Abstract: The caustic permanganate-rinse decontamination treatment was investigated. Loop and metallurgical studies were performed to determine optimum operating conditions as well as the metallurgical effects of the treatment. A treatment with 10 percent sodium hydroxide and 5 percent potassium permanganate solution followed by a rinse with a 5 percent ammonium citrate, 2 percent citric acid and 1/2 percent Versene solution was chosen for the decontamination of a stainless steel steam generator. Decontamination factors of greater than 50 were obtained in loop tests using the above treatment. Corrosion and metallurgical results indicated a total penetration of less than 0.01 mil on annealed Type 304 stainless steel with no evidence of any deleterious effects.

PuO2-UO2 Irradiation Capsules. Four capsules of Zircaloy-clad, sintered PuO2-UO2 mixed crystal oxides in a UO2 matrix are awaiting irradiation in the NTR.