A report which deals with the Redox IA Column studies made in small-scale columns packed with 3/16-in. Fenske helices and using NH4NO3 salting agent.

Introduction: Static, total immersion corrosion tests were carried out at room temperatures with Carboloy grades 44-A, 78, 907, X-3119-A and X-3119-B in Redox process solutions (ANL, June 1, 1949 Flowsheet) 1AX, 1AF, and 1AS.

Abstract: "The critical mass both of an untamped and water-tamped sphere with parabolic radial variation of the intrinsic buckling is calculated by a perturbation method. The result is applied to finding the minimum critical mass of plutonium in water suspension with infinite water temper; the calculations show that the minimum critical mass at constant concentration may be reduced by an amount of the order of 7.6% when the concentration of plutonium is permitted to vary throughout the suspension."

Summary: "Criticality was considered impossible in any contingency encountered in practice under either of the following conditions which include no safety factor: (a) In any isolated cylinder not more than 5 in. in disruptor, if the total amount of U235 present does not exceed 7.5 Eg. (b) In an isolated vessel of any shape and size, if the total amount of U235 present does not exceed 880 g. An "isolated" vessel is one which does not "see" more than 0.1 [...] other vessels containing fissionable material."

The following report examines methods to determine uranium nitrate hexahydrate on pretreated hexone in the range of 0 to 40 g./l. by infrared absorption measurements.

Introduction: "A laboratory investigation of the relative corrosion resistance of several austenitic stainless steels to the RAW stream of the Tributyl Phosphate Waste Metal Recovery Process was made during the first quarter of 1950. The results of this investigation are reported herein; all original data are recorded in laboratory notebook HW-3282-T."

Objective: "The observations summarized in the present report were made to determine the stability of ferrous and sulfamate ions and sulfamic acid in RA Column scrub solution (RAS) and in aqueous solution comparable to the RA Column feed tee composition (RAFS). Knowledge of the stability of the reducing agent (ferrous iron) is necessary to properly plan the method of preparation and introduction of this component into the RA system and to assure dependable and reproducible performance."

From introduction: "Analytical procedures for the determination of plutonium samples from the extraction and concentration plants utilize the carrying of the hydroxylamine-reduced trivulent plutonium by coprecipitation on lanthanum fluoride. Most other plutonium procedures also take advantage of the efficient carrying on lanthanum fluoride."

Report describing the temperature in the Brookhaven concrete shield proposed for the X reactor. The report details the methods and equations used to find the values that determined that the effect of the gun barrel assembly in cooling the concrete is negligible.

Report discussing the use of a small-source approximation for engineering calculation of thermal piles. Explanation for how this type of approximation is more appropriate in certain problematic situations where a homogenization approximation would be doubtful is given.

Report discussing a method of rear face monitoring by television as a form of visual contact and communication between Hanford Works crews. A conclusion and recommendation of the method is given as well as an explanation of necessary materials.

This report discusses the development of a method for creating leak-proof closures in aluminum sample casings in order to pass a standard bubble-test inspection.

Introduction: "A corrosion test program, to determine the suitability of LaBour B-55 and Worthite for use in the construction of circulating pumps for th UO3 process has been completed and the data are appended."

Introduction: A limited test progress on Alloghany-Ludlum type 347 stainless steel plate which failed the Huey test (ASTN A-262-44T) has been completed.

Report discussing studies regarding active atmospheric particles in several United States cities. Experimental data of particles collected in filters is given.

Report discussing progress in research and development by the Health Instrument Divisions, Hanford Works, for the term from January through March, 1951.

Report describing a study regarding the solubility and related properties of tributyl phosphate (TBP), which has lower solubility in water than most uranium solvents. Pure TBP and TBP in an inert diluent were tested for solubility in water, several nitric acid solutions of varying concentrations, and other solutions typical of process streams. For TBP-diluent-water system tests, equilibrium water content in organic phase was found.

This report follows an investigation on how hydrolysis products of tributyl phosphate (such as dibutyl and monobutyl phosphoric acids, orthophosphoric acid and butanol) effect the tributyl phosphate process for uranium recovery.

Recent developments in the field of photoconductive devices made possible the simplification and attendant improvement of the recording anemometer system used with the portable meteorological mast. The purpose of the work was to produce a simple, reliable recording anemometer system compatible with the project's existing instrumentation. Of primary importance was reduction of maintenance without loss of accuracy. This report discusses some of the factors considered in the design of the system, describes in detail the electronic circuitry and mechanical components, and presents some performance data. The data obtained from a twenty-four hour trial run indicates that the system has fulfilled the requirements.

This report has been prepared to review the status of design for buried waste line and presents the major factors involved in support of the conclusions. This report is the second in a series reporting on the general subject of underground corrosion. The first on cathodic protection of waste lines noted the technology of stainless steel and its effect on existing waste line and recommended continued use of the cathodic protection. Experience with buried stainless pipe had shown that, unless protected, such installations are subject to severe pit corrosion. As designs developed the use of encasements has become a standardized approach. This discussion will evaluate this trend.

Buckling measurements were taken with hollow natural uranium slugs in graphite-moderated lattices, in which the lattice spacing was varied from 6 3/16 to 15 inches in five steps. A 1.66" O.D. slug was used with two different core sizes, 1.11" I.D. and 0.81" I.D. The results of wet (water in the core) and dry measurements are reported. Buckling curves are given showing the effect on the buckling of coring the slug and placing water in the core. Simple three-region diffusion theory is applied to the measured lattices in an effort to correlate measurement with theory, but with only limited success.

Startup and testing of the PRTR has been divided into three parts, Design Tests, Critical Tests and Power Tests. This document is the third of the series and describes the performance tests which will be made under nuclear power and the general schedule of operation. Responsibility for the startup of the reactor has been assigned to the PRTR Startup Council. The Power Test Sub-Council, which has done the planning of the initial power operation, was established by the Startup Council. Operation of the reactor will be the responsibility of the PRTR Operation (PRTRO).

The spontaneous fission rate of plutonium-240 has been redetermined and found to be 1.51 X 106 events/g/hr.

Field tests were conducted to measure short-period pollutant concentrations at several stack heights during conditions of marked atmospheric instability and low wind speeds. The source was a mechanical smoke generator located at the 185-ft level of a tower.