This report covers progress in chemical and spectrographic analysis, chemical work, beta-counting methods of analysis, and ore-dressing and pyrometallurgical studies.

Abstract: The output signal of a linear accelerator may have a rise time of 1-2 x 10[minus]7 seconds. Therefore, the output of a pulse height selector operating on this signal has a variation of delay from the original signal of about this amount. In the instrument to be described in this technical report this difficulty is largely resolved.

Abstract: The distillation and residue extraction recovery procedures developed for the recovery of uranium from Kinney and diffusion pump oil, were applied to contaminated precipitron oil. The effectiveness and advisability of using the method, in whole or in part, is discussed, and various recommendations for processing this particular type of oil are presented. Additional contaminating substances present in this type of oil added to the complexity of the problem but a satisfactory recovery procedure was, nevertheless, successfully developed.

The following report briefly covers broad general features of the chemical studies to be used by the Atomic Energy Commission in considering future work on the chemical studies of phosphate rock and shale.

Description of a velocity analyzer (with diagrams) is given. It is a device for measuring the velocities of charged particles which comprises pairs of spaced electrodes, a collector for charged particles, and means for propelling charged particles in a direction so as to pass between the pairs of electrodes. The pairs of electrodes and the collector are so arranged to permit passage of the charged particles between them to the collector plate. Means are provided for applying an alternating substantially square wave potential of known frequency to the pairs of electrodes so that adjacent pairs are opposite in phase and so that one half-cycle of the wave appears as zero potential between the pairs of electrodes.

This report records analyses on the fluorescence procedure of uranyl salts.

Abstract: Exceedingly pure uranium tetrachloride was prepared for use in determining the physical constants of the compound. Measurements were obtained of the melting point and boiling point at pressures ranging from the triple point pressure to atmospheric pressure. Calculations were made of the vapor pressure equation for the liquid, the heat of evaporation, molar boiling point elevation, the vapor pressure equation for the solid, and the critical temperature.

"The effect of a single vacuum sublimation of contaminated uranium tetrachloride, with fractional condensation of the vapors, was investigated to determine whether a high degree of purity would result. It was found that this procedure was an excellent and simple method for obtaining exceedingly pure uranium tetrachloride."

Report discussing experiments to determine if the tri-ether (referred to in the report as dibutyl carbitol or carbitol) "was susceptible of a high degree of reactivity when used as an extraction agent for the removal of uranium from aqueous solutions."