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Two-Phase Spray Cooling with Water/2-Propanol Binary Mixtures for High Heat Flux Focal Source (open access)

Two-Phase Spray Cooling with Water/2-Propanol Binary Mixtures for High Heat Flux Focal Source

Two-phase spray cooling has been an emerging thermal management technique offering high heat transfer coefficients and critical heat flux levels, near-uniform surface temperatures, and efficient coolant usage that enables to design of compact and lightweight systems. Due to these capabilities, spray cooling is a promising approach for high heat flux applications in computing, power electronics, and optics. Two-phase spray cooling inherently depends on saturation temperature-pressure relationships of the working fluid to take advantage of high heat transfer rates associated with liquid-vapor phase change. When a certain application requires strict temperature and/or pressure conditions, thermo-physical properties of the working fluid play a critical role in attaining proper efficiency, reliability, or packaging structure. However, some of the commonly used single-component working fluids have relatively poor properties and heat transfer performance. For example, water is the best coolant in terms of properties, yet in certain applications where the system operates at low temperature ambient, it cannot be implemented due to freezing risk. The common solution for this problem is to use the antifreeze mixtures (binary mixtures of water and alcohol) to reduce the freezing point. In such cases, utilizing binary mixtures to tune working fluid properties becomes an alternative approach. This study has …
Date: December 2016
Creator: Obuladinne, Sai Sujith
System: The UNT Digital Library
Two-Phase Spray Cooling with HFC-134a and HFO-1234yf for Thermal Management of Automotive Power Electronics using Practical Enhanced Surfaces (open access)

Two-Phase Spray Cooling with HFC-134a and HFO-1234yf for Thermal Management of Automotive Power Electronics using Practical Enhanced Surfaces

The objective of this research was to investigate the performance of two-phase spray cooling with HFC-134a and HFO-1234yf refrigerants using practical enhanced heat transfer surfaces. Results of the study were expected to provide a quantitative spray cooling performance comparison with working fluids representing the current and next-generation mobile air conditioning refrigerants, and demonstrate the feasibility of this approach as an alternative active cooling technology for the thermal management of high heat flux power electronics (i.e., IGBTs) in electric-drive vehicles. Potential benefits of two-phase spray cooling include achieving more efficient and reliable operation, as well as compact and lightweight system design that would lead to cost reduction. The experimental work involved testing of four different enhanced boiling surfaces in comparison to a plain reference surface, using a commercial pressure-atomizing spray nozzle at a range of liquid flow rates for each refrigerant to determine the spray cooling performance with respect to heat transfer coefficient (HTC) and critical heat flux (CHF). The heater surfaces were prepared using dual-stage electroplating, brush coating, sanding, and particle blasting, all featuring "practical" room temperature processes that do not require specialized equipment. Based on the obtained results, HFC-134a provided a better heat transfer performance through higher HTC and …
Date: August 2017
Creator: Altalidi, Sulaiman Saleh
System: The UNT Digital Library
Seismic Performance Evaluation of Novel Cold-Formed Steel Framed Shear Walls Sheathed with Corrugated Steel Sheets (open access)

Seismic Performance Evaluation of Novel Cold-Formed Steel Framed Shear Walls Sheathed with Corrugated Steel Sheets

This thesis presents experiments and numerical analysis of a novel cold-formed steel framed shear wall sheathed with corrugated steel sheets. The objective of this newly designed shear wall is to meet the growing demand of mid-rise buildings and the combustibility requirement in the International Building Code. The strength of the novel shear wall is higher than currently code certified shear wall in AISI S400-15 so that it could be more favorable for mid-rise building in areas that are prone to earthquakes and hurricanes. Full-scale monotonic and cyclic tests were conducted on bearing walls and shear walls under combined lateral and gravity loads. Though the gravity loads had negative effects on the strength and stiffness of the shear wall due to the buckling of the chord framing members, it still shows promise to be used in mid-rise buildings. The objective of numerical analysis is to quantify the seismic performance factors of the newly design shear wall lateral-force resisting system by using the recommended methodology in FEMA P695. Two groups of building archetypes, story varied from two to five, were simulated in OpenSees program. Nonlinear static and dynamic analysis were performed in both horizontal directions of each building archetype. Finally, the results …
Date: August 2017
Creator: Lan, Xing
System: The UNT Digital Library
Investigation of Immersion Cooled ARM-Based Computer Clusters for Low-Cost, High-Performance Computing (open access)

