Identification of Reaction Products Formed During Magnesium Reduction of Uranium Tetrafluoride: Report (open access)

Identification of Reaction Products Formed During Magnesium Reduction of Uranium Tetrafluoride: Report

Abstract: "This report describes the results of X-ray diffraction examination of reaction products from a series of experiments performed by Mallinckrodt Chemical Works as an acid in understanding the process of bomb reduction of UF4. UF4 is initially reduced to UF3 by magnesium at 560 C., and subsequently to metal at 600 C. MgF2 from the initial reaction forms a coating on the magnesium which retards the final spontaneous reaction."
Date: May 15, 1953
Creator: Schwartz, C. M. & Vaughan, D. A.
Object Type: Report
System: The UNT Digital Library
The Identification of the Angular Inclusions Present in Rolled Uranium (open access)

The Identification of the Angular Inclusions Present in Rolled Uranium

Hanford uranium contains minute angular inclusions which affect the microstructure, reactivity, and other important factors controlling the serviceability of the metal. Small quantities of the inclusions have been isolated by chemical means, and the x-ray diffraction patterns and chemical analyses of the isolated materials have been determined. As a first step in the identification of the inclusions present in rolled uranium, a search was made for a chemical method of separating the inclusions from the matrix metal.
Date: May 15, 1953
Creator: Scott, F. A.
Object Type: Report
System: The UNT Digital Library
Removal of the Compound Layer From Decanned Hanford Uranium Slugs by the Use of Sodium Hydroxide (open access)

Removal of the Compound Layer From Decanned Hanford Uranium Slugs by the Use of Sodium Hydroxide

About twenty-five to thirty per cent of the uranium slugs canned in the Metal Preparation Section do not meet specifications and are rejected. These rejected slugs are recovered by a chemical process and prepared for re-canning. The current recovery process consists essentially of a sodium hydroxide-sodium nitrate bath for chemically removing the aluminum can and the bonding medium, followed by hydrofluoric acid and nitric acid baths to remove the remaining compound layer and to pickle the slugs before they are returned to the process canning line. Recent studies have indicated the possibility of using a more economical means of recovery. this includes the mechanical removal of the aluminum can and most of the bonding medium, followed by a chemical removal of the residual compound layer by a solution of sodium hydroxide.
Date: May 15, 1953
Creator: Brandt, H. L.
Object Type: Report
System: The UNT Digital Library
TNX Evaporator Incident January 12, 1953 (open access)

TNX Evaporator Incident January 12, 1953

From abstract: "The circumstances are described pertaining to an explosion in a TNX evaporator during the concentration of a uranyl nitrate-nitric acid solution. TBP and Amsco diluent were probably present in the evaporator charge. A laboratory program involving small-scale atmospheric and closed-vessel distillations of various mixtures of UNH, HNO3, Amsco, TBP, and water indicate that an exothermic reaction between TBP and UNH, or between TBP and HNO3, or both, was responsible for the explosion. The danger areas of temperature, TBP concentration, pressure, and heating rate are defined and recommendations are made for safe evaporator operation.
Date: May 15, 1953
Creator: Colven, T. J.; Nichols, G. M. & Siddall, T. H.
Object Type: Report
System: The UNT Digital Library
The Determination of Rare Earths in Thorium (open access)

The Determination of Rare Earths in Thorium

Abstract: "A quantitative method for the determination of individual rare earths in thorium down to a level of 0.05 ppm, is described. The procedure consists of a chromatographic cellulose-columns separation followed by a solution-type spectrographic determination. Values are given for the recovery of a number of rare earths using this combined procedure."
Date: May 15, 1952
Creator: Center, E. J.; Henry, W. M. & Householder, R. D.
Object Type: Report
System: The UNT Digital Library
Investigational Drilling, Hoskinnini Mesa (open access)

