The large aqueous pilot plant facilities at ORNL were cleaned and are being put in standby condition. Experience was gained during the year as anion exchange was used to recover more than one kg of plutonium left in the exploded evaporator system. This experience is being applied to a new recovery program just beginning in cell 1 of Building 4507. (auth)

Hydraulic tests were made on the Hallam Prototype Free-Surface Sodium Pump to determine the net positive suction head (NPSH) required at various sodium flow rates. Pump performance data were also collected. The results indicate that an NPSH of 22 ft sodium is required at the design flow rate of 7200 gpm at approximates 1000 deg F, agreeing with computed values, and that the pump is designed with a safety margin of slightly over l0%. (D.L.C.)

S>The compatibility of type 304L stainless steel in intimate contact with graphite is being studied as a function of temperature and contact pressure. This study is an outgrowth of materials compatibility problems in present and advanced gas-cooled reactors, where structural members in direct contact with graphite provide the possibility of both carburization and self-welding. Initial studies were concerned with surface reactions in the absence of gaseous contaminants under a vacuum of 10/sup -6/ mm Hg at 540 to 705 deg C. Stainless steel specimens are pretreated to provide three surface conditions: H/sub 2/- fired, preoxidized, and Cu-plated. Surface contact pressures ranged from 0 to 10,000 psi. Test results are presented which establish the lower temperature limit for significant diffusion between graphite and stainless steel at approximately 60O deg C. Above this temperature, diffusion between untreated or H2-fired stainless steel surfaces was found to effect complete bonding of the two materials at contact pressures as low as 500 psi. Bonding was effectively prevented by the presence of either an oxide film or a Cu plate at temperatures up to 700 deg C. Where bonding occurred, diffusion rates measured for C in stainless steel were comparable with those reported for stainless steel …

The specification contains information concerning the material, process, and product requirements to be met by the fabricator. (J.R.D.)

Run 25 was the final period of power operational of the HRT. The reactor was operated for periods of 62, 8, 52, and 80 hours at 5 Mw with no outward indication of fuel and core and blanket average temperatures of 270 and 230 deg C, respectively. The uranium concentration in the was 1.7 to 2.0 g U/kg D/sub 2/O. Longer periods of operation were prevented by mechanical difficulties, notably with the fuel feed pump. While the reactor was subcritical after the last of the above runs, the upper patch in the core tank wall became dislodged, allowing greater core-to-blanket mixing. The resultant blanket uranium concentration was 2.9 g U/kg D/sub 2/O. The reactor was subsequently operated at April 28, 1961. The experiment was operated at high temperature for a total of 10,866 hours. The system was critical for a total of 8,841 hours and produced 16,295 Mwhours of power. The fuel, heavy water, and some corrosion specimens were recovered, and the reactor was stored in an assembled state. (auth)

A seven- to twenty-fold volume reduction can be obtained from fluidized bed calcination of aqueous aluminum nitrate wastes, depending on the operating conditions employed and their effect on the intra-panticle porosity and absolute density of the calcined alumina. Among the calcining variables, only the bed temperature and the fuel aluminum concentration had a significant effect on the intra-particle porosity of alumina generated during studies conducted primarily in a two-foot-square fluidized bed calciner. A quantitative correlation of the effect of these variables is presented. Alumina with an intra-particle porosity as low as five per cent can be generated by employing a suitable combination of low bed temperature and dilute aluminum feed concentration. Feed sodium concentration and product alpha alumina content were found to have minor effect on intra-particle porosity. Results also show that an inverse relationship exists between the nitrate content of the calcine and the calcination temperature. (auth)

A spectrographic method using d-c arc excitation in a controlled atmosphere was developed to analyze for seven impurity elements in radioactive hafnium samples. Analysis requires as little as 35 mg of hafnium oxide. (auth)

An addition is presented for the IBM-7090 program MURGATROYD to produce a rough graph of reactor power versus time. A sample of output is included for the case given as an example. (J.R.D.)

