A stainless steel autoclave for superheated water corrosion test was installed and "conditioned". Tests were begun to investigate the feasibility of densifying slip cast stainless steel by means of liquid phase sintering. Attempts to prepare tubular fuel elements by vacuum forming were resumed. Although thick-walled vacuum formed casting have been sintered on the aluminum mandrels without cracking, this has not yet been accomplished with the think sections of interest.

During the past year, three papers covering results of a major series of experiments on intergenotype of blood-forming tissue have appeared, demonstrating successful implantation of isologues normal cells in anemic hosts, permanently correcting their genetic defect in hematopoiesis, both with and without irradiation of the host. Heavy host irradiation was shown ineffective as preparations for implantation of homologous cells of widely different antigenic types.

Thorium Procedure: As was mentioned in the last report, ammonium nitrate was substituted for ferric nitrate as a salting agent. Also, the acidity of the nitrate solution was reduced from 3.0 molar to 0.5 molar. the revised thorium procedure is described in the report. Radium Procedure: Work has ben initiated on the procedure of Petrow, Nietzel and DeSesa (Winchester Procedure) to determine if the procedure is suitable for very low level concentrations of radium.

Data obtained in test of Bureau of Mines electrocerium are presented. The cerium was subjected to spectrochemical analysis, x-ray diffraction analysis, thermal analysis, metallographic tests, and high-pressure experiments.

A device to extend the operation of a beam extraction system is described for low energies where the radiation loss per turn is ineffective. The device consists of a noisy radiofrequency field which excites the radial betatron oscillation

A preliminary mathematical study is made of the maximum expected expansion of barium titanate ceramic. It is noted that there is insufficient physical evidence for a complete answer and some possible mathematical models are discussed and compared.

This is the seventeenth quarterly report on our echelle project, as numbered above. Our work this quarter has to some extent been directed towards the Spectroscopy Symposium held at Argonne National Laboratory on February 15, 16, and 17. This report consists principally of brief abstracts of the two papers given at this meeting. Progress since the last quarterly report included completion of the echelle comparator calibration, and the successful production and photographing of the desired spectra of praseodymium and erbium in strong magnetic fields. Considerable interest was aroused by these papers, not only because rare earth spectra are being analyzed, but because of the general applicability of our experimental techniques in producing the spectra.

"An investigation was made into the various processes for the fixation of mixed fission products as solids in order to determine the extent they could be utilized as heat sources for thermoelectric generators. Generators of up to ten watts can be designed and built with state-of-art'' thermoelectric materials and mixed fission products soon to be available from the ldaho Falls calcination pilot plant. Mixed fission products from other processes and plants to be on stream'' in this decade will be capable of fueling practical generators into the kilowatt range using thermoelectric materials available in the same time period. A survey was made on current research and development efforts on waste fixation processes. Studies showed that a wide range of power densities (from 0.002 to 0.2 watts per cubic centimeter) will be available from calcined fission product wasted. An experimental program for the consolidation of low density, Idaho Chemical Processing Plant alumina type wastes is reviewed. Preliminary results indicated that densification factors of three to four are readily obtainable for such wastes."

"Mesic decay of hyperfragments is discussed systematically on the basis of a previous model for hyperfragments. The general formalism for the two-body and three-body mesic decay was developed. The polarization-direction correlation and the angular correlation for the two-body and the three-body decays are discussed together with the decay probability. The formalism was developed so as to include the isotopic spin selection rule ( DELTA I = 1/2 and 3/2) for the mesic decays. The theory was applied especially for the low mass number hypergragments where it was found that the branching ratios of the two-body and the three-body mesic decays of /sup 3/H/sub i and /sup 4/H/sub i, (/sup 3/ H/sub i yields /sup 3/He + i/sup -/)/(/sup 3/H/sub i yields D + p+ pi /sup -/) and (/sup 4/H/sub i yields /sup 4/He + pi /sup -/)/(/sup 4/H/ sub i yields /sup 3/H + p + pi /sup -/), could be used for the determination of the spins of both hyperfragments. The fraction of the p-wave decay rate for the free LAMBDA decay obtained from the reaction /sup 5/He/sub i yields /sup 4/He + p + pi where the decay proceeds through two-resonant states (p/sub 3/2/ and p/sub 1/2/) …

"Research in thermal contact resistance at MIT and advances made during the past year are summarized. The problem of predicting cortact resistance is examined in an analysis of a model for the contact which relates the geometry of actual surfaces in contact to the contact model, and a deformation analysis which relates the contact geometry to the load carried by the surfaces. Experimental procedures are described and are applied to two stainless steel surfaces in contact and to W and graphite surfaces in contact. A significant result is that a surface may be described by two measurable parameters which may be combined with two such parameters of any other surface to completely determine the geometry of the interface if they are placed in contact. It thus remains to construct a device which will readily measure these two parameters."

