Performance characteristics of two activated charcoal columns at room temperature in separating fission-product xenon from an air stream were investigated by installing each column in the exhaust from an enclosure in which irradiated slugs were dissolved. Breakthrough curves are presented and the variation in xenon concentration within the columns is examined. Theoretical treatments of adsorption columns in the literature are found to agree well with the experimental data. Performance of the colunms is evaluated in terms of concentration factor'' and number of effective theoretical plates. (auth)

After two batches (~ 340 kg) of fluoride salt from the ARE were reprocessed, pilot plant operations were terminated because of a leak through which an estimated 780 g of uranium (as UF6) escaped. Of the 21 kg of highly enriched uranium in the feed, 93.12% was collected as UF6 product, 0.13% represented measured losses, and 3.72% was unaccounted for (leak). An additional 3.03% was reclaimed from NaF beds and equipment washes. The product met both chemical purity and activity specifications for product level UF6. Decontamination from fission products was essentially complete. A gross gamma D.F. was apparently limited by the low activity of the feed salt.

Using a high intensity light source to produce chorioretinal lesions in the eyes of rabbits, cats, and guinea pigs, the authors determined, at different levels of retinal irradiance, the exposure time which produced an ophthalmoscopically visible lesion. It was found that, at irradiance levels greater than 2 cal/cm/sup 2/sec, a radiant exposure of 1.0 cal/cm/sup 2/ produced a threshold lesion. At irradiance levels less than 0.7 cal/cm/sup 2//sec, lesions could not be produced at any exposure time through ten seconds. Histological data on the nature of the legions and course of healing are presented and discussed. (auth)

None

The technique of high-frequency titrimetry was applied to the determination of thorium, uranium, sulfate, and free acid. In Part I, the reproducibility of the method for the titration of standard solutions that contained 50 rag of thorium in the absence of interferences is established. Under these conditions, the coefficient of variation of the method was <1%. In Part II, the effect of uranium on the highfrequency titration of thorium, as well as the application of the method to actual samples, is discussed. Uranium in a ratio of 5 to 1 to thorium can be tolerated. When the method is applied to the analysis of representative samples, the coefficient of variation is 1%. Attempts to determine uranium by high-frequency titration with 8-quinolinol were unsuccessful. Tests on this titration and possible reasons for its failure are discussed in Part III. The application of the high-frequency titration method to the determination of sulfate in solutions of uranyl sulfate is described in Part IV. The coefficient of variation, on titrating 40 to 70 mg of sulfate with barium chloride after the uranium is masked with citrate or fluoride, is 2%. In Part V, the high-frequency titration of free acid in solutions of uranyl sulfate …

The technique of high-frequency titrimetry has been applied to the determination of thorium, uranium, sulfate, and free acid. In Part I of this report, the reproducibility of the method for the titration of standard solutions which contained 50mg of thorium in the absence of interferences is established. The coefficient of variation of the method, under these conditions, was found to be less than one per cent. In Part II, the effect of uranium on the high-frequency titration of thorium, as well as the application of the method to actual samples, is discussed. Uranium in a ratio of 5 to 1 to thorium can be tolerated. When the method is applied to the analysis of representative samples, the coefficient of variation is one per cent.

Because of the excessive vertical fragility and high replacement costs of mice-window G-M tubes used in vertical and horizontal lead-pig shelf counters, it was requested that a simple system of conversions to reliable scintillation detection be accomplished.

Document issued by the Office of the Attorney General of Texas in Austin, Texas, providing an interpretation of Texas law. It provides the opinion of the Texas Attorney General, Will Wilson, regarding a legal question submitted for clarification: Constitutionality of H.B. 142, of the 56th Legislature, authorizing the State Parks Board to acquire public sites in proximity to the shores of public lakes, bays and gulfs for recreation purposes.

After two batches ( approximately 340 kg) of fluoride salt from the ARE were reprocessed, a pilot plant operations were terminated because of a leak through which an estimated 780 g of uranium (as UF/sub 6/ escaped. Of the 21 kg of highly enriched uranium in the feed, 93.12% was collected as UF/sub 6/ product, 0.13% represented measured losses, and 3.72% was unaccounted for (leak). An additional 3.03% was reclaimed from NaF beds and equipment washes. The produce met both chemical purity and activity specifications for product level UF/ sub 6/. Decontamination from fission products was essentially complete. A gross gamma decontamination factor was apparently limited by the low activity of the feed salt. (auth)