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Prediction of Corrosion of Alloys in Mixed-Solvent Environments
Corrosion is much less predictable in organic or mixed-solvent environments than in aqueous process environments. As a result, US chemical companies face greater uncertainty when selecting process equipment materials to manufacture chemical products using organic or mixed solvents than when the process environments are only aqueous. Chemical companies handle this uncertainty by overdesigning the equipment (wasting money and energy), rather than by accepting increased risks of corrosion failure (personnel hazards and environmental releases). Therefore, it is important to develop simulation tools that would help the chemical process industries to understand and predict corrosion and to develop mitigation measures. To create such tools, we have developed models that predict (1) the chemical composition, speciation, phase equilibria, component activities and transport properties of the bulk (aqueous, nonaqueous or mixed) phase that is in contact with the metal; (2) the phase equilibria and component activities of the alloy phase(s) that may be subject to corrosion and (3) the interfacial phenomena that are responsible for corrosion at the metal/solution or passive film/solution interface. During the course of this project, we have completed the following: (1) Development of thermodynamic modules for calculating the activities of alloy components; (2) Development of software that generates stability diagrams …
Date:
June 5, 2003
Creator:
A. Anderko, P. Wang, R. D. Young, D. P. Riemer, P. McKenzie and M. M. Lencka (OLI Systems Inc.) & Laboratory), S. S. Babu and P. Angelini (Oak Ridge National
Object Type:
Report
System:
The UNT Digital Library
Measurement of the Inelastic Proton-Proton Cross-Section at sqrt{s}=7 TeV with the ATLAS Detector
None
Date:
June 5, 2013
Creator:
Aad, Georges
Object Type:
Article
System:
The UNT Digital Library
Electricity: The Road Toward Restructuring
The Public Utility Holding Company Act of 1935 (PUHCA) and the Federal Power Act (FPA) were enacted to eliminate unfair practices and other abuses by electricity and gas holding companies by requiring federal control and regulation of interstate public utility holding companies. Comprehensive energy legislation has passed the House and Senate. The House passed H.R. 6 on April 11, 2003. On July 31, 2003, the Senate suspended debate on S. 14, inserted the text of H.R. 4 (107th Congress) as a substitute, and passed H.R. 6. A conference agreement was reached November 17, 2003, and passed by the House the next day. H.R. 6 includes an electricity title that would, in part, repeal PUHCA, would prospectively repeal the mandatory purchase requirement under PURPA, and would create an electric reliability organization. On June 15, 2004, H.R. 4503, a comprehensive energy policy bill, passed the House.
Date:
June 5, 2002
Creator:
Abel, Amy & Parker, Larry
Object Type:
Report
System:
The UNT Digital Library
RECERTIFICATION OF THE MODEL 9977 RADIOACTIVE MATERIAL PACKAGING
The Model 9977 Packaging was initially issued a Certificate of Compliance (CoC) by the Department of Energy’s Office of Environmental Management (DOE-EM) for the transportation of radioactive material (RAM) in the Fall of 2007. This first CoC was for a single radioactive material and two packing configurations. In the five years since that time, seven Addendums have been written to the Safety Analysis Report for Packaging (SARP) and five Letter Amendments have been written that have authorized either new RAM contents or packing configurations, or both. This paper will discuss the process of updating the 9977 SARP to include all the contents and configurations, including the addition of a new content, and its submittal for recertification.
Date:
June 5, 2013
Creator:
Abramczyk, G.; Bellamy, S.; Loftin, B. & Nathan, S.
Object Type:
Article
System:
The UNT Digital Library
PRECEDENTS FOR AUTHORIZATION OF CONTENTS USING DOSE RATE MEASUREMENTS
For the transportation of Radioactive Material (RAM) packages, the requirements for the maximum allowed dose rate at the package surface and in its vicinity are given in Title 10 of the Code of Federal Regulations, Section 71.47. The regulations are based on the acceptable dose rates to which the public, workers, and the environment may be exposed. As such, the regulations specify dose rates, rather than quantity of radioactive isotopes and require monitoring to confirm the requirements are met. 10CFR71.47 requires that each package of radioactive materials offered for transportation must be designed and prepared for shipment so that under conditions normally incident to transportation the radiation level does not exceed 2 mSv/h (200 mrem/h) at any point on the external Surface of the package, and the transport index does not exceed 10. Before shipment, the dose rate of the package is determined by measurement, ensuring that it conforms to the regulatory limits, regardless of any analyses. This is the requirement for all certified packagings. This paper discusses the requirements for establishing the dose rates when shipping RAM packages and the precedents for meeting these requirements by measurement.
