Report discussing the progress made on a research project for the preparation of ductile zirconium during April 1949.

This report analyzes Parian and Teflon that were exposed to solutions of 1AX, 1AS, and 1AF, ANL June 1, 1948 Flowsheet, under conditions described in the following report.

Abstract: "The uranium content of badly contaminated uranium solutions may be determined quickly using visual comparison methods to an accuracy of [...]. This accuracy may be considerably improved by employing the fluorimeter herein described. Interfering ions and their removal using liquid-liquid extractions are considered."

The operation of the Fast Reactor is considered in terms of normal equilibrium conditions and normal shut-down. The proposed loading, control rod adjustment and subsequent "floating" operation are discussed. Safety devices and interlocks are described. Temperature and reactivity changes are examined with respect to various system failures, phase changes, and "flashing" of the reactor. Slow changes due to faulty slug cooling are also considered. The calculations were initially based upon 10 kw operation. Performance tests of the mercury system now indicate that 20-kw operation may be feasible.

Technical report includes three reports of research progress: 1)Neutron scattering by A. Bratenahl; 2) Nuclear Cross Sections, Norman Knable.

This progress report discusses progress on oxidation-reduction studies, including polarography, as well as the Uranium-complex formation including electrical transport and spectro-photometric work. This report covers the work done in the period of February of 1945.

The following report analyzes the hydrolytic behavior of cerium and compares them with the actinides of uranium and plutonium.

Report discussing experiments that were performed to determine whether amino acids in urine could be used as a test of subtle uranium poisoning.

The following report describes procedures taken to utilize the photelometer to procure the most rapid and reliable determinations, but the goal of the tests presented was to create satisfactory dispersions of particles to analyze.

This report describes the use of pile control over atomic power, including the different methods of control.

Technical report includes three reports of research progress: 1)Meson Mass Determination by Grain Counting, W. H. Barkas; 2) The Magnetic Beta Ray Lens Spectrograph, A. C. Helmholz; 3) Anthracene Counters, E. Martinelli.

The following report examines the fission counter, fission plates and activation results of the neutron energy distribution in the center of the Los Alamos plutonium reactor.

The following report presents data and conclusions from investigations of the chemical properties of elements 95 (americium, Am) and 96 (curium, Cu) by means of tracer techniques.

This report for May, 1947 describes progress regarding analytical work, chemical work, beta-counting methods of analysis, ore-dressing and pyrometallurgical studies, and pyrometallurgical work.

Abstract: "Variations in receiver slot design produce changes in quantity and quality of product and recycle, not only instantaneously, but also as a function of time in approaching equilibrium. The case of fixed feed concentration and fixed inventory of Uranium is described here for standard and Dip-Lip wider R slot receivers. The effects of the two types of receivers on recycle and product X and W concentrations, X production rate, plant X utilization efficiency, integrated X production and effective mass output are shown graphically."

Abstract: The procedures recommended for analysis in Department 190 Laboratories, in the Limits Control Laboratory, and in the Analytical Development Laboratories, of all process materials from the HCP cycle are presented in a stepwise manner. A description of the characteristics of each sample type along with a brief description of factors involved in the Analytical Quality Control program is included.

Redux is a thermosetting synthetic resin manufactured by the Resinous Products & Chemical Co., Washington Square, Philadelphia 5, Pa. According to the manufacturer, it is intended for bonding metal to metal and metal to wood. It was apparently intended to replace rivets in aircraft structural parts and recent information indicates that a British airplane, the DeHaviland Dove, is in production using this resin. The adhesive was originally developed in England by Aero research Ltd. Experience at this laboratory has been confined to use of the resin for bonding electrical grade silicon steel laminations. Very strong bonds have been obtained under properly controlled conditions. The bond strength is sufficient to tear 29 gauge (.014") steel when attempting to peel off individual laminations. The bond is sufficiently homogeneous to prevent leaks parallel to the plane of the laminations into a high vacuum system. Experiments at the laboratory have been designed to test the adhesive for use in bonding the laminations which form the pole tips and vacuum chamber lids for the synchrontron magnet.

Report discussing assaying techniques used in the Department of Metallurgy at the Massachusetts Institute of Technology, as well as the equipment used for the techniques.

Report discussing tests that were carried out to determine if a few parts per million of boron can be removed directly from beryllium oxide powder without chemically changing the BeO during the process.

Introduction. The main objective of the Metallurgical Project was the preparation of large quantities of plutonium 239, an isotope of element 94, by the interaction of neutrons and uranium. At the beginning, only predictions of its chemical and biological properties could be made since it is a new element. It was predicted that it would be toxic to tissue by virtue of its high atomic weight, and in addition, that it would be toxic by virtue of its radioactivity. Thus, the preparation and use of the element on a large scale meant the manipulation of, and possible exposure to, toxic quantities. It was, therefore, of practical importance to obtain data which would elaborate on the predicted toxicity. The objectives of the work reported here were to establish the acute toxicity of plutonium in experimental animals and to study the distribution of the element in the body after the administration of a wide range of doses. In the interest of economy of what was, at that time, a rare substance, and of animals and facilities, these two objectives were frequently pursued in the same experiment. The information obtained from the separate experiments is therefore frequently incomplete in one or another respect. …

Abstract: An analysis of the improved Model Number 350 Process Monitor was made so that it could be determined if this instrument would fulfill the need for gamma radiation detection instruments in the production buildings of Y-12. The results of these tests indicated the possibility of marked improvement in the monitor characteristics with minor redesigns. After these improvements have been made, this instrument will be a satisfactory monitor for this area.

From introduction: "Due to the hydrogen overvoltage at the surface of a mercury cathode, uranium solutions is hydrochloric acid may be reduced not only to the tetravalent state, but until considerable trivalent uranium is formed. Other metallic ions act as oxidation-reduction catalysts as well as being reduced themselves. The following paper is a study of the various reactions taking place in solution and at the surface of the cathode."

Abstract. A method for the preparation of beryllium oxide of high purity is presented. Beryllium basic acetate (BeO-3Be(C2H3O2)2) is prepared from the metal or a convenient salt, a chloroform solution of this material extracted with redistilled water, the dried basic acetate distilled in a quartz apparatus, and this purified material converted to the oxide by fuming down with sulfuric acid and igniting at 1000 degrees C. Impurities detectable spectrographically were reduced to a very low level.

The following report discusses findings resulting from experiments on recycled carbon tetrachloride at various stages of the proposed purification process.