Investigational Drilling, Hoskinnini Mesa

From to the files: To date, all the mineralization seen in the Monument Valley area in the Shinarump formation has been in scour channels. The mineralized rock occurs at or near the bottom of the channel. On Hoskinnini Mesa, all the channels examined to date contain some mineralized material. Channels observed may in some cases contain copper without apparent uranium mineralization; others definitely exhibit copper-uranium mineralization.
Date: May 15, 1952
Creator: Chester, John W. & Pitman, R. K.
Object Type: Report
System: The UNT Digital Library
Neutron Distribution Measurements at Pajarito by Means of Photographic Emulsion (open access)

Neutron Distribution Measurements at Pajarito by Means of Photographic Emulsion

A method using photographic emulsions for the study of neutron distributions is described. The construction of a simple machine for producing experimental critical assemblies in which the method has been used is reported. Sources of error are discussed. Curves of the perturbations when small spheres of various materials are placed in the center of the assembly are shown.
Date: May 15, 1952
Creator: Young, Dwight S.
Object Type: Report
System: The UNT Digital Library
Altitude-performance and Reynolds number investigation of centrifugal-flow-compressor turbojet engine (open access)

Altitude-performance and Reynolds number investigation of centrifugal-flow-compressor turbojet engine

From Introduction: "Altitude-chamber and wind-tunnel investigations of the performance of turbojet engines such as those reported in references 1 to 4 have shown that the conventional correction factors fail to generalize the engine performance variables at high altitudes. An investigation was therefore made at the NACA Lewis laboratory to determine the altitude performance of the J33-A-23 turbojet engine and to demonstrate the magnitude of departure of actual altitude performance from that predicted from sea-level performance."
Date: May 15, 1951
Creator: Wilsted, H. D. & Grey, R. E.
Object Type: Report
System: The UNT Digital Library
Combustion performance evaluation of magnesium-hydrocarbon slurry blends in a simulated tail-pipe burner (open access)

Combustion performance evaluation of magnesium-hydrocarbon slurry blends in a simulated tail-pipe burner

Report presenting an experimental investigation to determine the combustion properties of several magnesium-hydrocarbon slurry blends and to indicate the feasibility of the application of slurry-type fuels to high-speed aircraft. High-concentration magnesium slurries showed large improvements in combustion stability and tail-pipe-burner net thrust.
Date: May 15, 1951
Creator: Tower, Leonard K. & Branstetter, J. Robert
Object Type: Report
System: The UNT Digital Library
Development of the Flow Sheet for Incinerating Contaminated Combustible Waste: Engineering Research Final Report (open access)

Development of the Flow Sheet for Incinerating Contaminated Combustible Waste: Engineering Research Final Report

From introduction: This report serves as a recommendation that a full-scale incineration process be installed at Mound Laboratory and provides a complete flow sheet for this process and recommended designs for the critical parts of the processing equipment. It contains justification for the process, a history of the investigation including early work and pilot plant results, an explanation of the values and information given in the flow sheet, and the reasons for the recommended design features.
Date: May 15, 1951
Creator: McEwen, M.; Schauer, P. J. & Aponyi, T.
Object Type: Report
System: The UNT Digital Library
NACA investigation of fuel performance in piston-type engines (open access)

NACA investigation of fuel performance in piston-type engines

This report is a compilation of many of the pertinent research data acquired by the National Advisory Committee for Aeronautics on fuel performance in piston engines. The original data for this compilation are contained in many separate NACA reports which have in the present report been assembled in logical chapters that summarize the main conclusions of the various investigations. Complete details of each investigation are not included in this summary; however, such details may be found, in the original reports cited at the end of each chapter.
Date: May 15, 1951
Creator: Barnett, Henry C.
Object Type: Report
System: The UNT Digital Library
Corrosion of Stellite in Redox Streams (open access)

Corrosion of Stellite in Redox Streams

The following report provides results from laboratory tests on the corrosion resistance of various types of stellite facings on astenitic stainless steel T-347 to Redox streams.
Date: May 15, 1950
Creator: Koenig, W. W.
Object Type: Report
System: The UNT Digital Library
Compilation of Test Data on 111 Free-Spinning Airplane Models Tested in the Langley 15-Foot and 20-Foot Free-Spinning Tunnels (open access)