Date:
June 5, 2012
Creator:
Abramczyk, G.; Bellamy, S.; Nathan, S. & Loftin, B.
Object Type:
Article
System:
The UNT Digital Library
DEVELOPMENT OF THE H1700 SHIPPING PACKAGE
The H1700 Package is based on the DOE-EM Certified 9977 Packaging. The H1700 will be certified by the Packaging Certification Division of the National Nuclear Security Administration for the shipment of plutonium by air by the United Stated Military both within the United States and internationally. The H1700 is designed to ship radioactive contents in assemblies of Radioisotope Thermoelectric Generators (RTGs) or arrangements of nested food-pack cans. The RTG containers are designed and tested to remain leaktight during transport, handling, and storage; however, their ability to remain leaktight during transport in the H1700 is not credited. This paper discusses the design and special operation of the H1700.
Date:
June 5, 2009
Creator:
Abramczyk, G.; Loftin, B. & Mann, P.
Object Type:
Article
System:
The UNT Digital Library
Operating Instructions for the UNIVAC Program OCUSOL-A : a Modification of the Eyewash Program
The Eyewash program, written by James H. Alexander and Nancy D. Given, provides solutions of reactor criticality problems in spherical geometry by means of the group diffusion method. It employs thirty lethargy groups (plus one thermal group) in nine regions. The input consists principally of specifying the geometrical scaling factor, boundaries and compositions of the various regions, and temperature level. The output includes the value of vc that would render the system critical, the relative fission density distribution, fissions, absorptions, and leakages in each lethargy group in each region, and, if desired, an edit of the flux at each space point, each lethargy, and an edit of the macroscopic cross sections for each lethargy, each region. OCUSOL-A is a minor modification and extension of Eyewash. It provides for the computation and editing, on the supervisory control typewriter, of the total absorptions in selected nuclides in the various regions. This information is useful in the computation of breeding ratios and the preparation of detailed neutron balances, and in the estimation of flux-averaged cross sections for use in estimating the rate of change of concentration of the various nuclides with burn-up. The program also provides for saving and transferring the final fission …
Date:
June 5, 1957
Creator:
Alexander, L. G.; Carrison, D. A.; Roberts, J. T. & Van Norton, R.
Object Type:
Report
System:
The UNT Digital Library
Plasma Diagnostic Calibration and Characterizations with High Energy X-rays
National Security Technologies’ High Energy X-ray (HEX) Facility is unique in the U.S. Department of Energy complex. The HEX provides fluorescent X-rays of 5 keV to 100 keV with fluence of 10^5–10^6 photons/cm^2/second at the desired line energy. Low energy lines can be filtered, and both filters and fluorescers can be changed rapidly. We present results of calibrating image plates (sensitivity and modulation transfer function), a Bremsstrahlung spectrometer (stacked filters and image plates), and the National Ignition Facility’s Filter- Fluorescer Experiment (FFLEX) high energy X-ray spectrometer. We also show results of a scintillator light yield and alignment study for a neutron imaging system.
Date:
June 5, 2009
Creator:
Ali, Zaheer
Object Type:
Article
System:
The UNT Digital Library
Radiation-induced segregation and the relationship to physical properties in irradiated austenitic alloys.
Radiation-induced changes in composition are studied because these changes can degrade failure of materials irradiated in nuclear reactors. In this work, the effect of alloy composition on radiation-induced segregation, hardening, and void swelling is presented. Five alloys, Fe-18Cr-8Ni, Fe-16Cr-13Ni, Fe-18Cr-40Ni, Fe-16Cr-13Ni+Mo, and Fe-16Cr-13Ni+Mo+P (all compositions in wt. %), were irradiated with 3.2 MeV protons at 400 C to a dose of 0.5 displacements per atom. The change in grain boundary composition was measured using field emission gun scanning transmission electron microscopy and the hardening was measured using Vickers indentation. Void swelling is calculated from the void size distribution measured using transmission electron microscopy. After irradiation, Cr depletes and Ni enriches at grain boundaries. Increasing bulk Ni concentration causes greater Cr depletion and Ni enrichment at grain boundaries. For alloys with 16 Cr, the addition of P reduces the Cr depletion and Ni enrichment. Hardening does not directly correlate with composition, but a framework for isolating the effect of hardening and segregation on cracking is suggested. The amount of void swelling in the irradiated material is shown to correspond inversely with segregation. Those alloys with greater segregation tend to swell less.
