The Coulometric Determination of Acid (open access)

The Coulometric Determination of Acid

Introduction: "The need for a method of acid determination which could be used for small samples and easily adapted to remote control led to the investigation of the use of electrolytically generated base for the titration of acid in certain solutions. The use of electrolytically generated base for the titration of acetic acid in the presence of nitric acid has been reported (1)."
Date: March 1, 1950
Creator: Carson, W. N. & Ko, Roy
System: The UNT Digital Library
The Development of Plutonium Electrodeposition Methods : Interim Report (open access)

The Development of Plutonium Electrodeposition Methods : Interim Report

From introduction: "The following report presents a body of information obtained in the Health Instrument Development Laboratory from September, 1948, to the present, and is intended to be a preliminary review of [the study of electrodeposition of plutonium]. Many improvements in technique and methods and investigations along lines not explored are suggested by the present work. These will be undertaken as time permits, and reported at a later time."
Date: March 1, 1950
Creator: Schwendiman, L. C.
System: The UNT Digital Library
The Gasometric Determination of Nitrite and Sulfamate (open access)

The Gasometric Determination of Nitrite and Sulfamate

This report covers an investigation made to develop a gasometric determination that can determine 1.2 x 10-(-5) g. of nitrite with a precision (99% limits) of +/- 8%, and discusses how this procedure works.
Date: March 6, 1950
Creator: Carson, W. N.
System: The UNT Digital Library
Corrosion of Stellite in MJ-1 Streams (open access)

Corrosion of Stellite in MJ-1 Streams

The following report provides data from completed tests for corrosion testing of stellite-T347 stainless steel test cylinders.
Date: March 8, 1950
Creator: Koenig, W. W.
System: The UNT Digital Library
Infrared Absorption Measurements Indicating Intermolecular Association of Water and Hexone (open access)

Infrared Absorption Measurements Indicating Intermolecular Association of Water and Hexone

This report analyzes infrared absorption measurements that were made in the regions of carbonyl band and hydroxyl band absorptions on solutions of water in hexone and water in acetone, confirming intermolecular association of water and hexone.
Date: March 8, 1950
Creator: Moore, R. H.
System: The UNT Digital Library
The Determination of Tributyl Phosphate in Deodorized Shell Base with the Infrared Spectrometer (open access)

The Determination of Tributyl Phosphate in Deodorized Shell Base with the Infrared Spectrometer

The following report describes methods used to determine tributylphosphate in a deodorized shell base. An infrared absorption method is developed to emphasize toward determination of TBP in RCW streams, the organic waste streams.
Date: March 10, 1950
Creator: Moore, R. H.
System: The UNT Digital Library
Statistical evaluation of calibrartion data-infrared method for determination of % TBP (open access)

Statistical evaluation of calibrartion data-infrared method for determination of % TBP

A report which discusses the data submitted for evaluation. This data is about optical densities from infrared spectrometer readings on eight standard samples, ranging in percent TBP from 6.71 to 17.85.
Date: March 21, 1950
Creator: Healy, W. C.
System: The UNT Digital Library
The Oxidation of Plutonium to the Plutonyl State (open access)

The Oxidation of Plutonium to the Plutonyl State

This report follows the study of the oxidation of plutonium III and IV to the plutonyl state.
Date: March 22, 1950
Creator: Miller, H. W. & Brouns, R. J.
System: The UNT Digital Library
The Preparation of Thin Films of Plutonium by Electrodeposition (open access)

The Preparation of Thin Films of Plutonium by Electrodeposition

This report discusses methods for preparing thin films of plutonium on metallic disks, which are used for alpha energy analysis, fission counting, and preparation of geometry standards in ordinary counting. Various methods of preparation were tested and analyzed, but electrodeposition was the most effective method. Deposition was then tested, but the yields were "somewhat erratic".
Date: March 22, 1950
Creator: Miller, H. W. & Brouns, R. J.
System: The UNT Digital Library
P-10 Chemical Equilibria (open access)

P-10 Chemical Equilibria

This report studies tritium oxides and tritium in water vapor, a product of P-10.
Date: March 23, 1950
Creator: Roesch, William C.
System: The UNT Digital Library
Solubility relationships of acidified stored metal wastes (open access)

Solubility relationships of acidified stored metal wastes

The reports aims to determine the solubility limitation of concentrations of uranium in the food preparation step of the tributyl phosphate waste metal recovery process, and the subsequent solubilities in the RA column.
Date: March 24, 1950
Creator: Curtis, M. H.
System: The UNT Digital Library
Uranium phase equilibria in the TBP process (open access)

Uranium phase equilibria in the TBP process

A report intended to correlate the RA and RC Column uranium equilibrium data presented in the reports cited in the introduction.
Date: March 1, 1951
Creator: Granquist, D. P. & Merrill, E. T.
System: The UNT Digital Library
Kinetics of Plutonium Reduction in the Redox IB Column (open access)

Kinetics of Plutonium Reduction in the Redox IB Column

The following report describes work carried out to investigate whether the Hanford IB column as designed in a previous report will decontaminate the uranium adequately from plutonium, particularly if there's any slowness in either the rate of reduction or transfer of the plutonium.
Date: March 20, 1951
Creator: Moore, Robert Lee
System: The UNT Digital Library
Canning depleted uranium : production test 313-110-M, final report (open access)

