Two high-pressure flow microreactors continue to function effectively for studies of the hydrodesulfurization of dibenzothiophene, methyl-substituted dibenzothiophene and also for studies of the hydrodenitrogenation of quinoline. The hydrodesulfurization of dibenzothiophene has been examined in a flow system in a totally reproducible fashion free from catalyst deactivation for extended periods. The reaction is first-order in dibenzothiophene, and all of the reaction products except H/sub 2/S are sulfur free. A program for determining the kinetics and reaction network of methyl-substituted dibenzothiophenes was started. For example, the rate for hydrodesulfurization of 4,6-dimethyldibenzothiophene is about one-fifth the rate for dibenzothiophene. The hydrocarbon reaction products except H/sub 2/S are sulfur free; therefore, the initial point of attack is concluded to be the C-S bond. The hydrodenitrogenation of quinoline was examined further by replacing white oil with hexadecane; this substitution permits the determination of the nitrogen-free reaction products by gas chromatography. These studies show that the C-N bond is broken after at least the heterocyclic ring and preferably both rings are hydrogenated. The hydrogenolysis reactions are rate limiting for the overall process of nitrogen removal. The hydrodenitrogenation of acridine is slower than that of quinoline. The reaction network shows that the molecule must be hydrogenated before …

Large quantities of bulk powder can be separated according to particle size and density by air classifiers. Classifiers disperse the powder and usually achieve size differentiation by drag and centrifugal forces acting on individual particles in the gas stream. A Donaldson ''acucut'' Classifier for the separation of B/sub 4/C powder is evaluated. Experimental tests were conducted to determine the particle cut sizes and powder yields obtained by variation of operating parameters. To assess the classifier's performance further results of the sharpness of the powder cuts were evaluated and compared with the vendor's prediction. 7 figures, 3 tables.

The report describes and highlights the more important factors associated with the termination of the Special Metallurgical (SM) Building at Mound Laboratory. As a result, a written record of the more important techniques and procedures is now available for reference by others involved in similar termination efforts. Included in this report is a description of the organizational units that were used in this effort along with a description of their responsibilities. A general description of the SM Building and a discussion of the more relevant procedures and equipment that were used are also presented. In addition, pertinent Health Physics information, such as personnel exposure, final wipe levels in the terminated facility, and assays of the structure, are provided. Based on the experience gained from this project, recommendations were made regarding the design of future radioactive material handling facilities so that when they are ultimately terminated the effort can be accomplished more efficiently.

This report discusses the current status of liquid-metal fast breeder reactor (LMFBR) development and one of the principal safety issues, a hypothetical core-disruptive accident (HCDA). Bibliographic information on worldwide LMFBRs relative to the development of the breeder reactor as a safe source of nuclear power is presented for the period 1970 through 1972. The bibliography consists of approximately 1620 abstracts covering early research and development and operating experiences leading up to the present design practices that are necessary for the licensing of breeder reactors. Key-word, author, and permuted-title indexes are included for completeness.

The extent to which earth subsidence may be caused by in situ coal gasification is studied using the method of finite elements. This study takes into account rock failure modes and nonlinearity of rock stiffness. Two models were studied for the site at Hoe Creek, where a coal seam is overlain and underlain by interbedded clays and sandstones. These two studies are expected to bracket any subsidence that may occur. Maximum subsidence was 0.06 in. using the stiff model and 3.5 in. using the soft model, neither of which suggests undesirably large subsidence.

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/sup 238/PuO/sub 2/ contamination of the grit blasted surface of the primary impact shell assembly (PISA) of the multi-hundred watt isotopic heat source was measured. The study determined the amount and distribution of the /sup 238/PuO/sub 2/ and characterization of its behavior during aging at 1350/sup 0/C. The results concluded that normal decontamination effectively removes the superficial /sup 238/PuO/sub 2/ but does not extract the /sup 238/PuO/sub 2/ which is deep within the grit blasted structure. Subsequent heating results in migration of microcurie amounts of plutonium out of the grit blasted structure.

Document issued by the Office of the Attorney General of Texas in Austin, Texas, providing an interpretation of Texas law. It provides the opinion of the Texas Attorney General, John L. Hill, regarding a legal question submitted for clarification: Whether a county may contract with an individual to prepare an economic redevelopment plan to make the county and private agencies in the county eligible for federal grants.

A description is given of the design and application of a simple e-beam generator for the repetitive pulse pumping of gas lasers. The circuit uses a low inductance Marx and series tuned pulse forming elements.

Recent experiments at the LLL 2.0 terawatt laser irradiation facility Argus have been conducted on glass microshells filled with equimolar DT gas. A variety of microshell dimensions and laser pulse widths have been used with the best results producing in excess of 10/sup 8/ fusion reactions. Numerical simulation of selected experiments using the LASNEX computer code confirm the measured performance. Peak DT ion temperatures of about 5 keV and densities of .2 gm/cm/sup 3/ are calculated and are in agreement with that from neutron time-of-flight and alpha particle spectral measurements together with x-ray diagnostics. Laser light absorption is about 20% efficient. General characteristics of ''exploding pusher'' targets will be discussed.

