This report analyzes a procedure based on the production of acetylene from the active water, with subsequent measurement of the ionization caused by the tritium beta particle. This eliminates the troublesome absorption on the chamber walls when hydrogen is used, and provides a rapid method for the preparation of the urine samples.

Report discussing change in absorptivity of some rare earth elements over time.

A report which intends to acquaint the reader with the planning of the radiochemical laboratory designed for the analytical control of the radiolanthanum process and to define the terminal status of the design of this laboratory and its equipment.

Report presenting data on freezing point for UNH - NH₄NO₃ - HNO₃ - H₂O Systems. A range of concentrations of systems was used and data is presented.

"The purpose of this present document is twofold: (1) To acquaint the reader with the planning of the radiochemical laboratory designed for the analytical control of the Radio-lanthanum Process. (2) To define the terminal status of the design of this laboratory and its equipment."

Report describing the results of the cupferron extraction-copper spark method in determining the impurity elements in plutonium metal. This was required the 234-5 Project analytical program.

Summary: "The quantity of water adsorbed by graphite at various relative pressures has been determined and the data are presented in graphical and tabular form."

Introduction: "The observations reported in this document were obtained by C.H. Pitt during his assignment to the Corrosion Group September through October 1951. The tubes examined were: 1.) 0893-F Discharged for corrosion examination after leaking; 2.) 1488-DR Discharged to determine caused of obstruction; 3.) 2276-D Discharged for corrosion examination; 4.) 2376-D Discharged for corrosion examination; 5.) 1185-H Discharged to evaluate the effect of magnesium front dummies."

From abstract: "The present paper proposes a lattice test pile, (or LTP) as an alternate to the continuing program of building up and tearing down of exponential piles."

"The following is an alphabetical listing of terms and units in common usage at HAPO. Other terms and definitions may be added as the need becomes apparent or as revisions or additional terms are issued by the NCRP and ICRP."

From introduction: "The purpose of this report is to summarize some of the observations on the dispersion and rate of disengaging of liquid-liquid systems and suggest some possible lines of future work."

Report describing methods of determining trace impurities in plutonium in connection with the Metal Fabrication Process. The methods included are the cupferron extraction-copper spark method and the direct copper spark method.

Abstract: "A method has been devised and successfully used for marking a leaking pile process tube prior to its removal from the pile, such that subsequent location of the leak is more easily accomplished. An acetone solution of Testor's Dark Red Airplane Dope is poured into the suspect tube. The solution leaks from the hole and stains the surrounding area a light pink. To date the method has been used on tubes 3573F, 0486F, 0867F, and 3670F."

The following report observes infrared measurements in the region of OH bands, the C2O band vicinity, the low frequency end of the spectrum, and the region of the UO2 band on the system hexone - water - uranyl nitrate.

This report discusses properties and data regarding the neutralized and concentrated aqueous waste produced during studies of the tributyl phosphate (TBP) solvent extraction process.

This report follows work with the purposes of determining the minimum amount of nitric acid required to dissolve slurries of stored metal waste, determining the stability of such metastable solutions as a function of their chemical compositions - primarily acidity - versus time and temperature, and to define a feed suitable for a low-acid TBP process flowsheet, and to indicate the range of variations in composition which can be tolerated for plant operation.

The following report records a total of forty-nine graphite core samples that have been bored from process tube blocks in the Hanford piles with the intention to provide results to indicate that core boring is an entirely practical operation over bore scraping in obtaining powder samples.

The following report discusses a method developed by Broida and Moyer, the method describes an emission spectrometer procedure for the determination of the ratio 100 D/(H4D).

From introduction: "The prime motive behind the experiments described in this report and in those preceding it in this series is the desire to reduce the number of Redox cycles necessary for decontamination from fission products of the plutonium and uranium streams sufficient to allow final disposition of these two products...This report deals with the mechanics of manganese dioxide handing, laboratory development of manganese dioxide scavenging, and a series of experiments at multicurie level combining ruthenium volatilization and manganese dioxide scavenging in stainless steel equipment."

Abstract: The data obtained from the radioassay of fish collected in vicinity of the Hanford Works between April, 1948 and June, 1950 are presented. Most of the radioactivity in the fish resulted from the concentration of p32 in the scales, bone, and certain visceral organs. The level of activity density in the fish was influenced by size, feeding habits and metabolic rate in addition to the activity density of the water. Changes in operation of nuclear reactors have resulted in progressive increases in activity densities of fish from one year to the next. The levels of radioactivity are not sufficiently high to be hazardous to either the fish or persons eating them.

A preliminary report has shown the potential importance of organic reactor coolants to Hanford technology. The salient points are complete avoidance of corrosion problems and accomplishment of DPR performance with low pressure technique. The recommendation of the report that loop tests be made at Hanford is to be acted upon by Recirculation Technology Unit as soon as organic coolant material is received. To insure starting this experimental work fully abreast of the information available, a trip to sites working with organic coolants was made. Specifically, data were sought on practical details of design for handling organic coolants, heat transfer and fouling characteristics, corrosion of materials, and hazards of handling organics.

Contemplated higher tube power for future reactor operation will probably require a fuel element jacketing material more corrosion resistant than presently available aluminum alloys. Zirconium and its alloys are generally regarded as the most promising jacketing candidates for high temperature operation, particularly for exposures of long duration. In order to obtain assembly, welding, and corrosion data, twenty Al-Si bonded and twenty unbonded Zircaloy fuel elements were prepared for KER loop testing. This report describes the technique developed to weld Zircaloy jacketed fuel elements and presents the results of end closure corrosion testing and metallographic examination.

The dependence of the resonance integral for thorium upon geometry and thorium temperature has been determined through reactivity coefficient measurements performed in the Hanford Test Pile. The geometry dependence was investigated using thorium cylinders of various diameters in the form of solid elements and shells. The temperature dependence (Doppler broadening) was studied by heating thorium elements and permitting them to cool while observing the change in pile reactivity.

Neutron attenuation in the old pile shields is dependent more and more on the slowing down characteristics of the iron as the hydrogen is baked out of the masonite. For neutrons above 1 or 2 Mev, iron does a good job by inelastic scattering. However, below this energy attenuation can be done only by the gradual moderation by elastic scattering to thermal energies with subsequent capture in the iron. Since iron is heavy and thus a poor moderator, there is a good possibility that many neutrons of intermediate energy will leak out of a burned out shield. Also, iron has a large dip in its cross section at 25 Kev which might allow a large burst of neutrons at this energy to leak out. Measurements using a lucite moderator with gold foil detectors indicate a large leakage of neutrons of intermediate energy, but interpretation of these measurements is difficult. These considerations prompted an attempt to get a rough idea of the energy distribution of the leakage neutrons through pure iron using a simple qualitative theory.