Investigation of Immersion Cooled ARM-Based Computer Clusters for Low-Cost, High-Performance Computing

This study aimed to investigate performance of ARM-based computer clusters using two-phase immersion cooling approach, and demonstrate its potential benefits over the air-based natural and forced convection approaches. ARM-based clusters were created using Raspberry Pi model 2 and 3, a commodity-level, single-board computer. Immersion cooling mode utilized two types of dielectric liquids, HFE-7000 and HFE-7100. Experiments involved running benchmarking tests Sysbench high performance linpack (HPL), and the combination of both in order to quantify the key parameters of device junction temperature, frequency, execution time, computing performance, and energy consumption. Results indicated that the device core temperature has direct effects on the computing performance and energy consumption. In the reference, natural convection cooling mode, as the temperature raised, the cluster started to decease its operating frequency to save the internal cores from damage. This resulted in decline of computing performance and increase of execution time, further leading to increase of energy consumption. In more extreme cases, performance of the cluster dropped by 4X, while the energy consumption increased by 220%. This study therefore demonstrated that two-phase immersion cooling method with its near-isothermal, high heat transfer capability would enable fast, energy efficient, and reliable operation, particularly benefiting high performance computing applications where …
Date: August 2017
Creator: Mohammed, Awaizulla Shareef
System: The UNT Digital Library
A Computer-Based Process Control System for a Target Station in a LINAC Facility (open access)

A Computer-Based Process Control System for a Target Station in a LINAC Facility

An event-driven, sequential, process control system was designed for International Isotopes, Inc., to automate and remotely control a target station at the company's linear accelerator facility. The designed system consisted of two major sections: a software program (virtual instrument), which was developed by LabVIEW, and a hardware interface (FieldPoint Modular Distributed I/O System by National Instrument), which had to be a pre-developed system that did not require customization. The designed virtual instrument was tested on a simulation model that mimed the target station. The result was a valid design.
Date: May 1999
Creator: Al-Shantaf, Abdulraouf O.
System: The UNT Digital Library
Development of a Simplified Fracture Toughness Tool for Polymers (open access)

Development of a Simplified Fracture Toughness Tool for Polymers

This thesis presents research toward the development of a simple inexpensive fracture toughness tool for polymeric materials. Experiments were conducted to test the specimen configuration and the fracture toughness tool against an established ASTM standard for polymer fracture toughness, D5045, and a commonly used four-point bend method. The materials used in this study were polycarbonate and high density polyethylene. Reductions in both the production time and the variability resulting from the preparation of the specimens were addressed through the use of specially designed fixtures. The effects from the razor cut depths used in the chevron notch were compared to the fracture toughness values obtained in order to determine the effect upon the validity of the fracture toughness.
Date: August 1997
Creator: Marnock, Patrick J. (Patrick Joseph)
System: The UNT Digital Library
Fracture Toughness Testing of Plastics under Various Environmental Conditions (open access)

Fracture Toughness Testing of Plastics under Various Environmental Conditions

The primary objective of this study is to test the applicability to plastics of a fracture toughness testing tool developed for metals. The intent is to study pre-test conditioning of several plastic materials and the effect of the depth of the razor notch cut in the chevron notched fracture toughness test specimens. The study includes the careful preparation of samples followed by conditioning in various environments. Samples were subjected to laboratory air for a specific duration or to a controlled temperature-humidity condition as per the ASTM D1870. Some of the samples were subjected to vacuum conditioning under standard test specifications. Testing was conducted using the conventional three-point bend test as per ASTM D5045-95. ASTM E1304, which sets a standard for short rod and bar testing of metals and ceramics provides some basis for conducting chevron notched four-point bend tests to duplicate the toughness tool. Correlation of these results with the ASTM test samples is determined. The four-point bend test involves less specimen machining as well as time to perform the fracture toughness tests. This study of fracture toughness testing has potential for quality control as well as the fracture property determination.
Date: December 1997
Creator: Velpuri, Seshagirirao V.
System: The UNT Digital Library
A Data Acquisition System Experiment for Gas Temperature and Pressure Measurements on a Liquid-Nitrogen-Powered Vehicle (open access)

A Data Acquisition System Experiment for Gas Temperature and Pressure Measurements on a Liquid-Nitrogen-Powered Vehicle

