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Kinetics and mechanism of desulfurization and denitrogenation of coal-derived liquids. Eleventh quarterly report, December 21, 1977-March 20, 1978
Three high-pressure flow microreactors and two batch autoclave reactors have been used to study the reaction networks and kinetics of (1) catalytic hydrodesulfurization of dibenzothiophene and methyl-substituted dibenzothiophenes, and (2) catalytic hydrodenitrogenation of quinoline, methyl-substituted quinolines, acridine, benzacridines, dibenzacridine, and carbazole. The catalysts were commercial, sulfided CoO-MoO/sub 3//..gamma..-Al/sub 2/O/sub 3/, NiO-MoO/sub 3//..gamma..-Al/sub 2/O/sub 3/, and NiO-WO/sub 3//..gamma..-Al/sub 2/O/sub 3/. The results of the experiments are described. (LTN)
Date:
May 20, 1978
Creator:
Gates, B. C.; Katzer, J. R.; Olson, J. H.; Kwart, H. & Stiles, A. B.
System:
The UNT Digital Library
Pressure bonding molybdenum alloy (TZM) to reaction-bonded silicon nitride
Topping cycles could boost the energy efficiencies of a variety of systems by using what is now waste heat. One such topping cycle uses a ceramic helical expander and would require that a reaction-bonded silicon nitride (RBSN) rotor be bonded to a shaft of TZM (Mo-0.5 wt % Ti-0.08 wt % Zr). Coupon studies show that TZM can be bonded to RBSN at 1300/sup 0/C and 69 MPa if there is an interlayer of MoSi/sub 2/. A layer of finely ground (10 ..mu..m) MoSi/sub 2/ facilitates bond formation and provides a thicker bond interface. The hardness and grain structure of the TZM and RBSN were not affected by the temperature and pressure required to bond the coupons.
Date:
May 20, 1978
Creator:
Huffsmith, S. A. & Landingham, R. L.
System:
The UNT Digital Library