Compilation of Test Data on 111 Free-Spinning Airplane Models Tested in the Langley 15-Foot and 20-Foot Free-Spinning Tunnels

"A compilation of free-spinning-airplane model data on the spin and recovery characteristics of 111 airplanes is presented. These data were previously published in separate memorandum reports and were obtained from free-spinning tests in the Langley 15-foot and the Langley 20-foot free-spinning tunnels. The model test data presented include the steady-spin and recovery characteristics of each model for various combinations of aileron and elevator deflections and for various loadings and dimensional configurations" (p. 1).
Date: May 15, 1947
Creator: Malvestuto, Frank S., Jr.; Gale, Lawrence J. & Wood, John H.
Object Type: Report
System: The UNT Digital Library
The Deposition of Plutonium and Certain Fission Products in Bone as a Decontamination Problem (open access)

The Deposition of Plutonium and Certain Fission Products in Bone as a Decontamination Problem

The following report discusses the deposition of radioactive elements during a nuclear fission in the skeleton. Studies are concerned with chronic effects of toxic radiation developing within the bone marrow and decontaminating the cells.
Date: May 15, 1946
Creator: Copp, D. Harold; Greenberg, David M. & Hamilton, Joseph G.
Object Type: Report
System: The UNT Digital Library
Analysis of Heavy Water by Equilibration (open access)

Analysis of Heavy Water by Equilibration

Technical report discussing that the deuterium concentration of heavy water can be determined by equilibrating the water with deuterium gas in the presence of a catalyst with subsequent analysis of the equilibrated gas on the mas spectrometer. The apparatus for equilibration analyses maybe be considered in three parts: 1) apparatus for introducing the ingredients into the reaction chambers; 2) the reaction chambers; 3) the mass spectrometer for analysis of the equilibrated gas. The isotopic composition of the deuterium gas to be used as the starting material is primarily governed by what gases are available. In general it is best to use gas within about one percent on either side of the final equilibrium composition. No reaction takes place between deuterium gas and water molecules in the absence of a catalyst. Platinum oxide is used as the catalyst.
Date: May 15, 1945
Creator: Fischer, R. B.; Potter, R. A. & Voskuyl, R. J.
Object Type: Report
System: The UNT Digital Library
Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Month Ending May 15, 1943 (open access)

Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Month Ending May 15, 1943

Technical report that information has bee obtained on the effect of beta and gamma radiation on the electrical resistance of insulating materials The results are summarized. The recovery to original resistance values has been measured. In general, the initial rate is rapid for the first few hours; the rate then decreases sharply. Certain samples show evidence of complete recovery. Effects on mechanical properties of several plastics has also been studied. Data on gas evolution from several organic materials including those suggested by the physiological shield have been extended to include both beta and deuteron bombardments. Samples of "Press-wood" are being evaluated. The effect of current on the H2O2 production in water containing I- has been studied at several I- concentrations. Water contain-dissolved CO2 shows the presence of oxidant (presumably H2O2). H2O2 has been produced by recoil protons from the scattering of fast neutrons in de-oxygenated water. Radioactive solutions do not greatly affect the applicability the glass electrode providing the electrode is thoroughly washed with distilled water before immersion in the standard buffer solution.
Date: May 15, 1943
Creator: Franck, J.
Object Type: Report
System: The UNT Digital Library
Rates of fuel discharge as affected by the design of fuel-injection systems for internal-combustion engines (open access)

Rates of fuel discharge as affected by the design of fuel-injection systems for internal-combustion engines

Using the method of weighing fuel collected in a receiver during a definite interval of the injection period, rates of discharge were determined, and the effects noted, when various changes were made in a fuel-injection system. The injection system consisted primarily of a by-pass controlled fuel pump and an automatic injection valve. The variables of the system studied were the pump speed, pump-throttle setting, discharge-orifice diameter, injection-valve opening and closing pressures, and injection-tube length and diameter.
Date: May 15, 1932
Creator: Gelalles, A. G. & Marsh, E. T.
Object Type: Report
System: The UNT Digital Library