Abstract: An investigation was conducted to determine the absorption and translocation of fission products by Russian thistle from a localized spot of contaminated soil. The amount and identity of the radioactive elements absorbed and translocated by the Russian thistle is given along with the location of these elements in the plants. Beta radioactivity to the amounts of 10 microcuries per gram caused no visible effects on the growth habits of sectioned material are included.

The following document describes data collected from a 14-month period of analyzing crustaceans containing radioactivity. Provided is information based on the change of radioactivity through seasonal changes.

From statement of objectives: The purposes of the work described in this report are to provide data useful for designing and operating the dissolver solution clarification equipment to be installed in the Redox production plant.

The following report covers a test with the objective to demonstrate that the plutonium and uranium losses associated with the aluminum jacket dissolution could be reduced by substituting a water wash for the 5 per cent nitric acid wash following the coating removal and that this change would not adversely effect the product yield of decontamination in subsequent process steps.

A new package type facility for corrosion decontamination studies has been designed and fabricated. This report gives a description, drawings, and comments on its operation. It has been in operation since December, 1958.

Introduction:"A corrosion test program in support of the Redox Project was carried out during the second quarter of 1950 to determine the corrosion rates of several austenitic stainless steels in simulated 202-B Waste Storage solution containing HF, HN03, and H2SO4 acids. The results of this program are contained herein and all original data are recorded in laboratory notebook HW-3282-T."

Abstract: "A new method of determining 8-hydroxyquinoline by titration with electrolytucally-generated bromine has been developed. Results show good precision in the range 0.4 mg. to 1.6 mg. total 8-hydroxyquinoline, with 99% confidence limits of less than +/- 2%. An electronically-regulated constant current source, required by the method, is described. A new indicator system with high sensitivity to free bromine is discussed."

A means for decontaminating the primary system of recirculating type reactor is necessary to insure operation and maintenance. This recirculation system can be contaminated by fuel element rupture products and induced corrosion product activities.

In the Sulfex process, stainless steel cladding, generally 304-L, is removed from fuel elements by dissolution in boiling four to six molar sulfuric acid. When cladding removal is complete, the decladding solution is removed is removed to waste. The exposed fuel cores are rinsed and dissolved in nitric acid.

The transfer or circulation of raw dissolver solutions containing gross particulate matter presents many problems not easily overcome by standard pumping equipment. In April of 1956 the HAPO concept of a modified Archimedes screw pump was developed. Two basic models, externally powered and driven through extended shafts, were constructed and tested. Operation of these preliminary models was so satisfactory that a third unit, integrally formed into drive motor, was built and placed in extended life test. This report describes construction and testing of the third and final model.

Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated potentiometrically with standard potassium hydroxide solution. Since nitric acid and organic acids are present, two end points are observed. The potassium hydroxide added between these end points is equivalent to the organic acids. In the titration, CO2 from the atmosphere or in the potassium hydroxide is a source of error. The former was avoided and correction was made for the latter."

The following report examines a rapid method used to eliminate the possibility of explosive perchlorate-organic mixtures in a control laboratory in order to determine radiocesium. These methods include the usage of chloroplatinic acid as a precipitate of radocesium.

Plutonium Fuels Development Basic studies. Experiments to determine the effect of plutonium dioxide additions on the sinterability of UO2 have continued. PuO2 has been added to ball milled PWR grade UO2 as a physical mixture, and in the form of the mixed crystal oxide.

Introduction: "Evidence of masonite deterioration in test hole plugs was interpreted to mean that a previous estimate of the minimum lifetime of the masonite in a Hanford biological shield might be somewhat optimistic. The importance of understanding the effects of radiations on masonite for both present and future pile shields dictated that masonite be sampled from an operating pile shield and studied. The results and techniques are discussed in the following sections of this report."

Abstract: "The sensitivity to fast neutrons of a CP Meter ionization chamber of the type used for health physics beta and gamma survey measurements has been investigated."

At the present time, high-radioactivity-level wastes at Hanford are neutralized and stored as liquid in underground tanks lined with mild steel. This method of storage is relatively inexpensive and is satisfactory on a short-term basis. However, on a long term basis, liquid storage is less desirable than solid storage because of the greater mobility of the liquid. In addition, storage as aa solid would significantly reduce the volume of waste stored. Consequently, various research and development studies have been undertaken in an attempt to develop a practical waste solidification.

The purpose of the Analytical Laboratory Manual is to assemble the basic procedures to be used for the analyses of materials employed within the Fuels Preparation Department. The methods appear in detailed steps suitable for laboratory use. This document replaces the "Essential Material Analytical Manual, " HW-25375 and "Metal Preparation Analytical Manual," HW-30862.

It is being considered that the in-reactor portion of the test section of the PRTR Gas-Cooled Loop Facility consist, in part, of two concentric Inconel-X tubes. The outer tube is the main stress member, with 3.5 O.D. and a wall thickness of 0.065. The inner tube is 3.0 O.D. and has a wall thickness of 0.030. The inner tube provides an annular gas space to serve as thermal insulation.

Introduction: "This report covers progress on the testing of the General Engineering and Consulting Laboratories Turbine Pump No. 1 from May 1, 1948 to Jun 15, 1948. All testing prior to April 30, 1948 has been described in Redox Experiment Testing Report No. 1 (Document HW-9474) and No. 2 (Document HW-9694)."

From summary: "The relative absorptions of X-rays by various substances are listed as a guide to the application of the X-ray photometric method in chemical analysis and to the estimation of interference by extraneous substances."

This report follows an investigation of a cargo truck found contaminated by various radioactive material on a routine trip from Arco, Idaho to the Hanford plant on May 8, 1952. The report analyzes the truck's route in an attempt to find the location of the contaminating region.

At present, emphasis is being given the application of nondestructive testing to the inspection of nuclear fuel in conjunction with complete product specifications. The objective is to quantitatively specify fuel quality parameters, and to measure the entire fuel production against these specifications nondestructively. Under this concept the acceptability of a given fuel element becomes a well-defined factor readily determined by appropriate nondestructive tests.

Zirflex cladding waste is to be neutralized to pH 10 before transfer to waste storage tanks. This treatment causes the precipitation of zirconium oxide or hydroxide, which may lead to flow difficulties during transfer. The purpose of this investigation was to determine the physical properties and flow characteristics of the neutralized slurry to assist in the selectin of satisfactory transfer equipment and storage conditions.

The instability of the steel tank bottom of 113SX waste storage tank was postulated to have been caused by a pressure underneath the steel liner which was in excess of the hydrostatic liquid load of the waste resting on the steel bottom.