A data acquisition system was set up to measure gas temperatures and pressures at various points on a liquid-nitrogen-powered vehicle. The experiment was attempted to develop a data acquisition method for applications on engines that use liquid air as the fuel. Two thermocouples and a pressure transducer were connected using data acquisition instruments interfaced to a laptop computer to acquire data.
Date: May 1998
Creator: Lui, Samson Sze-Sang
System: The UNT Digital Library
Laser Cutting Machine: Justification of initial costs (open access)

Laser Cutting Machine: Justification of initial costs

The Industrial Laser is firmly established in metalcutting as the tool of choice for many applications. The elevator division of Montgomery KONE Inc., in an effort to move towards quality, ontime, complete deliveries and 100% customer satisfaction, decided to invest in new equipment to improve manufacturing processes. A huge investment is proposed for a laser-cutting machine. It is the responsibility of Manufacturing Engineering to direct the management by justifying its benefits, which includes payback time and financial gains. Factors such as common line cutting, automated material handling system and cutting time were involved in justification of the initial cost of a laser-cutting machine. Comparative statistics on appropriate factors accurately determine and justify the initial cost of a laser-cutting machine.
Date: May 2001
Creator: Nagaraja, Dwarakish
System: The UNT Digital Library
Investigation of the feasibility of non-invasive carbon dioxide detection using spectroscopy in the visible spectrum. (open access)

Investigation of the feasibility of non-invasive carbon dioxide detection using spectroscopy in the visible spectrum.

Pulse oximeters are used in operating rooms and recovery rooms as a monitoring device for oxygen in the respiratory system of the patient. The advantage of pulse oximeters over other methods of oxygen monitoring is that they are easy to use and they are non-invasive, which means it is not necessary break the skin to extract blood for information to be obtained. The standard for the measurement of partial pressure of CO2 and O2 is an arterial blood gas analysis (ABG). However routine monitoring using this method on a continuous basis is impractical since it is slow, painful and invasive. Measuring carbon dioxide is critical to preventing ailments such as carbon dioxide poisoning or hypoxia. The problem is, currently there is no known effective non-invasive method for accurately measuring carbon dioxide in the body to properly assess the adequacy of ventilation. The objective of this study was to experimentally use spectroscopy in the visible spectrum and the principles of operation of a pulse oximeter to incorporate a method of non-invasive real-time carbon dioxide monitoring that is as quick and easy to use.
Date: December 2007
Creator: Marks, Damian
System: The UNT Digital Library
Determination of the Shelf Life of Aluminum Electrolytic Capacitors. (open access)

Determination of the Shelf Life of Aluminum Electrolytic Capacitors.

The aluminum electrolytic capacitor is used extensively in the electric utility industry. A factor limiting the storage of spare capacitors is the integrity of the aluminum oxide dielectric, which over time breaks down contributing to a shelf life currently estimated at one nuclear power electric generating station to be approximately five years. This project examined the electrical characteristics of naturally aged capacitors of several different styles to determine if design parameters were still within limits. Additionally, the effectiveness of a technique known as “Reforming” was examined to determine its impact on those characteristics.
Date: May 2002
Creator: Wynne, Edward McFaddin
System: The UNT Digital Library
Effects of Rebar Temperature and Water to Cement Ratio on Rebar-Concrete Bond Strength of Concrete Containing Fly Ash (open access)

Effects of Rebar Temperature and Water to Cement Ratio on Rebar-Concrete Bond Strength of Concrete Containing Fly Ash

This research presents the results on an experimental investigation to identify the effects of rebar temperature, fly ash and water to cement ratio on concrete porosity in continuously reinforced concrete pavements (CRCP). Samples were cast and analyzed using pullout tests. Water to cement ratio (w/c) and rebar temperature had a significant influence on the rebar-concrete bond strength. The 28-day shear strength measurements showed an increase in rebar-concrete bond strength as the water to cement ratio (w/c) was reduced from 0.50 to 0.40 for both fly ash containing and non fly ash control samples. There was a reduction in the peak pullout load as the rebar surface temperature increased from 77o F to 150o F for the cast samples. A heated rebar experiment was performed simulating a rebar exposed to hot summer days and the rebar cooling curves were plotted for the rebar temperatures of 180o F - 120o F. Fourier transform infrared spectroscopy was performed to show the moisture content of cement samples at the rebar-concrete interface. Mercury intrusion porosimetry test results on one batch of samples were used for pore size distribution analysis. An in-depth analysis of the morphological characteristics of the rebar-concrete interface and the observation of pores …
Date: May 2010
Creator: Pati, Ardeep Ranjan
System: The UNT Digital Library
Cost Savings Realized Through Proper Sizing of an Excessive Instrument Air System. (open access)

Cost Savings Realized Through Proper Sizing of an Excessive Instrument Air System.