Date:
June 5, 2002
Creator:
Allen, T. R.; Cole, J. I.; Was, G. S. & Kenik, E. A.
Object Type:
Article
System:
The UNT Digital Library
Properties of 20% cold-worked 316 stainless steel irradiated at low dose rate.
To assess the effects of long-term, low-dose-rate neutron exposure, tensile, hardness, and fracture properties were measured and microstructural characterization performed on irradiated 20% cold-worked Type 316 stainless steel. Samples were prepared from reactor core components retrieved from the EBR-II reactor following final shutdown. Sample locations were chosen to cover a dose range of 1-56 dpa at temperatures from 371-390 C and dose rates from 0.8-3.3 x 10{sup -7} dpa/s. Irradiation caused hardening, with the ultimate tensile strength (UTS) reaching about 800 MPa near 20 dpa and appearing to saturate at higher doses. The yield strength (YS) follows approximately the same trend as the ultimate tensile strength. At higher dose, the difference between the UTS and YS decreases, suggesting the work-hardening capability of the material is decreasing with increasing dose. The hardness and yield strength increases occur roughly over the same range of dose. While the material retained respectable ductility at 20 dpa, the uniform and total elongation decreased to <1 and <3%, respectively, at 47 dpa. Fracture in the 30 dpa specimen is mainly ductile but with local regions of mixed-mode failure, consisting mainly of dimples and microvoids. The fracture surface of the higher-exposure 47 dpa specimen displays more brittle …
Date:
June 5, 2002
Creator:
Allen, T. R.; Tsai, H.; Cole, J. I.; Ohta, J.; Dohi, K. & Kusanagi, H.
Object Type:
Article
System:
The UNT Digital Library
Pumping-Engine.
Patent for a pumping engine that pumps air, water, oil, or other agents. It was designed to be used for air pumps on locomotives, inflating tires on automobiles, pumping water in steam operated machines, and other uses.
Date:
June 5, 1917
Creator:
Allison, Jesse H.
Object Type:
Patent
System:
The Portal to Texas History
Analysis of Enriched Uranium and Weapons Plutonium Reloads for PWRs Using BRACC
Comparisons of the multicycle results demonstrate that the correlation coefficients based on the CASMO3 data were implemented correctly and that the Linear Reactivity Model is acceptably accurate for missed reloads containing both uranium and weapons plutonium fuel. The expanded set of correlation coefficients make BRACC a useful tool for performing multi-cycle in-core fuel management studies of PWR cores containing weapons plutonium.
Date:
June 5, 1997
Creator:
Alonso, G. & Parish, T. A.
Object Type:
Article
System:
The UNT Digital Library
Three-dimensional thermal analysis of a baseline spent fuel repository
A three-dimensional thermal analysis has been performed using finite difference techniques to determine the near-field response of a baseline spent fuel repository in a deep geologic salt medium. A baseline design incorporates previous thermal modeling experience and OWI recommendations for areal thermal loading in specifying the waste form properties, package details, and emplacement configuration. The base case in this thermal analysis considers one 10-year old PWR spent fuel assembly emplaced to yield a 36 kw/acre (8.9 w/m/sup 2/) loading. A unit cell model in an infinite array is used to simplify the problem and provide upper-bound temperatures. Boundary conditions are imposed which allow simulations to 1000 years. Variations studied include a comparison of ventilated and unventilated storage room conditions, emplacement packages with and without air gaps surrounding the canister, and room cool-down scenarios with ventilation following an unventilated state for retrieval purposes. At this low power level ventilating the emplacement room has an immediate cooling influence on the canister and effectively maintains the emplacement room floor near the temperature of the ventilating air. The annular gap separating the canister and sleeve causes the peak temperature of the canister surface to rise by 10/sup 0/F (5.6/sup 0/C) over that from a …
Date:
June 5, 1980
Creator:
Altenbach, T.J. & Lowry, W.E.
