Report describing the results of the cupferron extraction-copper spark method in determining the impurity elements in plutonium metal. This was required the 234-5 Project analytical program.

The following document describes the usage of Vinylite or plastic sheeting for operation and maintenance across a contamination barrier, presenting ecological advantages, photos of special equipment and techniques used during procedure, and the purpose of eliminating open air transfer in contaminated area.

Summary: "The laboratory data collected during the metallurgical evaluation of these rods indicate that lower rolling temperatures increased the ultimate and yield strength, the amount of cold work, and the degree of preferred orientation existing in these uranium rods."

Abstract: "A batch of slugs is being prepared for which the U-235 content will be 1.75 per cent, and it is of interest to calculate the minimum number of such slugs required for a critical assembly in water. Using Handbook (CL-697) methods, a critical assembly of these slugs arranged in a lattice with a spacing of 5.5 cm."

Introduction: "When uranium slugs are irradiated in the Hanford piles, one of the many substances formed is U-237. It arises primarily from the reaction: U-238 (n,2n) U-237. This uranium isotope is a beta and gamma emitter with a half-life of 6.7 days. Because it is isotopic with U-238, it accompanies the uranium recovered by the Redox Process, and its concentration is, of course, not diminished by the fission-product decontamination cycles. As a consequence, the maximum total decontamination of irradiated uranium which can be achieved depends upon the quantity of U-237 present in the processed uranium."

The purpose of the test used to make this report was to determine if anodizing could become a part of the canning operation prior to autoclaving, other factors permitting, or if it must follow autoclaving.

Introduction: "The carrier (pyroelectric) concentration method is commonly used in the spectrographic analysis of plutonium metal. This report describes work which lead to substantial improvements in accuracy, precision and ease with which the analysis is made. Included are data from analyses of plutonium metal by the original and the improved carrier methods, and the cupferron extraction method."

The following report describes a successful procedure used for the determination of americium in the presence of plutonium. Provided are articles listed that describe the research done in developing the method.

"An apparatus was designed and fabricated to obtain film samples from irradiated process slugs. This apparatus has been used to obtain film samples from slugs of the sodium dichromate elimination test."

This report discusses preliminary results acquired from investigations made on the ultrasonic properties of uranium, such as sonic vibrations in the megacycle frequency range.

From abstract: "Three methods for measuring the iodine which passes through a charcoal trap in a stream of helium are discussed."

Report describing alternative methods for depleting a large turnings inventory in a short period of time.

Introduction: "During the early planning of the multicurie cells at Hanford it was decided that a slave type manipulator would be necessary to perform the experiments for which the cells were being designed. The design required steel roofs for installation through a port hole in the face. Technical Services Equipment Development began developing the proposed manipulator in January 1951 by making a study of those existing at that tune. None met the requirements which had been established; therefore, the design of a special manipulator was started immediately."

From introduction: "This report gives the results of a 1000-hour corrosion test of SAE 1010, low carbon steel, in synthetic Redox waste solutions...The present test was designed to obtain corrosion rates for waste solution temperatures of 180 F, 200 F, and 220 F in solutions neutralized to pH values of 11, 12, and 13.

Introduction: "Knowledge of the mechanical properties of uranium at elevated temperature is essential in order to understand and predict the fabrication characteristics and pile behavior of this metal. This report presents the experimental data obtained from beta heat-treated specimens which were originally machined from one production, alpha-rolled uranium rod."

This following report discusses certain topics pertinent to the x-ray photometric method, such as the optimum size of sample and of sample concentration, the technique of measurement for high precision, the use of easily prepared uranium standards for future calibrations and corrections for extraneous substances, and it compares results obtained by both x-ray and chemical assays.

Abstract: "Experiments were performed to characterize the types of nitro compounds that might be formed by reaction of Shell Spray Base with nitric acid, to determine the extent of their formation, if any, and their path under conditions of nitric acid recovery in the Purex Process. It is concluded that the instability of Shell Spray Base to nitration, under conditions to prevail in the plant, presents neither a disposal problem nor a safety problem."

The following report deals with the application of the water boiler neutron source to the exponential experiments in an attempt to speed up lattice testing measurements.

This report discusses the calcination or heating of UO₃. When UO₃ is heated, it loses ionic impurities and can produce uranyl peroxide.

This report follows a manuscript report made in January 11, 1952, and provides results of a survey that gives corrections as well as suggestions for new and local sources of aggregate material in comparison to the original report. These reports were made in response to a heavy desire of improvement in reactor design and shielding.

The following report provides the results of an accelerated corrosion test that was performed to compare the effect of two coagulants on the corrosion rates of aluminum slug jacket alloy and 72S. Additionally, some analytical data on the water from the two treatments were obtained and are presented in this report.

Summary: "Analysis of the power-level transient following the rapid insertion of a large absorber into an operating pile provides an excellent means of determining the reactivity effect of the absorber . Recent improvements in instrumentation make possible the measurement of the strength of the entire vertical safety rod system of the production units by means of this technique, and rapid calibration of the high-speed control rods by means of this technique, and rapid calibration of the high-speed control rods in the H unit is also feasible. The details of the method are presented together with recent experimental confirmation from the Test Pile of certain features of the theory."

Objective: "Production Test 235-1 and an amendment, were written to outline the procedures for reducing the outgassing time and evaluating the effects of these reductions."

From abstract: "The purpose of this investigation was to establish basic rates of formation of chemical films deposited on aluminum surfaces from water flowing over such surfaces. It was desired to obtain specific information, within certain ranges, as to the influence of temperature, water velocity, and type of aluminum on the rate of film formation."