The main goals of this research were to fabricate magnetic cobalt nanoparticles and study their structural, crystal structure, optical, and magnetic properties. Cobalt nanoparticles with average particle size 8.7 nm were fabricated by the method of high temperature reduction of cobalt salt utilizing trioctylphosphine as a surfactant, oleic acid as a stabilizer, and lithium triethylborohydride as a reducing reagent. Energy-dispersive X-ray spectroscopy (EDX) analysis confirmed the formation of cobalt nanoparticles. High resolution transmission electron microscopy images show that Co NPs form both HCP and FCC crystal structure. The blocking temperature of 7.6 nm Co NPs is 189 K. Above the blocking temperature, Co NPs are single domain and hence showed superparamagnetic behavior. Below the blocking temperature, Co NPs are ferromagnetic. Cobalt nanoparticles with a single-domain crystal structure support a sharp plasmon resonance at 280 nm. Iron nanoparticles with average particle size 4.8 nm were fabricated using chemical reduction method show plasmon resonance at 266 nm. Iron nanoparticles are ferromagnetic at 6 K and superparamagnetic at 300 K.

In this project, the main research objective is intend to seek criteria for evaluating the capacity of BAC screw fasteners with mixed configuration of waterproof seal washer, sealer tape and different pre-drill holes to determine shear and tension strength values for the screws used in cold-formed steel connections. The thesis presents the design methods and test program conducted to investigate the behavior and strength of the screw connections in shear and tension test. Test results were compared with AISI design provisions to determine if new design equations will be developed for those screws used in BAC cooling tower applications. LRFD resistance factors and ASD safety factors were investigated to the proposed design equations.