The purpose of this research was to determine if installing a smaller air compressor could reduce the electrical usage of a large semiconductor manufacturing plant. A 200 horsepower Atlas Copco compressor was installed with the existing 500 horsepower Ingersoll-Rand compressors. Testing was conducted during the regular manufacturing process at MEMC Southwest in Sherman, Texas. Analysis of the data found that installing the new compressor could reduce electrical consumption. The study also found there are specific operational setpoints that allow the compressor to operate more efficiently.
Date: December 2003
Creator: Condron, Ewell D.
System: The UNT Digital Library

Effects of Thickness and Indenter Tip Geometry in Nanoindentation of Nickel Films

Access: Use of this item is restricted to the UNT Community
Nanoindentation has become a widely used technique to measure the mechanical properties of materials. Due to its capability to deform materials in micro- and nano-scale, nanoindentation has found more applications in characterizing the deformation behavior and determining the mechanical properties of thin films and coatings. This research deals with the characterization of samples received from Center for Advanced Microstructures and Devices (CAMD) and Integran Technologies Inc., Toronto, Canada and the objective of this investigation was to utilize the experimental data obtained from nanoindentation to determine the deformation behavior, mechanical properties of thin films on substrates and bulk materials, and the effect of geometrically different indenters (Berkovich, cubecorner, and conical). X-ray diffraction (XRD), transmission electron microscope (TEM), scanning electron microscopy (SEM), and atomic force microscopy (AFM) analysis were performed on these materials to determine the crystal orientation, grain size of the material, and also to measure any substrate effects like pile-up or sin-in respectively. The results indicate that indentation size effect (ISE) strongly depends on shape of the indenter and less sensitive to penetration depth where as the hardness measurements depends on shape of indenter and depth of penetration. There is a negligible strain rate dependency of hardness at deeper depths …
Date: May 2004
Creator: Parakala, Padma
System: The UNT Digital Library

Design of Power Amplifier Test Signals with a User-Defined Multisine

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Cellular radio communication involves wireless transmission and reception of signals at radio frequencies (RF). Base stations house equipment critical to the transmission and reception of signals. Power amplifier (PA) is a crucial element in base station assembly. PAs are expensive, take up space and dissipate heat. Of all the elements in the base station, it is difficult to design and operate a power amplifier. New designs of power amplifiers are constantly tested. One of the most important components required to perform this test successfully is a circuit simulator model of an entire communication system that generates a standard test signal. Standard test signals 524,288 data points in length require 1080 hours to complete one test of a PA model. In order to reduce the time taken to complete one test, a 'simulated test signal,' was generated. The objective of this study is to develop an algorithm to generate this 'simulated' test signal such that its characteristics match that of the 'standard' test signal.
Date: May 2004
Creator: Nagarajan, Preeti
System: The UNT Digital Library
Sunlight readability and luminance characteristics of light-emitting diode push button switches. (open access)

Sunlight readability and luminance characteristics of light-emitting diode push button switches.

Lighted push button switches and indicators serve many purposes in cockpits, shipboard applications and military ground vehicles. The quality of lighting produced by switches is vital to operators' understanding of the information displayed. Utilizing LED technology in lighted switches has challenges that can adversely affect lighting quality. Incomplete data exists to educate consumers about potential differences in LED switch performance between different manufacturers. LED switches from four different manufacturers were tested for six attributes of lighting quality: average luminance and power consumption at full voltage, sunlight readable contrast, luminance contrast under ambient sunlight, legend uniformity, and dual-color uniformity. Three of the four manufacturers have not developed LED push button switches that meet lighting quality standards established with incandescent technology.
Date: May 2004
Creator: Fitch, Robert J.
System: The UNT Digital Library
Effect of Amines as Corrosion Inhibitors for a Low Carbon Steel in Power Industry (open access)

Effect of Amines as Corrosion Inhibitors for a Low Carbon Steel in Power Industry