The effect of modifying the dislocation structure by room-temperature prestraining on the subsequent yielding behavior at 77 deg K is being studied. Results on tantalum single crystals indicated that a considerable decrease in the early yield stress for a given strain is effected by prestraining at room temperature. Twinning was observed in the tantalum at 77 deg K and normal rates of strain. It is shown that the potential barrler to dislocation motion in crystalline solids can be measured in relatively pure bcc transition metals such as Nb, Ta, Mo, and W. Work is being carried out to extend the method of differential calorimetry to measurements of stored-energy-release spectra in deformed bcc metals. Measurements for copper are discussed. (M.C.G.)

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Calculations are presented which show that the reactivity effect of flooding and unflooding the fast superheating section of the Mixed Spectrum Superheater can be made small by the addition of epithermal poisons to the superheater. The reactivity effects of flooding superheater sections ranging in size from 1.25 to 3.5 ft cubes and containing U/sup 23/5/sup >/oxide or Pu/sup 239/ oxide fuel and various amounts o f the epithermal poison europium were calculated. Reactivity changes during several postulated flooding processes are given. Methods for deterthination of fissile and fertile material and poison cross sections in the resonance- region are discussed. (auth)

Laboratory results are presented for a flowsheet study of a process for decontaminating ORNL low level waste water. The water is adjusted to approximately pH 12 with NaOH, clarified, and passed through a bed of phenolic cation exchange resin. This study, using a phenolic-carboxylic resin, showed essentially the same results as those previously reported using a phenolic-sulfonic resin, i.e., radioactivities in ORNL waste were reduced to the order of 10% of MPC. The phenolic-carboxylic resin has the advantage that it can be regenerated with 0.5 M HNO/sub 3/ instead of the 5 M HCl required for the phenolic-sulfonic resin. Volume reduction factors of 2000 to 3000 were achieved.

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Recently a T = 1 resonance in the {Lambda}{pi} system called Y*{sub 1} has been observed with a mass of 1385 Mev. Two types of resonances have been predicted that might relate this observation to other elementary-particle interactions: (1) P 3/2 resonances in the {Lambda}{pi} and {Sigma}{pi} systems predicted by global symmetry corresponding to the (3/2, 3/2) resonance of the {pi}N system; (2) a spin-1/2 Y-{pi} resonance resulting from a bound state in the KN system. The position and width of the observed Y*{sub 1} resonance agree with both theories, but since the spin and parity have not yet been determined, it is impossible at present to distinguish between the two theoretical interpretations.

It was the practice for several years to estimate the potential dose rate to the gastrointestinal from sanitary water sources by evaluating the results of radiochemical analysis of individual nuclides. The proposed method estimates the GI tract dose from Pasco and Richland domestic water from measurements of the total beta activity, and permits more frequent and more economical evaluation of a variable source of radiation exposure. Beginning with 1964 data, the GI tract dose rate for Richland and Pasco sanitary water has been obtained by multiplying the total beta count by a conversion factor derived from the historical relationship between the radiochemical analyses and the total beta counts. Either the accumulation of more data or changes in the relative abundance of the more significant nuclides in the water may result in changes in this factor.

Station 1A was the emplacement hole for the nuclear device used in the Advanced Research Project Agency's and U.S. Atomic Energy Commission's 5-kT nuclear Salmon Event of October 22, 1964. The hole penetrated the Pascagoula and Hattiesburg Formations, undifferentiated, and the Catahoula Sandstone, all of Miocene age, before entering the caprock at a depth of 882 feet. In continued through the calcite, gypsum, and anhydrite units of the caprock, which extend to a depth of 1,469.5 feet, and terminated in the salt stock at a depth of 2,802 feet. Five sand aquifer units lie above the caprock, whereas one sand aquifier lies within the calcite unit of the caprock. Drilling activities did not cause noticeable water-level fluctuations in the sand aquifers; however, during drilling in the calcite caprock, drilling fluid losses twice caused significant but temporary rises in water level in three observation wells that monitor the calcite limestone aquifer. The microscopic examination of drill cuttings collected at 10-foot intervals to a depth of 1,220 feet in Station 1A is presented. 2 figures, 1 table.