Object Type:
Article
System:
The UNT Digital Library
EPSILON HYPERONS IN THE REACTION K- + P -->+ K+
None
Date:
June 5, 1962
Creator:
Alvarez, Luis W.; Berge, J. Peter; Kalbfleisch, George R.; Button-Shafer, Janice; Solmitz, Frank T.; Stevenson, M. Lynn et al.
Object Type:
Article
System:
The UNT Digital Library
Investigation of moisture-induced embrittlement of iron aluminides. Final report
Iron-aluminum alloys with 28 at.% Al and 5 at.% Cr were shown to be susceptible to hydrogen embrittlement by exposure to both gaseous hydrogen and water vapor. This study examined the effect of the addition of zirconium and carbon on the moisture-induced hydrogen embrittlement of an Fe{sub 3}Al,Cr alloy through the evaluation of tensile properties and fatigue crack growth resistance in hydrogen gas and moisture-bearing air. Susceptibility to embrittlement was found to vary with the zirconium content while the carbon addition was found to only affect the fracture toughness. Inherent fatigue crack growth resistance and fracture toughness, as measured in an inert environment, was found to increase with the addition of 0.5 at.% Zr. The combined addition of 0.5 at.% Zr and carbon only increased the fracture toughness. The addition of 1 at.% Zr and carbon was found to have no effect on the crack growth rate when compared to the base alloy. Susceptibility to embrittlement in moisture-bearing environments was found to decrease with the addition of 0.5 at.% Zr. In gaseous hydrogen, the threshold value of the Zr-containing alloys was found to increase above that found in the inert environment while the crack growth resistance was much lower. By …
Date:
June 5, 1997
Creator:
Alven, D. A. & Stoloff, N.S .
Object Type:
Report
System:
The UNT Digital Library
Insulated Concrete Homes Increase Durability and Energy Efficiency
New houses designed by Mercedes Homes in Melbourne, Florida, with technical support from the U.S. Department of Energy's Building America Program, save their homeowners money by using energy efficient features such as a high performance heat pump and solar control glazing to reduce cooling costs.
Date:
June 5, 2001
Creator:
America, Building; Hendron, B. & Poole, L.
Object Type:
Book
System:
The UNT Digital Library
Baling-Press.
Patent for a baling-press for cotton and uses a compression chamber and a head or compressor block to compress the cotton. The invention is more effective and more expeditious than other baling-presses.
Date:
June 5, 1894
Creator:
Anderson, Alva E.
Object Type:
Patent
System:
The Portal to Texas History
A korarchaeal genome reveals insights into the evolution of the Archaea
The candidate division Korarchaeota comprises a group of uncultivated microorganisms that, by their small subunit rRNA phylogeny, may have diverged early from the major archaeal phyla Crenarchaeota and Euryarchaeota. Here, we report the initial characterization of a member of the Korarchaeota with the proposed name,"Candidatus Korarchaeum cryptofilum," which exhibits an ultrathin filamentous morphology. To investigate possible ancestral relationships between deep-branching Korarchaeota and other phyla, we used whole-genome shotgun sequencing to construct a complete composite korarchaeal genome from enriched cells. The genome was assembled into a single contig 1.59 Mb in length with a G + C content of 49percent. Of the 1,617 predicted protein-coding genes, 1,382 (85percent) could be assigned to a revised set of archaeal Clusters of Orthologous Groups (COGs). The predicted gene functions suggest that the organism relies on a simple mode of peptide fermentation for carbon and energy and lacks the ability to synthesize de novo purines, CoA, and several other cofactors. Phylogenetic analyses based on conserved single genes and concatenated protein sequences positioned the korarchaeote as a deep archaeal lineage with an apparent affinity to the Crenarchaeota. However, the predicted gene content revealed that several conserved cellular systems, such as cell division, DNA replication, and tRNA …
Date:
June 5, 2008
Creator:
Anderson, Iain J; Elkins, James G.; Podar, Mircea; Graham, David E.; Makarova, Kira S.; Wolf, Yuri et al.
