette, P. R.
System: The UNT Digital Library
Progress Report: May 1949: Preparation of Ductile Zirconium (open access)

Progress Report: May 1949: Preparation of Ductile Zirconium

Report discussing progress made by the National Research Corporation regarding preparation of ductile zirconium during the month of May, 1949.
Date: July 8, 1949
Creator: DiPietro, W. O.; Findlay, G. R. & Mellen, G. L.
System: The UNT Digital Library
Mound Laboratory Liquid Waste Disposal Research Quarterly Report for April 1 - June 30, 1949 (open access)

Mound Laboratory Liquid Waste Disposal Research Quarterly Report for April 1 - June 30, 1949

The following report is a quarterly report by the Monsanto Chemical Company for liquid waste disposal research, covering the period between April 1 to June 30, 1949.
Date: July 1, 1949
Creator: Monsanto Chemical Company
System: The UNT Digital Library
The Isolation and Properties of Curium (open access)

The Isolation and Properties of Curium

From introduction: "The discovery of element number 96, curium, was realized by the preparation and identification of the isotope Cm-242 by G. T. Seaborg, R. A. James and A. Ghiorso by cyclotron bombardment of Pu-239 with helium ions."
Date: July 28, 1948
Creator: Werner, Louis Bernard
System: The UNT Digital Library
Artificial Radioactive Isotopes of Cerium and Lanthanum (open access)

Artificial Radioactive Isotopes of Cerium and Lanthanum

The following document describes some studies of the radioactive isotopes of cerium and lanthanum lying on the light or neutron-deficient side of stability.
Date: July 20, 1948
Creator: Chubbuck, James B.
System: The UNT Digital Library
Redox Process Chemistry: Freezing Point Data for UNH - NH₄NO₃ - HNO₃ - H₂O Systems (open access)

Redox Process Chemistry: Freezing Point Data for UNH - NH₄NO₃ - HNO₃ - H₂O Systems

Report presenting data on freezing point for UNH - NH₄NO₃ - HNO₃ - H₂O Systems. A range of concentrations of systems was used and data is presented.
Date: July 7, 1948
Creator: Harmon, M. K. & Cooper, V. R.
System: The UNT Digital Library
Results of Some Statistical Tests of Particle Detectors (open access)

Results of Some Statistical Tests of Particle Detectors

Abstract: The value of routine statistical tests of counter performance in the field has been investigated. The necessity for more elaborate statistical tests than those now used at the Hanford Works has not been indicated by this work.
Date: July 1948
Creator: Portch, W. R. & Whipple, G. H., Jr.
System: The UNT Digital Library
Acute Radiotoxicity of Injected Yttrium91 (open access)

Acute Radiotoxicity of Injected Yttrium91

Report describing results of experiments that involved injecting radioactive yttrium into animals: "The excretion, retention, and distribution of the yttrium was measured, and its effect on survival and growth was observed. The average total excretion of Y91 to the time of death (from 76 hours to 24 days) was a little less than 30 per cent of the injected dose" (p. 2).
Date: July 31, 1947
Creator: Anthony, David S.
System: The UNT Digital Library
The Emf of Cells with Uranium: Uranium Halide Couples in Fused Salt Electrolytes (open access)

The Emf of Cells with Uranium: Uranium Halide Couples in Fused Salt Electrolytes

The emf of galvanic cells at high temperatures was measured using uranium metal in equilibrium with its chloride as one half of the cell, the other half of the cell being some reference electrode such as silver - silver chloride. Several designs of cells tried are described. A value of 2.83 volts/eq. at 1170[degree]K and also at 990[degree]K is considered as the most probably value for the potential of the uranium halide couple.
Date: July 31, 1947
Creator: Eastman, E. D. (Ermon Dwight), 1891-1945.; Campbell, J. A.; Cubicciotti, D. D. & Sienko, Michell J.
System: The UNT Digital Library
Problems of Air-Borne Contamination in Handling of Pu F₄ Powders (open access)

Problems of Air-Borne Contamination in Handling of Pu F₄ Powders

Abstract: Studies were made of the air-borne contamination present during the operation of reducing plutonium tetrafluoride powder to the metal. Equipment design changes were made and operation technique changes were made until the amount of contamination present during operations was well below tolerance levels.
Date: July 31, 1947
Creator: Kennedy, William R.; Dumrose, A. & Ludwig, A.
System: The UNT Digital Library
Studies of Liver Function in Experimental Animals With Special Reference to Radiation and Metal Exposure (open access)

Studies of Liver Function in Experimental Animals With Special Reference to Radiation and Metal Exposure

Report discussing experiments investigating the effects of radiation and metal toxicity on the function of the liver, kidneys, adrenals, and bone marrow of experimental animals.
Date: July 31, 1947
Creator: Schwartz, Samuel; Schneider, Lorraine; Porter, Lillie Mae; Tinsley, Mary & Wallace, Jean
System: The UNT Digital Library
Factors Affecting the Penta-Ether Extraction Uranium (open access)

Factors Affecting the Penta-Ether Extraction Uranium

This report discusses the contributions of the workers at Tennessee Eastman Corporation in the investigation of limiting conditions in the application of penta-ether (aka. dibutoxytetraethylene).
Date: July 25, 1947
Creator: Musser, D. F.; Krause, D. P. & Smellie, Robert H.
System: The UNT Digital Library
Solvent Extraction (open access)