This review contains more than 100 observations and 224 references on the dissolution phenomenon. The dissolution processes are grouped into three categories: methods of aqueous attack, fusion methods, and miscellaneous observations on phenomena related to dissolution problems. (DLC)

Considerable need has arisen for the development of well-calibrated x-ray detectors capable of detecting photons with energies between 100 and 1000 electron-volts. This energy region is of significant interest since the x-ray emission from high-temperature (kT approximately 1.0 keV), laser-produced plasmas is predominantly in this range. A high-intensity, subkilovolt x-ray calibration source was developed which utilizes proton-induced inner-shell atomic fluorescence of low-Z elements. The high photon yields and low bremsstrahlung background associated with this phenomenon are ideally suited to provide an intense, nearly monoenergetic x-ray calibration source for detector development applications. The proton accelerator is a 3 mA, 300 kV Cockroft-Walton using a conventional rf hydrogen ion source. Seven remotely-selectable liquid-cooled targets capable of heat dissipation of 5 kW/cm/sup 2/ are used to provide characteristic x-rays with energies between 100 and 1000 eV. Source strengths are of the order of 10/sup 13/ to 10/sup 14/ photons/sec. A description of the facility is presented. Typical x-ray spectra (B-K, C-K, Ti-L, Fe-L and Cu-L) and flux values will be shown. Problems such as spectral contamination due to carbon buildup on the target and to backscattered particles are discussed.

In order to view the thermonuclear burn generated by laser driven implosions of D-T filled microspheres ten to twenty micron diameter gold and tantalum pinholes have been built to image 3.52 MeV alpha particles. KODAK Pathe LR115 Cellulose Nitrate is used as a detector behind an 8.3 x 10/sup -3/ gm/cm/sup 2/ tantalum filter. The 3.52 MeV alpha particles reach the emulsion with approximately 0.9 MeV energy and are absorbed in the first three microns. High energy x-rays and electrons are also imaged, but their greater penetration allows discrimination.

As laser capabilities increase, implosions will be performed to achieve high densities. Criteria are discussed for formation of a low-density corona, preheated supersonically, which increases the tolerance of high convergence implosions to non-uniform illumination by utilizing thermal smoothing. We compare optimized double shell target designs without and with atmosphere production. Two significant penalties are incurred with atmosphere production using 1 ..mu..m laser light. First, a large initial shock at the ablation surface limits the pulse shaping flexibility, and degrades implosion performance. Second, the mass and heat capacity of the atmosphere reduce the energy delivered to the ablation surface and the driving pressures obtained for a given input energy. Improvement is possible using 2 ..mu..m light for the initial phase of the implosion. We present results of 2-D simulations which evaluate combined symmetry and stability requirements. At l = 8, the improvement produced in the example is a factor of 10, giving tolerance of 10 percent.

Reduction of input power requirements for laser and charged particle fusion targets has been predicted by implosion calculations that simulate ignition of only a small fraction of the DT fuel instead of the total mass. Once ignition is reached in this localized region, the burn can propagate through the rest of the fuel mass. An approach that achieves this ignition by use of preheat and self-generated magnetic fields is described here, with the result of lower input requirements, i.e., 30 TW and 100 kJ, to achieve breakeven.

Document issued by the Office of the Attorney General of Texas in Austin, Texas, providing an interpretation of Texas law. It provides the opinion of the Texas Attorney General, John L. Hill, regarding a legal question submitted for clarification; Expenditure of municipal funds for expenses of defending suits brought against mayor, city policeman, and members of the city council.

A weekly publication, the Texas Register serves as the journal of state agency rulemaking for Texas. Information published in the Texas Register includes proposed, adopted, withdrawn and emergency rule actions, notices of state agency review of agency rules, governor's appointments, attorney general opinions, and miscellaneous documents such as requests for proposals. After adoption, these rulemaking actions are codified into the Texas Administrative Code.

This report is on the Basic Aspects of International Monetary Reform.

Performance of laser fusion targets depends critically on the characteristics of the incident beam. The spatial distribution and temporal behavior of the light incident on the target varies significantly with power, with choice of beam spatial profile and with location of spatial filters. On each ARGUS shot we photograph planes in the incident beams which are equivalent to the target plane. Array cameras record the time integrated energy distributions and streak cameras record the temporal behavior. Computer reduction of the photographic data provides detailed spatial energy distributions, and instantaneous power on target vs. time. Target performance correlates with the observed beam characteristics.

This report concerns efficacy in stimulating home construction and the outcome of this, as well as if the Brooke-Cranston Program has mostly assisted wealthy households in purchasing new homes, as opposed to low and middle income families.

The uranium-niobium alloy system was examined in the range of 5.3-to-6.9 weight percent niobium with respect to shape memory, mechanical properties, metallography, Coefficients of linear thermal expansion, and differential thermal analysis. Shape memory increased with increasing niobium levels in the study range. There were no useful correlations found between shape memory and the other tests. Coefficients of linear thermal expansion tests of as-quenched 5.8 and 6.2 weight percent niobium specimens, but not 5.3 and 6.9 weight percent niobium specimens, had a contraction component on heating, but the phenomenon was not a contributor to shape memory.

Document issued by the Office of the Attorney General of Texas in Austin, Texas, providing an interpretation of Texas law. It provides the opinion of the Texas Attorney General, John L. Hill, regarding a legal question submitted for clarification; Application of Texas Surface Mining and Reclamation Act to Clay Mining Which Incidentally produce lignite.

Error field multipoles due to systematic errors in the current distribution are computed and compared with the error field multipoles due to random errors in the current distribution. The systematic field error multipoles are found to vary rapidly across the aperture, and in some cases may be the dominant error multipoles.

This fact sheet for distribution at the flash and flow test of HGP-A, July 22, 1976 contains a temperature-depth plot, a brief chronology, and a budget summary. (MHR)