Commonly used amines in power industry, including morpholine, DBU (1,8-diazabicyclo[5.4.0]undec-7-ene), and DMA (dimethylallylamine) were evaluated for their effect on AISI 1018 steel at 250oF. Samples were exposed to an autoclave containing amine added aqueous solution at pH of 9.5 for 1, 2, 4, 6, 8, and 12 hours. Morphology studies were carried using scanning electron microscope (SEM), phase analysis was done utilizing Fourier transform infrared spectroscopy (FTIR), and weight loss was performed to assess kinetics of oxidation. Control samples showed the highest metal dissolution rate. DBU showed the best performance in metal protection and SEM indicated the presence of a free-crack layer formed by fine particles in that set. FTIR showed that DBU apparently favored the formation of magnetite. It is believed that fine particles impede intrusion of aggressive ions into the metal surface by forming a barrier layer. FTIR demonstrated that DMA formed more oxyhydroxides, whereas morpholine presented magnetite to hematite transformation as early as 2 hours. SEM revealed that control and DMA produced acicular particles characteristic of oxyhydroxides while morpholine and DBU presented more equiaxed particles.
Date: December 2004
Creator: Díaz, Jorge G.
System: The UNT Digital Library
Computer Virus Spread Containment Using Feedback Control. (open access)

Computer Virus Spread Containment Using Feedback Control.

In this research, a security architecture based on the feedback control theory has been proposed. The first loop has been designed, developed and tested. The architecture proposes a feedback model with many controllers located at different stages of network. The controller at each stage gives feedback to the one at higher level and a decision about network security is taken. The first loop implemented in this thesis detects one important anomaly of virus attack, rate of outgoing connection. Though there are other anomalies of a virus attack, rate of outgoing connection is an important one to contain the spread. Based on the feedback model, this symptom is fed back and a state model using queuing theory is developed to delay the connections and slow down the rate of outgoing connections. Upon implementation of this model, whenever an infected machine tries to make connections at a speed not considered safe, the controller kicks in and sends those connections to a delay queue. Because of delaying connections, rate of outgoing connections decrease. Also because of delaying, many connections timeout and get dropped, reducing the spread. PID controller is implemented to decide the number of connections going to safe or suspected queue. Multiple …
Date: December 2004
Creator: Yelimeli Guruprasad, Arun
System: The UNT Digital Library
Characterization of Boron Nitride Thin Films on Silicon (100) Wafer. (open access)

Characterization of Boron Nitride Thin Films on Silicon (100) Wafer.

Cubic boron nitride (cBN) thin films offer attractive mechanical and electrical properties. The synthesis of cBN films have been deposited using both physical and chemical vapor deposition methods, which generate internal residual, stresses that result in delamination of the film from substrates. Boron nitride films were deposited using electron beam evaporation without bias voltage and nitrogen bombardment (to reduce stresses) were characterize using FTIR, XRD, SEM, EDS, TEM, and AFM techniques. In addition, a pin-on-disk tribological test was used to measure coefficient of friction. Results indicated that samples deposited at 400°C contained higher cubic phase of BN compared to those films deposited at room temperature. A BN film containing cubic phase deposited at 400°C for 2 hours showed 0.1 friction coefficient.
Date: August 2007
Creator: Maranon, Walter
System: The UNT Digital Library

Synthesis of cubic boron nitride thin films on silicon substrate using electron beam evaporation.

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Cubic boron nitride (cBN) synthesis has gained lot of interest during the past decade as it offers outstanding physical and chemical properties like high hardness, high wear resistance, and chemical inertness. Despite of their excellent properties, every application of cBN is hindered by high compressive stresses and poor adhesion. The cost of equipment is also high in almost all the techniques used so far. This thesis deals with the synthesis of cubic phase of boron nitride on Si (100) wafers using electron beam evaporator, a low cost equipment that is capable of depositing films with reduced stresses. Using this process, need of ion beam employed in ion beam assisted processes can be eliminated thus reducing the surface damage and enhancing the film adhesion. Four sets of samples have been deposited by varying substrate temperature and the deposition time. scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS), and Fourier transform infrared spectroscopy (FTIR) techniques have been used to determine the structure and composition of the films deposited. X-ray diffraction (XRD) was performed on one of the samples to determine the thickness of the film deposited for the given deposition rate. Several samples showed dendrites being formed as …
Date: May 2004
Creator: Vemuri, Prasanna
System: The UNT Digital Library