Solvent Extraction

Report discussing methods and theories of solvent extraction. Factors that influence solvent extraction, such as the distribution coefficient, relative solubility, and physical properties of the solvent, are discussed as well.
Date: July 18, 1947
Creator: Smellie, Robert H., Jr. & Krause, D. P.
System: The UNT Digital Library
Modified Simpson Methane Flow Proportional Alpha Counter and Fission Counter (open access)

Modified Simpson Methane Flow Proportional Alpha Counter and Fission Counter

Abstract: This technical report consists of series of drawings of the instrument with the following explanation. The modification of the Simpson Methane flow proportional counter consists of a means for inserting and replacing samples into the chamber through an air-lock device which avoids the introduction of even a small quantity of air into the active volume of the chamber. This is accompanied by sweeping out the small volume of the air-lock containing the sample with methane gas before the sample is introduced into the chamber -- this sweeping out requiring only a few seconds. The mechanical construction is somewhat simplified over that employed in the Simpson counter design, although the electrical and counting characteristics are essentially duplicates of those employed in the Simpson version. Voltage plateaus about 400 volts long, flat within 1% per 100 volts are obtained with the counter, with the operating point at about 2500 volts for methane at one atmosphere pressure. A plateau extending over a range of about 40% variation in amplification factor is obtained. Standard samples have been checked to standard deviation of +/-0.3% over a period of one year. The counter is rather gas-tight and is ready for use within about ten minutes …
Date: July 9, 1947
Creator: Freedman, M. S.
System: The UNT Digital Library
The General Picture of Irradiation Damage to Tissues (open access)

The General Picture of Irradiation Damage to Tissues

The following report is divided into two parts, both parts center around the effects of radiation on skin tissue. Part one focuses on superficial radiation, or Beta rays, while part two is on penetrating radiation, or neutrons and gamma rays.
Date: July 8, 1947
Creator: Henshaw, Paul S. & Snider, Ray S.
System: The UNT Digital Library
High-Frequency Pulse Generator (open access)

High-Frequency Pulse Generator

Introduction: "The purpose of this work was to develop a high-frequency pulse generator that could be used in conducting research on high-rate trigger pairs and scaler circuits. The need for an instrument of this type arose because there was no parallel commercial instrument having this type arose because there was no parallel commercial instrument having a pulse recurrence frequency over approximately 200,000 pulses per second."
Date: July 3, 1947
Creator: Ohmart, Philip E.
System: The UNT Digital Library
Beta-Counting Methods Applied to the Determination of Uranium in Low-Grade Ores (open access)

Beta-Counting Methods Applied to the Determination of Uranium in Low-Grade Ores

The following report covers investigations on the application of the beta counter as an analytical tool for use in experiments on the extraction and concentration of uranium from low-grade (.005-.02 % uranium) shale and phosphate rock ores.
Date: July 1947
Creator: Doig, J. R.; Igelsrud, Iver; Nelson, H. R. & Schwartz, C. M.
System: The UNT Digital Library
The Spectrographic Determination of Iron in Uranium and Its Compounds (open access)

The Spectrographic Determination of Iron in Uranium and Its Compounds

Abstract: A spectrophotometric determination of iron employing the ferrous-1, 10-phenanthroline complex has been developed. The colored complex is measured at a wave-length where interference of the yellow uranyl ion is a minimum. Recommended procedures and analytical results using these procedures are given. Data are presented which indicate that the iron in the acid-insoluble residue is negligible. A method for the determination of iron in ammonium oxalate is included.
Date: July 1947
Creator: Fassel, Velmer A.; Tuthill, S. M. & Buckheim, O. J.
System: The UNT Digital Library
Influence of Total Surface Beta Irradiation on the Gross Metabolic Pattern of Rats (open access)

Influence of Total Surface Beta Irradiation on the Gross Metabolic Pattern of Rats

The following report records the study of albino rats subjected to beta rays and analyzes the skin reactions and metabolic patterns.
Date: July 30, 1946
Creator: Anderson, Elizabeth
System: The UNT Digital Library
Factors Affecting the Extraction of Uranium with Dibutyl Carbitol (open access)

Factors Affecting the Extraction of Uranium with Dibutyl Carbitol

Abstract: "This is a compilation of the material in several reports on the extraction of uranium from aqueous solutions with dibutyl carbitol. Data is presented concerning the optimum conditions for the extraction of the uranium and elimination of impurities."
Date: July 8, 1946
Creator: Weaver, Boyd S. & Larson, C. E.
System: The UNT Digital Library
Factors Affecting the Precipitation of Uranium Peroxide (open access)

Factors Affecting the Precipitation of Uranium Peroxide

Abstract: "This is a compilation of the data on uranium peroxide precipitations appearing in several reports. The solubility product is measured. The effect of many individual ions on the hydrogen peroxide decomposition rate and the complexing of uranium is demonstrated. Studies on plant and other highly contaminated solutions are not included."
Date: July 8, 1946
Creator: Mogg, D. W. & Larson, C. E.
System: The UNT Digital Library