Object Type:
Article
System:
The UNT Digital Library
The Work Incentive (WIN) Program Establishment and Early Implementation
This report addresses the Work Incentive (WIN) program
Date:
June 5, 1969
Creator:
Arner, Frederick B.
Object Type:
Report
System:
The UNT Digital Library
Preliminary Investigation of the Transonic Characteristics of an NACA Submerged Inlet
Report presenting an investigation of an NACA submerged inlet operating over a range of mass-flow ratios and oncoming flow angles through a range of Mach numbers by use of a transonic bump. Results regarding the ram-recovery ratio, pressure distributions, and tuft studies are provided.
Date:
June 5, 1950
Creator:
Axelson, John A. & Taylor, Robert A.
Object Type:
Report
System:
The UNT Digital Library
New Evidence From Soudan 1 for Underground Muons Associated With Cygnus X-3
The Soudan 1 experiment has obtained additional evidence for underground muons associated with the x-ray pulsar Cygnus X-3. We report the preliminary analysis of data recorded during the October 1985 radio outburst of Cygnus X-3, which show a significant excess of muons for a narrow range of Cygnus X-3 phases.
Date:
June 5, 1986
Creator:
Ayres, D. S.
Object Type:
Article
System:
The UNT Digital Library
Letter of intent to build an off-axis detector to study nu(mu) ---> nu(e) oscillations with the NuMI neutrino beam
None
Date:
June 5, 2006
Creator:
Ayres, D.; Drake, G.; Goodman, M.; Guarino, V.; Joffe-Minor, T.; Reyna, D. et al.
Object Type:
Report
System:
The UNT Digital Library
DUAL ION EXPOSURE VS. SPLIT-DOSE EXPOSURES IN HUMAN CELL NEOPLASTIC TRANSFORMATION.
Since radiation fields of space contain many-fold more protons than high atomic number, high energy (HZE) particles, cells in astronaut crews will experience on average several proton hits before an HZE hit. Thus radiation regimes of proton exposure before HZE particle exposure simulate space radiation exposure, and measurement of the frequency of neoplastic transformation of human primary cells to anchorage-independent growth simulates in initial step in cancer induction. Previously our group found that exposure to 20 cGy 1 GeV/n protons followed within about 1 hr by a HZE ion (20 cGy 1 GeV/n Fe or Ti ions) hit gave about a 3-fold increase in transformation frequency ([1]). To provide insight into the H-HZE induced increased transformation frequencies, we asked if split doses of the same ion gave similar increased transformation frequencies. However, the data show that the split dose of 20 cGy plus 20 cGy of either H or HZE ions gave about the same effect as the 40 cGy uninterrupted dose, quite different from the effect of the mixed ion H + HZE irradiation. We also asked if lower proton doses than 20 cGy followed 15 minutes later by 20 cGy of HZE ions gave greater than additive transformation …
Date:
June 5, 2006
Creator:
BENNETT, P.V.; CUTTER, N.C. & SUTHERLAND, B.M.
Object Type:
Article
System:
The UNT Digital Library
A process model of natural attenuation in drainage from a historic mining district
A process model was used to better understand the controls on the chemical evolution of drainage in a historic mining district. At the Pecos Mine Operable Unit, New Mexico, drainage near the waste rock pile is acidic (pH varies from 3.0--5.0) and carries high concentrations of Zn, Al, Cu and Pb. As drainage flows toward the Pecos River, pH increases to greater than 7 and heavy metal content decreases. A process model of natural attenuation in this drainage shows the main controls on pH are reaction with a local bedrock that contains limestone, and concurrent mixing with tributary streams. Models that account for both calcite dissolution and mixing reproduce the observed decrease in aqueous metal concentrations with increasing pH. Contaminant concentrations attenuate primarily via two distinct pathways: Al, Cu, Fe and Pb precipitate directly from solution, whereas Zn, Mg, Mn and SO{sub 4} concentrations decrease primarily through dilution. Additionally, Pb adsorbs to precipitating hydroxide surfaces.
Date:
June 5, 2000
Creator:
BERGER,AMY C.; BETHKE,CRAIG M. & KRUMHANSL,JAMES L.
Object Type:
Article
System:
The UNT Digital Library