This report analyzes a procedure based on the production of acetylene from the active water, with subsequent measurement of the ionization caused by the tritium beta particle. This eliminates the troublesome absorption on the chamber walls when hydrogen is used, and provides a rapid method for the preparation of the urine samples.

A report which intends to acquaint the reader with the planning of the radiochemical laboratory designed for the analytical control of the radiolanthanum process and to define the terminal status of the design of this laboratory and its equipment.

Summary: "The quantity of water adsorbed by graphite at various relative pressures has been determined and the data are presented in graphical and tabular form."

Introduction: "The observations reported in this document were obtained by C.H. Pitt during his assignment to the Corrosion Group September through October 1951. The tubes examined were: 1.) 0893-F Discharged for corrosion examination after leaking; 2.) 1488-DR Discharged to determine caused of obstruction; 3.) 2276-D Discharged for corrosion examination; 4.) 2376-D Discharged for corrosion examination; 5.) 1185-H Discharged to evaluate the effect of magnesium front dummies."

"The following is an alphabetical listing of terms and units in common usage at HAPO. Other terms and definitions may be added as the need becomes apparent or as revisions or additional terms are issued by the NCRP and ICRP."

From introduction: "The purpose of this report is to summarize some of the observations on the dispersion and rate of disengaging of liquid-liquid systems and suggest some possible lines of future work."

Abstract: "A method has been devised and successfully used for marking a leaking pile process tube prior to its removal from the pile, such that subsequent location of the leak is more easily accomplished. An acetone solution of Testor's Dark Red Airplane Dope is poured into the suspect tube. The solution leaks from the hole and stains the surrounding area a light pink. To date the method has been used on tubes 3573F, 0486F, 0867F, and 3670F."

The following report observes infrared measurements in the region of OH bands, the C2O band vicinity, the low frequency end of the spectrum, and the region of the UO2 band on the system hexone - water - uranyl nitrate.

This report follows work with the purposes of determining the minimum amount of nitric acid required to dissolve slurries of stored metal waste, determining the stability of such metastable solutions as a function of their chemical compositions - primarily acidity - versus time and temperature, and to define a feed suitable for a low-acid TBP process flowsheet, and to indicate the range of variations in composition which can be tolerated for plant operation.

The following report records a total of forty-nine graphite core samples that have been bored from process tube blocks in the Hanford piles with the intention to provide results to indicate that core boring is an entirely practical operation over bore scraping in obtaining powder samples.

The following report discusses a method developed by Broida and Moyer, the method describes an emission spectrometer procedure for the determination of the ratio 100 D/(H4D).

From introduction: "The prime motive behind the experiments described in this report and in those preceding it in this series is the desire to reduce the number of Redox cycles necessary for decontamination from fission products of the plutonium and uranium streams sufficient to allow final disposition of these two products...This report deals with the mechanics of manganese dioxide handing, laboratory development of manganese dioxide scavenging, and a series of experiments at multicurie level combining ruthenium volatilization and manganese dioxide scavenging in stainless steel equipment."

Abstract: The data obtained from the radioassay of fish collected in vicinity of the Hanford Works between April, 1948 and June, 1950 are presented. Most of the radioactivity in the fish resulted from the concentration of p32 in the scales, bone, and certain visceral organs. The level of activity density in the fish was influenced by size, feeding habits and metabolic rate in addition to the activity density of the water. Changes in operation of nuclear reactors have resulted in progressive increases in activity densities of fish from one year to the next. The levels of radioactivity are not sufficiently high to be hazardous to either the fish or persons eating them.

This paper describes the measurement of control rod strength in the PCTR. The first section outlines the theory and method of such a measurement, and the second section presents the results of the measurement of the Experimental Gas Cooled Reactor (EGCR) control rod strength. The reactor parameter actually inferred is the difference in the infinitive multiplication factor for a control rod supercell with and without the control rod in place in the supercell. These measurements are, therefore, very closely related to the measurement of k∞ for an ordinary lattice cell.

This document authorizes the performance in accordance with the specifications noted, the PRTR Critical Tests described herein. The experiments described have the following objectives:

This development work was undertaken to investigate and standardize scintillation detector and transistorized circuitry techniques in instruments used for detecting and measuring alpha and beta particles, gamma photons, and both slow and fast neutrons. At the present time, the standard radiation detection instrumentation used at Hanford employ vacuum-tube circuitry with typical detectors being ion chambers, G-M tubes, HF3 tubes, etc. The vacuum tubes require excessive battery power, and some of the circuits are adversely affected by humidity and temperature conditions.

This report summarizes the research and development work carried out during March, April and May, 1959, for Budget Activity 2790 - Separations Development for Non-Production Reactors, The effort on Activity 2790 will enable Hanford to begin reprocessing in January, 1962, the fuel elements from power reactors which employ depleted or slightly enriched uranium fuels.

The Single Tube Prototype Mockup (STPM) was constructed to be used as a tool to evaluate the mechanical problems involved in operating and maintaining many components of the Plutonium Recycle Test Reactor (PRTR). This report has been written to acquaint interested HAPO components with the capability of the STPM and for use as an aid in scheduling tests and/or to properly evaluate testing results obtained from the mockup.

Two water quality control labs are being provided for the the NPR. One, a "cold" lab, is located in the183 Building adjacent to the control room. Its primary purpose is to provide facilities for quality control of the output of the filter plant and the demineralizer plant. The other, a "hot" lab, is located in the 190 Building. Its primary purpose is to provide facilities for the quality control of the primary and secondary coolants, and the moderator coolant.

A study of metallurgical problems resulting from variation in grain boundaries, bonding layers, and inclusions in metals and alloys has become increasingly important over the past several years. To keep pace with and aid in these studies, several new techniques have been developed in emission and X-ray spectroscopy. In X-ray, areas as smalls as one square micron can be studied by making them targets for a focused electron beam and observing the X-rays emitted (5,2). Such an instrument would be quite helpful at Hanford, but the high original cost is prohibitive.

The recovery of plutonium and neptunium by anion exchange has been well demonstrated on a laboratory scale. (1, 2,3,4) The specific adsorbed by the resin is the tetravalent hexanitrate complex of either element. With plutonium (IV) and neptunium(V) in IWW, the plutonium is adsorbed but the neptunium is not. If nitrite is used as the reductant in strong (preferably 8 M or over) nitric acid, both plutonium and neptunium are obtained in the tetravalent state, and both are adsorbed on the resin. With stronger reductants, such as semi carbazide or ferrous sulfamate, plutonium (III) and neptunium (IV) are obtained so that only the neptunium is adsorbed. Optimum recovery of either element is obtained with between seven and eight M nitric acid.

This report is a summary of work done for system development on the NPR ball safety backup for the horizontal rods. This phase of the system development is limited to discussion of the horizontal rod counting circuitry utilizing a direct current bridge network.

The Stack Effluent Radioisotope Monitor is an instrument which continuously measures and records the amounts of each of several different radioactive isotopes in the stack effluent of the Redox Facility. An informal report, HW-56151, describing the theory of operation and the circuits was prepared and is available to Hanford personnel from the technical files. The formal report, HW-56151 Rev, containing essentially the same information, is available from the Office of Technical Services, Department of Commerce, Washington 25, D. C.

The hazards associated with several possible mechanical failures were analyzed for the PRTR. The consequences of these failures were evaluated for inclusion in the Final Hazards Summary Report.