Recovery of Plutonium From Slag and Crucible (open access)

Recovery of Plutonium From Slag and Crucible

Report evaluating different methods of preparing nitric acid solution and different methods of separating plutonium from this nitric acid solution of slag and crucible. Methods are explained and experimental data is given.
Date: June 15, 1951
Creator: Groot, C.; Hopkins, H. H. & Schulz, W. W.
System: The UNT Digital Library
Recovery of Plutonium from Slag and Crucible (open access)

Recovery of Plutonium from Slag and Crucible

Slag and crucible can be dissolved satisfactorily by the Los Alamos method of total dissolution with nitric acid in the presence of aluminum nitrate. Extraction of 99% of the plutonium from total dissolution salted with aluminum nitrate was achieved by three successive contactings with 1/10 volumes of 30% TBp- AMSCO 125-90W. The TBPAMSCO phases contacted with leaching solutions salted with calcium nitrate must be scrubbed to remove calcium. Stripping with three 1/10 volumes of 0.1M hydroxylamine sulfate removes 99% of the plutonium from the 30% TBPAMSCO, initially O.lM HNO/sub 3/. Plutonium(III) oxalate, (which could be blended into 234-5 operations) can be precipitated from the aqueous strip solution. It is chemically feasible to recycle slag and crucible solution to the Redox IIA column in amounts up to at least lO% of IIAF by volume. It is also chemically feasible to recycle nitric acid solution of slag crucible obtained in the presence of aluminum nitrate to the Product Precipitation step of the Second Decontamination Cycle of the Bismuth Phosphate Process. (auth)
Date: June 15, 1951
Creator: Groot, C.; Hopkins Jr., H. H. & Schulz, W. W.
System: The UNT Digital Library
An experimental study at moderate and high subsonic speeds of the flow over wings with 30 degrees and 45 degrees of sweepforward in conjunction with a fuselage (open access)

An experimental study at moderate and high subsonic speeds of the flow over wings with 30 degrees and 45 degrees of sweepforward in conjunction with a fuselage

Report presenting pressure distributions and wake measurements for wings with 30 and 45 degrees of sweepforward, in conjunction with a midwing fuselage, at Mach numbers up to 0.96. The wings had an NACA 65-210 section, a taper ratio of 0.38, and aspect ratios of 7.5 and 5.2. Results regarding pressure distributions, wake measurements, and corrections are provided.
Date: June 15, 1951
Creator: Whitcomb, Richard T.
System: The UNT Digital Library
An experimental study at moderate and high subsonic speeds of the flow over wings with 30 degrees and 45 degrees of sweepback in conjunction with a fuselage (open access)

An experimental study at moderate and high subsonic speeds of the flow over wings with 30 degrees and 45 degrees of sweepback in conjunction with a fuselage

Report presenting pressure distributions, wake measurements, and tuft patterns for wings with 30 and 45 degrees of sweepback in conjunction with a midwing fuselage at Mach numbers to 0.96. The wings have an NACA 65-210 section, a taper ratio of 2.6:1, and aspect ratios of 7.5 and 5.2. The study indicated that when the Mach number reached high subsonic values at low angles of attack, the locations of peak negative pressure coefficients on the upper surfaces of the sections near the wing-fuselage junctures shifted rearward.
Date: June 15, 1951
Creator: Whitcomb, Richard T.
System: The UNT Digital Library
Removal of ruptured slug from tube No. 2278-H (open access)

Removal of ruptured slug from tube No. 2278-H

None
Date: June 15, 1951
Creator: Lewis, C. G.
System: The UNT Digital Library
Retention of Iodine in Process Solutions by Mercuric Salts (open access)

Retention of Iodine in Process Solutions by Mercuric Salts

Report discussing a study of various types of mercuric salts in order to determine which salt prevents the evolution of iodine which results from sparging.
Date: June 15, 1951
Creator: Holm, C. H.
System: The UNT Digital Library
Investigation of the Potential Hazard in Releasing Scrap Steel Contaminated with Uranium to Commercial Channels (open access)

Investigation of the Potential Hazard in Releasing Scrap Steel Contaminated with Uranium to Commercial Channels

Tests were conducted on a laboratory and semi-plant scale to determine the effect of permitting scrap grossly contaminated with uranium to be used in steel manufacture. It was found the most of the uranium is removed with the slag. Steel made with this scrap would have a uranium constituent so little above that made with uncontaminated scrap as to be hardly significant. The slag itself would not present any hazard in handling or normal use. It is recommended, therefore, that in the future steel with only surface uranium contamination be released through normal scrap channels.
Date: June 15, 1951
Creator: Blatz, Hanson; Harley, John H. & Eisenbud, Merril
System: The UNT Digital Library
The Synthetic Liquid Fuel Potential of Oklahoma (open access)

The Synthetic Liquid Fuel Potential of Oklahoma

Report documenting the suitability of Oklahoma for plant locations to produce synthetic liquid fuels, based on raw materials, water sources, and local interest.
Date: June 15, 1951
Creator: Ford, Bacon, and Davis
System: The UNT Digital Library