" A reliable, efficient and economical method is needed to remove radioactive halogens such as iodine and bromine and particulates from air in many atomic energy installations. One method we have developed which is particularly suited to reactor containment vessels or other large confined areas is foam containment. In this method an ether lauryl sulfate foam containing an iodine reactant is generated, rapidly filling the entire containment volume. This provides a tremendous surface area to which the encapsulated gases and particles can diffuse and be removed."

"Muon capture rates have been measured in a large number of the heavier elements in recent years. The amount of data available on the light elements, however, is scant. It would seem that lifetime measurements of muons in light elements would be of particular interest with regard to understanding the nuclear structure and determining the strength of the weak interaction. Furthermore, only one previous measurement of the muon capture "'isotope effect" has been done, that being for chlorine isotopes. In view of these considerations, the series of muon capture experiments reported in this paper was undertaken."

"This is the third quarterly report on Task II dealing with Methods Development for Radio-Tracing of Coal Product Hydrocarbons With Tritium. The problem of accurate low-level tritium assay for tagged hydrocarbons has been resolved and attention is now primarily directed at the questions of tritium mobility and radio-chemical purity in tagged tracers."

Abstract. In the first section of this technical report a new method of extracting uranium from thorium nitrate solution is discussed. This method consists of extracting an aqueous solution of thorium nitrate, nitric acid, sodium sulphate, and potassium thiocyanate with hexone. By this procedure, using an equal volume of hexone it is possible to extract 83 percent of the uranium while only 0.3 percent of the thorium is extracted. other experiments show that even greater separations are possible. In the second section of this report the use of antipyrine in solvent extraction procedures is discussed. Experiments are described in which 90 percent of the uranium is extracted while the thorium is extracted to the order of 3 to 5 percent.

Technical report containing short articles on (1) Determination of physical constants for U233; (2) Determination of decay chain of U233; (3) Extraction of U233; (4) Extracting solvents for uranium; (5) Factors affecting the extraction uranium and thorium by organic solvents, especially ether; and (6) Analysis of ore samples for protoactinium.

Technical report with short reports covering (1) Effect of radiation on water and aqueous systems; (2) Effect of neutrons on graphite; (3) Effect of radiation on solid compounds; and (4) Scattering, stopping-power, ion-pair production, etc.

Technical Report: A generalized review of the chemical problems and researches related principally to the heavy water homogeneous pile is presented herewith. The report covers researches performed principally by the Columbia Group who initiated the study. This report contains a chronological outline of the development, a discussion of some special topics whose significance is paramount in any slurry pile discussion, and finally an outline of important research problems remaining, roughly graded in order of their importance. No attempt has been made to be either complete or detailed in the discussion. The emphasis has been principally on furnishing a broad guide to those who may t some future date take up this work.

Technical report describing a gasometrical method for the determination of H2 in extruded U rods.

Technical report summarizing our knowledge of the chemical effects of ionizing radiation upon water and upon aqueous solutions of inorganic compounds. The types of radiation considered are beta rays, gamma and X rays, and heavy particles, notably neutrons, deuterons, alpha rays and fission recoils.

Abstract. A review of all work on uranium hydride published in the CC, CT, CN and CE reports to January 1, 1944, is presented. Some additional information not yet published has been included, so this report includes all data known from the above sources and at Ames to the above date. This report supersedes all previous report on uranium hydride coming out of the Ames laboratory.

The Technical Data Book compiles useful chemical and physical data of feed materials, chemicals, uranium intermediates and end products of the FMPC, Fernald, Ohio. The data presented encompass the process operations involved in the original integrated FMPC project, the uranium hexafluoride reduction plant and the throium plant.

"The principal uranium deposits in southcentral Wyoming and north-western Colorado are located in or at the margins of broad Tertiary basins. Interesting and possibly commercially significant occurrences are found in other Tertiary and older rocks at widely separated locations within this region. The six maps accompanying this report give the location, name, and ownership of the mines and occurrences from which samples assaying greater than 0.10% U3O8 have been collected. Claim names, location, and ownership are also given for occurrences outside the map areas."

Maps and charts illustrating aspects of a photogeologic reconnaissance study of the spatial relationship of uranium deposits to structure and stratigraphy in Duval County, Texas.

A report discussing a diamond drilling project in the Silver Reef District and adjacent areas, with the propose to obtain geologic information as well as to further explore the Chinle formation for new ore bodies.