Much of the shielding work carried out with the Bulk Shielding Reactor (BSR) has yielded data of particular interest for the design of swimming pool type reactors, However, it is often difficult for a reactor designer to locate such data since it may be recorded in a report primarily concerned with shielding problems. Therefore, this memorandum presents a bibliography of reports from the Bulk Shielding Facility arranged according to the application of data to the various aspects of reactor design.

Semiannual Progress report of the Oak Ridge National Laboratory Chemistry Division providing updates on various projects, experiments, and other work in inorganic and physical chemistry, nuclear chemistry, organic chemistry, chemical physics, chemistry of separation processes, radiation chemistry, and reactor chemistry.

Progress report of the Oak Ridge National Laboratory Biology Division providing updates on various projects, experiments, and other work. This report includes a summary of scholarly output from the division and departmental activities in cytology and genetics, mammalian genetics and development, microbial protection and recovery, mammalian recovery, pathology and physiology, general physiology, biochemistry, enzymology and photosynthesis, microbiology, plant biochemistry, and biophysics.

Gram amounts of americium were separated quantitatively from kilogram quantities of lanthanum to yield an americium product approaching 90% purity. The remaining impurity was chiefly yttrium. Elution of americium from 25% loaded Dowex 50 resin column with 0.15 M citric acid— 0.10 M diammonium citrate — 0.3 M ammonium nitrate, pH 3.3 gave a product containing 99% of the americium with a La/Am ratio of 1/100 or less in one fourth of a column volume, in this case about 1 100-fold volume reduction. Approximately 9 g of americium was purified by this method. Elution with 12.8 M hydrochloric acid from a 20 to 30% loaded column gave 90% of the americium in two column volumes of product with a La/Am ratio of about 1/4. About 1 g of americium was purified by this method.

Two revised Excer process flowsheets are presented for the production of UF4 from urnayl nitrate solution. In both, the uranium is sorbed on a cation-exchange resin and eluted with aqueous HF. In one, the resulting UO2F2 in dilute HF is mixed with dilute sulfuric or hydrochloric acid and electrolytically reduced in a cation-exchange-membrane cell, and the precipitated UF4·0.75H2O is dried and dehydrated to anhydrous UF4. A cost of 20¢ per pound of reduced uranium is estimated. In the other, ammonium fluoride is also added to the uranyl fluoride solution before the electrolytic reduction step, and the precipitate is UF4·04NH4F. A flowsheet for preparing UF4 from raw ore is also shown. The uranium is sorbed on an anion-exchange resin from a sulfuric acid leach liquor and eluted with dilute HCl. Ammonium fluoride and HF are added to the UO2Cl2-HCl solution before the uranyl ion is electrolytically reduced to precipitate UF4·0.4NH4F. Decontamination factors as high as 45 and 9 for gross beta and gamma activities and of 10 to 5000 for light metal impurities were obtained in the electrolytic reduction step.