Report issued by the Brookhaven National Laboratory discussing progress of waste concentration studies. As stated in the introduction, "the present report covers all experimental hot runs up to the time the still was turned over to the Waste Control Section for intermediate handling of laboratory D waste" (p. 1). This report includes tables, illustrations, and photographs.

From purpose of report: The primary purpose of this report and its appendices is to transmit to the AEC the principal results of the experimental and engineering work done on the low-temperature process and to describe the factors which led to the designs finally adopted.

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Technical report describing the results of the chemical reaction between potassium amide and liquid ammonia and the exchange of hydrogen between hydrogen gas and liquid ammonia. This report finds that the reactions may be sufficiently rapid to be useful for isotope separations on a larger scale.

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Report evaluating different methods of preparing nitric acid solution and different methods of separating plutonium from this nitric acid solution of slag and crucible. Methods are explained and experimental data is given.

Document issued by the Office of the Attorney General of Texas in Austin, Texas, providing an interpretation of Texas law. It provides the opinion of the Texas Attorney General, Price Daniel, regarding a legal question submitted for clarification: Legality under nepotism statutes of continuing county employment of a brother of a newly elected County Commissioner under submitted facts.

Document issued by the Office of the Attorney General of Texas in Austin, Texas, providing an interpretation of Texas law. It provides the opinion of the Texas Attorney General, Price Daniel, regarding a legal question submitted for clarification: Authority of the Highway Commission to authorize motor buses to have priority over other traffice in boarding the Galveston-Bolivar ferry.

The purpose of the research work reported in this volume is the development of a process for the separation and subsequent purification of radium from the K-65 (pitchblende) residue. Except for the accumulation of additional experimental data the process is essentially complete. After a preliminary extraction of about 85% of the lead and 40% of the silica with a 40% sodium hydroxide solution, the residue is treated with a solution containing both sodium hydroxide and sodium carbonate to obtain additional lead removal and partial conversion of the radium and barium sulfates to carbonates. After leaching out the soluble carbonates, the residue containing unconverted sulfates is treated with a sodium carbonate solution at 170{sup o} under pressure. A study of the amount and concentration of sodium carbonate required to obtain a satisfactory conversion of the sulfates has shown that the total sodium carbonate may be reduced by 40% and that smaller volumes of solution may be employed without serious decrease in the efficiency of the conversion. In order to make calculations on the number of steps and tank sizes for the radium-barium separation by fractional precipitation, equations have been developed to calculate this information from the theoretical separation factors determined experimentally. …

On 2/8/1950, there was mined from process tube 2273 in D pile at Hanford a quantity of graphite power, which was expected to show the most extensive radiation damage of any graphite available at that time. A series of samples of this powder were annealed in 100 degrees increments from 100 degrees to 2000 degrees C at this labaoratory. There were returned to Hanford and shipped by them to the National Bureau of Standards for total stored energy measurements. The present memorandum is comprised of a description of the annealing procedure used here, curves giving the detailed annealing history of each sample, and various curves derived from data obtained from these samples at Hanford and at the National Bureau of Standards.

The purpose of the research work presented in this volume is to develop a process for the separation and purification of actinium-227 produced by neutron bombardment of radium-226 and to develop methods by which uniform films of actinium metal may be deposited on metallic surfaces. The design work on the cave structure and mechanical equipment used in the actinium separation is proceeding on schedule. As the mechanical design phase is nearing completion the emphasis is being directed toward processing equipment. The process as well as the mechanical equipment has been adapted from the research work of F. T. Hagemann and the Remote Control Group at Argonne National Laboratory. Consequently, one of the first objectives is to become familiary with the chemistry of the process and the operation of the mechanical equipment. Cold runs have been made on the T.T.A. benzene extraction using lanthanum and barium in place of actinium and radium. No difficulty with the operation was observed. The formation of precipitates was one of the difficulties encountered with the process as the precipitates carry radium. It has been found that metals such as nickel cause these precipitates to form and should, therefore, be avoided in the construction of equipment. …

Slag and crucible can be dissolved satisfactorily by the Los Alamos method of total dissolution with nitric acid in the presence of aluminum nitrate. Extraction of 99% of the plutonium from total dissolution salted with aluminum nitrate was achieved by three successive contactings with 1/10 volumes of 30% TBp- AMSCO 125-90W. The TBPAMSCO phases contacted with leaching solutions salted with calcium nitrate must be scrubbed to remove calcium. Stripping with three 1/10 volumes of 0.1M hydroxylamine sulfate removes 99% of the plutonium from the 30% TBPAMSCO, initially O.lM HNO/sub 3/. Plutonium(III) oxalate, (which could be blended into 234-5 operations) can be precipitated from the aqueous strip solution. It is chemically feasible to recycle slag and crucible solution to the Redox IIA column in amounts up to at least lO% of IIAF by volume. It is also chemically feasible to recycle nitric acid solution of slag crucible obtained in the presence of aluminum nitrate to the Product Precipitation step of the Second Decontamination Cycle of the Bismuth Phosphate Process. (auth)

Report documenting the suitability of North Carolina for plant locations to produce synthetic liquid fuels, based on raw materials, water sources, and local interest.

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From introduction: This report serves as a recommendation that a full-scale incineration process be installed at Mound Laboratory and provides a complete flow sheet for this process and recommended designs for the critical parts of the processing equipment. It contains justification for the process, a history of the investigation including early work and pilot plant results, an explanation of the values and information given in the flow sheet, and the reasons for the recommended design features.

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The effectiveness of molybdenum disulfide MoS2 as a bearing lubricant was determined at high temperature and at high speeds. A 1-inch-bore ball bearing operated at temperatures to 1000 F, a speed of 1725 rpm, and a thrust load of 20 pounds when lubricated only with MoS2-air mist. A 75-millimeter-bore cageless roller bearing, provided with a MoS2-syrup coating before operation, operated at DN values to 1 x 10(exp 6) with a load of 368 pounds.

Report presenting the results of a free-flight investigation of two drag research models equipped with canopies for a range of Mach numbers from 0.8 to 1.5. The main difference between the models was the location of the canopy, which was at the 15-percent fuselage station on one model and the 25-percent fuselage station on the other. The additional drag due to the canopies was about 10 to 20 percent of the total configuration drag at supersonic speeds.