Nodal Resistance Measurement System

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The latest development in the measurement techniques has resulted in fast improvements in the instruments used for measurement of various electrical quantities. A common problem in such instruments is the automation of acquiring, retrieving and controlling the measurements by a computer or a laptop. In this study, nodal resistance measurement (NRM) system is developed to solve the above problem. The purpose of this study is to design and develop a compact electronic board, which measures electrical resistance, and a computer or a laptop controls the board. For the above purpose, surface nodal points are created on the surface of the sample electrically conductive material. The nodal points are connected to the compact electronic board and this board is connected to the computer. The user selects the nodal points, from the computer, between which the NRM system measures the electrical resistance and displays the measured quantity on the computer.
Date: May 2005
Creator: Putta, Sunil Kumar
System: The UNT Digital Library

Development of a Hybrid Molecular Ultraviolet Photodetector based on Guanosine Derivatives

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Modern studies on charge transfer reaction and conductivity measurements of DNA have shown that the electrical behavior of DNA ranges from that of an insulator to that of a wide bandgap semiconductor. Based on this property of DNA, a metal-semiconductor-metal photodetector is fabricated using a self-assembled layer of deoxyguanosine derivative (DNA base) deposited between gold electrodes. The electrodes are lithographically designed on a GaN substrate separated by a distance L (50nm < L < 100nm). This work examines the electrical and optical properties of such wide-bandgap semiconductor based biomaterial systems for their potential application as photodetectors in the UV region wherein most of the biological agents emit. The objective of this study was to develop a biomolecular electronic device and design an experimental setup for electrical and optical characterization of a novel hybrid molecular optoelectronic material system. AFM results proved the usage of Ga-Polar substrate in conjugation with DG molecules to be used as a potential electronic based sensor. A two-terminal nanoscale biomolectronic diode has been fabricated showing efficient rectification ratio. A nanoscale integrated ultraviolet photodetector (of dimensions less than 100 nm) has been fabricated with a cut-off wavelength at ~ 320 nm.
Date: December 2005
Creator: Liddar, Harsheetal
System: The UNT Digital Library

Surface Plasmon Based Nanophotonic Optical Emitters

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Group- III nitride based semiconductors have emerged as the leading material for short wavelength optoelectronic devices. The InGaN alloy system forms a continuous and direct bandgap semiconductor spanning ultraviolet (UV) to blue/green wavelengths. An ideal and highly efficient light-emitting device can be designed by enhancing the spontaneous emission rate. This thesis deals with the design and fabrication of a visible light-emitting device using GaN/InGaN single quantum well (SQW) system with enhanced spontaneous emission. To increase the emission efficiency, layers of different metals, usually noble metals like silver, gold and aluminum are deposited on GaN/InGaN SQWs using metal evaporator. Surface characterization of metal-coated GaN/InGaN SQW samples was carried out using atomic force microscopy (AFM) and scanning electron microscopy (SEM). Photoluminescence is used as a tool for optical characterization to study the enhancement in the light emitting structures. This thesis also compares characteristics of different metals on GaN/InGaN SQW system thus allowing selection of the most appropriate material for a particular application. It was found out that photons from the light emitter couple more to the surface plasmons if the bandgap of former is close to the surface plasmon resonant energy of particular metal. Absorption of light due to gold reduces the …
Date: December 2005
Creator: Vemuri, Padma Rekha
System: The UNT Digital Library

Characterization of Iron Oxide Deposits Formed at Comanche Peak Steam Electric Station

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The presence of deposits leading to corrosion of the steam generator (SG) systems is a major contributor to operation and maintenance cost of pressurized water reactor (PWR) plants. Formation and transport of corrosion products formed due to the presence of impurities, metallic oxides and cations in the secondary side of the SG units result in formation of deposits. This research deals with the characterization of deposit samples collected from the two SG units (unit 1 and unit 2) at Comanche Peak Steam Electric Station (CPSES). X-ray diffraction (XRD), Fourier transform infrared spectrophotometry (FTIR), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) techniques have been used for studying the compositional and structural properties of iron oxides formed in the secondary side of unit 1 and unit 2. Magnetite (Fe3O4) was found to be predominant in samples from unit 1 and maghemite (g-Fe2O3) was found to be the dominant phase in case of unit 2. An attempt has been made to customize FTIR technique for analyzing different iron oxide phases present in the deposits of PWR-SG systems.
Date: May 2003
Creator: Namduri, Haritha
System: The UNT Digital Library