Canning depleted uranium : production test 313-110-M, final report

From summary: "Uranium billets deficient in U235 were subjected to the normal successive steps in the slug fabrication process; viz., rolling, machining, and canning. No unusual behavior was observed at any point in the process, thus indicating that the depleted metal from the standpoint of mechanical properties can be considered equivalent to normal uranium."
Date: March 27, 1951
Creator: Jones, T. S.
System: The UNT Digital Library
Recent Changes Affecting the Specifications Concerning Activity Levels in Reclaimed Uranium (open access)

Recent Changes Affecting the Specifications Concerning Activity Levels in Reclaimed Uranium

Report that communicates a new permissible activity level of plutonium and uranium.
Date: March 27, 1951
Creator: Gamertsfelder, C. C.
System: The UNT Digital Library
Review of the Xenon Problem (open access)

Review of the Xenon Problem

Report discussing studies regarding the properties and nuclear constants of xenon, an element relevant to use of high power thermal neutron reactors.
Date: March 12, 1952
Creator: Gast, P. F.
System: The UNT Digital Library
Corrosive Effects of Heavy Metal Ions on Aluminum (open access)

Corrosive Effects of Heavy Metal Ions on Aluminum

From summary: The object of the study was to determine if the heavy metal ions within the concentration ranges normally found in pile cooling water were responsible for corrosion of aluminum.
Date: March 17, 1953
Creator: Fujioka, G. S.
System: The UNT Digital Library
Investigation of Explosive Characteristics of Purex Solvent Decomposition Products (Red Oil) (open access)

Investigation of Explosive Characteristics of Purex Solvent Decomposition Products (Red Oil)

Abstract: "Laboratory production of an explosion between UNH and "red oil" under calcination conditions has been accomplished. Attempted production of a vapor phase explosion was unsuccessful below 150-160 C. Since such severe conditions are necessary to obtain an explosive reaction, it appears that present Purex plant design is adequate to avoid explosive conditions."
Date: March 17, 1953
Creator: Wagner, Robert M.
System: The UNT Digital Library
The Quantitative Recovery of Plutonium From Laboratory Residues (open access)

The Quantitative Recovery of Plutonium From Laboratory Residues

Report discussing the procedures and experimental data of various plutonium waste recovery methods. The report elaborates on the different methods of collection necessary for different wastes.
Date: March 18, 1953
Creator: Ferguson, W. S.
System: The UNT Digital Library
Factors Affecting the Concentration of TBP Plant Wastes (open access)

Factors Affecting the Concentration of TBP Plant Wastes

Introduction: "The problem of determining the properties and necessary controls on the TBP Plant waste disposal to eliminate transport line plugging and to permit higher concentration prior to return of this to the tank farms was studied. A report of preliminary findings was made to L. W. Finsh on January 31, 1953. This report compiles information in the aforementioned report and findings since its issuance. Previous studies related to this problem are summarized in the U. R. Technical Manual, HW-19140."
Date: March 25, 1953
Creator: Shepard, D. F.
System: The UNT Digital Library
General Flattening and Power Curves (open access)

General Flattening and Power Curves

Introduction: "In the evaluation of pile designs it is necessary to know how the production varies with the number of tubes. It has been possible to solve the problem in terms of some general parameters whose values may be quickly computed for any specific design when the pertinent information is available."
Date: March 30, 1953
Creator: Gast, Paul F.
System: The UNT Digital Library
Investigation of Redox D-12 Waste Concentrator No. 2 Coil Nest Failure (open access)

Investigation of Redox D-12 Waste Concentrator No. 2 Coil Nest Failure

Four D-12 coil nests have failed since the start-up of the Redox Separations plant. Due to the high contamination and radiation levels of these vessels, the cost of decontamination has prevented the examination of all but one of the four. It was hoped that the examination of D-12 pot #2 would lead to an explanation of all four failures. This report will deal primarily with the metallurgical examination of the failure of D-12 pot #2.
Date: March 2, 1954
Creator: Groves, N. D. & Smith, W. R.
System: The UNT Digital Library
The Resistance of Various Bearing Materials to Chemical Attack by Nitric Acid and Uranyl Nitrate Hexahydrate (open access)

The Resistance of Various Bearing Materials to Chemical Attack by Nitric Acid and Uranyl Nitrate Hexahydrate

The purpose of this study has been to evaluate the chemical resistance of various bearing materials to solutions of nitric acid and uranyl nitrate hexahydrate with views toward selecting the best material to be used as bearings in Purex submerged rotating equipment.
Date: March 11, 1954
Creator: Groves, Norman D.
System: The UNT Digital Library
Laboratory Development of an Electromagnetic Test for Uranium Quality (open access)

Laboratory Development of an Electromagnetic Test for Uranium Quality

An electromagnetic instrument similar to the Multitest was built and used to test 2200 uranium slugs. It was found that the equipment could be used to detect inclusions and cracks in the uranium, but that small cracks are not readily detectable on a production basis unless the material is absolutely uniform in inclusion content. The instrument can be used, however, to sort out hidden defects of a reasonable size and to reject grossly dirty uranium.
Date: March 30, 1954
Creator: Headrick, H. B. & Wood, E. C.
System: The UNT Digital Library