The Coulometric Titration of 8-Hydroxyquinoline (open access)

The Coulometric Titration of 8-Hydroxyquinoline

Abstract: "A new method of determining 8-hydroxyquinoline by titration with electrolytucally-generated bromine has been developed. Results show good precision in the range 0.4 mg. to 1.6 mg. total 8-hydroxyquinoline, with 99% confidence limits of less than +/- 2%. An electronically-regulated constant current source, required by the method, is described. A new indicator system with high sensitivity to free bromine is discussed."
Date: June 16, 1949
Creator: Carson, W. N.
System: The UNT Digital Library
Determination of Organic Acids in Process Solutions (open access)

Determination of Organic Acids in Process Solutions

Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated potentiometrically with standard potassium hydroxide solution. Since nitric acid and organic acids are present, two end points are observed. The potassium hydroxide added between these end points is equivalent to the organic acids. In the titration, CO2 from the atmosphere or in the potassium hydroxide is a source of error. The former was avoided and correction was made for the latter."
Date: June 29, 1949
Creator: Brouns, R. J. & Pollock, C. W.
System: The UNT Digital Library
Fast Neutron Sensitivity of the CP Meter (open access)

Fast Neutron Sensitivity of the CP Meter

Abstract: "The sensitivity to fast neutrons of a CP Meter ionization chamber of the type used for health physics beta and gamma survey measurements has been investigated."
Date: June 10, 1949
Creator: Baker, E. E.; Gydesen, F. R. & Whipple, G. H., Jr.
System: The UNT Digital Library
Redox : Analytical Research Group Report [for] March and April 1949 (open access)

Redox : Analytical Research Group Report [for] March and April 1949

Report discussing the results of research conducted by the Hanford Works Analytical Research Group during the period from March 1949 to April 1949.
Date: June 21, 1949
Creator: Schmidt, H. R.
System: The UNT Digital Library