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This report gives the exposure data for the C Reactor at the Hanford Reservation February 1965.

During the 18-year history of Hanford operations, a high degree of safety has been provided at reasonable cost by the storage of high-activity liquid wastes in underground tanks, by the percolation of low-activity liquid wastes (principally water) through the soil to the ground water, and by the adsorption or filtration of radioactive materials from gaseous effluents prior to their discharge to the atmosphere. Studies of the Hanford area indicate that current practices could be continued almost indefinitely without jeopardizing environmental safety, provided the stored liquid wastes are periodically transferred to new tanks before the existing ones fail. In 1960, a Fission Product Recovery Program was prepared outlining a plan to meet the Atomic Energy Commission`s needs for isolated fission products. Emphasis was placed on developing processes for isolating selected fission products and on providing interim production capability for recovering the fission products of immediate interest. In 1961, development efforts were channeled almost exclusively toward meeting the immediate needs of the Commission for separated strontium-90 and cesium-137. During this time, it became increasingly evident that substantial economies could be realized, both in immediate development and subsequent operating efforts, if the separate fission product recovery and waste management programs were merged. The …

The information presented is a collection of most of the physics information available for the New Production Reactor. The details of some of the physics information, particularly those dealing with exposure and temperature effects, are by no means to be considered the final word since there has been no experimental verification of these effects. However, the gross physics characteristics described are felt to be reasonable representations of the expected physics behavior of N Reactor and should serve as useful guides throughout the startup planning and initial operation.

It is recommended that the ``square pile`` concept be adopted for all disaster total control calculations, and that the basic reactor constants listed in HW-62884, except for Ball 3X local strength at the DR Reactor, be used in applying this method. Curves are included for each reactor type, indicating allowable enrichment based on appropriate local control strengths. (The reactors whose operating methods are affected by disaster total control requirements are B, D, F, and DR Reactors; the remaining piles have sufficient geometrical coverage). An example of the analytical method is included.

Production Test IP-584-D, Supplement B authorized the irradiation of target assemblies in KER-1 and KER-2. Furthermore, the production test authorized that these target assemblies be irradiated with)other approved production tests; for this test, N Reactor inner fuel elements (NIE-1) will be irradiated. The production test required that specific operating conditions and loading patterns would be approved by the managers of Testing, Process and Reactor Development, and Process Technology Subsections prior to charging.

Reactor support charge designs and patterns have been numerous and varied over the past few years, the basis for acceptance of a particular support loading being determined from a consideration of fabrication costs and the hydraulic characteristics of the proposed dummy load as it applies to a particular reactor. Since the first three or four dummy pieces downstream of the fuel column (and upstream of the column in a spline tube) are discarded after the irradiation process, it is desirable to use tubular dummies for this portion of the support charge which are less expensive to fabricate and which are easily identified during the charging-discharging process. However, there exists a remote possibility that one or more tubular pieces could be inadvertently placed in a rear nozzle resulting in a flow restriction in the process tube. These arrangements of tubular support pieces in the dummy pattern, i.e., tubulars positioned against the fuel column and/or in the process tube rear nozzles, have been hydraulically tested to determine if there is adequate and unrestricted flow at normal operating header pressures.

The objective of this irradiation is to further verify the corrosion rate of tubular-type fuel elements under conditions of high specific power and central core temperatures. This fuel will be the inner tube only of an NPR fuel assembly. As in previous tests, this inner tube rupture will be used to further substantiate the rupture detection instrumentation that is being used in the development of the NPR. Previously unirradiated fuel will be used in this test. The reactor is to operate at full power during the test. Permission is requested for charging two tubular elements The top element will have attached to it a hydraulic mechanism for opening a defect in the outer surface of the tube. The second or bottom element, will be used as a heater element to maintain loop temperature.