Report describing the results of the cupferron extraction-copper spark method in determining the impurity elements in plutonium metal. This was required the 234-5 Project analytical program.

Report describing methods of determining trace impurities in plutonium in connection with the Metal Fabrication Process. The methods included are the cupferron extraction-copper spark method and the direct copper spark method.

This report follows work with the purposes of determining the minimum amount of nitric acid required to dissolve slurries of stored metal waste, determining the stability of such metastable solutions as a function of their chemical compositions - primarily acidity - versus time and temperature, and to define a feed suitable for a low-acid TBP process flowsheet, and to indicate the range of variations in composition which can be tolerated for plant operation.