Strubl's polarographic method for the determination of uranium in the presence of iron can be used for the determination of uranium in plutonium solutions. A hydroxylamine hydrochloride solution (2M) is used as the supporting electrolyte. This reduces the plutonium to the plus three oxidation state without reducing the uranium. The uranium may then be determined polarographically by measuring the height of the uranyl reduction wave (UVI to UV) at -0.35 volts (vs. S.C.E.) applied potential. Solutions with a U/Pu weight ratio as low as 3.5 x 10(-3) were analyzed with an error of less than 2%. This error increased to 6% for solutions of 1 x 10(-3) U/Pu ration and is considerably larger for smaller U/Pu ratios.

The following report analyzes whether there is a difference between the neutron streaming in the "armor plate" and 347 stainless steel.

A spectrometer has been used with a hollow prism electrically heated to 70 C to measure the refractive indices of solutions of uranium hexafluoride in bromine trifluoride and uranium hexafluoride in bromine pentafluoride. The refractive indices of the two binary systems have been expressed as a function of composition.

The results of an experimental pilot study on the location time, for a sequence of N specified positions on a panel, are given for 1 <_ N <_ 30. The positions to be located were randomly arranged on one set of panels and arranged according to an ordering scheme on a second set of panels. Th location time for N positions randomly arranged on a panel varies approximately as N(2). In the case of an order arrangement the location time is essentially proportional to N. Even for as few as 30 positions, the location time for an random arrangement was twelve times greater than for an order panel. For 60 positions the ratio would be 19, and for 90 positions the ratio would be 26.

Electrodialysis in an ion-exchange membrane cell was shown to be technically feasible for the concentration of an azeotropic mixture of HF and water. A flowsheet is presented for recovery of anhydrous HF by distillation and electrodialysis of the azeotropic residue. In the electrodialysis step, 2.6 kwhr of energy per pound of anhydrous product was consumed, with electricity at 1¢ per kilowatt-hour, the total operating cost of the electrodialysis equipment alone, including amortization, would be 6¢ per pound of HF.

Average coefficients of thermal expansion of the temperature range 25 C to approximately 425 C are reported for numerous types of graphite. The dependence of thermal expansion on crystal orientation and crystallite size and the effects of oxidation and cold test hole irradiation are discussed. An empirical relationship between thermal expansion and the initial rate of physical expansion under cold test hole irradiation is formulated.

In early July, 1958, it appeared that Columbia River temperature at HAPO would be near 24.5ºC by the end of August. River temperature were averaging 4º to 5º above 1957 figures and were 3º to 4º above the ten year highs. It seemed desirable to examine the problem to determine if any corrective measure could be taken, since it was apparent that production losses were imminent.

The design of internally cooled electrical coils for the production of high frequency intensity magnetic fields presents many new aspects and combinations of the familiar modes of heat transfer. However, the customary methodology appears to be sufficient for preliminary analysis and understanding of those problems. This methodology comprises the derivation of a qualitative, approximate equation expressing the relative performance of the various parts of a system, followed by an examination of this equation in order to locate the limiting features of the system. These features are then investigated by more powerful methods, which in turn provide guidance for development research in the laboratory.

In the use of a reactor as a device to measure neutron cross sections, the pile oscillator is often employed because of its much higher sensitivity compared to that available in static reactivity measurements. The factor limiting the available in static reactivity measurements. The factor limiting the available sensitivity is the generation of random noise, which originates in the statistical nature of the chain reaction. In other words, the nuclear reactions which maintain the chain reaction do not proceed uniformly, but rather at rates which fluctuate in time around some average values. These fluctuations limit the accuracy of measurements in the reactor.

Hastelloy F is a prime contender as a material of construction for plant dissolvers in the power fuel reprocessing program. Consequently, the fabrication and installation of dissolver was undertaken to delineate any unknown problems associated with the use of Hastelloy F; and, at the same time, to provide a vessel for development studies on the Niflex or the Sulfex processes. The purpose of this report is to describe the actual basis for design as well as to present the problems encountered during the fabrication of the vessels.

In considering the problems associated with the measurement of SSNM content of Non-Production Fuels, two distinct problems are apparent. The first is the technical problem of obtaining highly accurate measurements in a complicated chemical and physical system. The second is the administrative problem of choosing a measurement system which provides a basic of financial settlement acceptable to both the seller (reactor operator) and the buyer (Commission).

The spatial distribution of thermal neutrons in a reactor lattices cell is of fundamental importance for many reasons. First of all, this information allows the determination of the relative absorption rates in each component of the cell which in turn enables a determination of the thermal utilization, and the diffusion length of the lattice. In addition, the observed spatial distributions of thermal neutrons in the lattice cell is of major interest in testing various approximations to the solution of the transport equation such as the P1 and P3 solutions.