Quantitative Microanalysis with high Spatial Resolution: Application of FEG-DTEM XEDS Microanalysis to the Characterization of Complex Microstructures in Irradiated Low Alloy Steet (open access)

Quantitative Microanalysis with high Spatial Resolution: Application of FEG-DTEM XEDS Microanalysis to the Characterization of Complex Microstructures in Irradiated Low Alloy Steet

To assist in the characterization of microstructural changes associated with irradiation damage in low alloy steels, the technique of quantitative x-ray mapping using a field emission gun scanning transmission electron microscope (FEG-STEM) equipped with an x-ray energy Dispersive spectrometer (XEDS) has been employed. Quantitative XEDS microanalyses of the matrix and grain boundaries of irradiated specimens have been compared with previous quantitative analyses obtained using 3D-Atom Probe Field-Ion Microscopy (3D-APFIM). In addition, the FEG-STEM XEDS maps obtained from the irradiated steel have revealed the presence of 2 to 3 nm Ni-enriched 'precipitates' in the matrix, which had previously been detected using 3D-APFIM. These quantitative FEG-STEM XEDS results represent the first direct and independent microchemical corroboration of the 3D-APFIM results showing ultra-fine irradiation-induced hardening features in low alloy steel.
Date: November 14, 2001
Creator: Williams, D.B., Watanabe, M. and Burke, M.G.
Object Type: Report
System: The UNT Digital Library
RSP Tooling Technology (open access)

RSP Tooling Technology

RSP Tooling{trademark} is a spray forming technology tailored for producing molds and dies. The approach combines rapid solidification processing and net-shape materials processing in a single step. The general concept involves converting a mold design described by a CAD file to a tooling master using a suitable rapid prototyping (RP) technology such as stereolithography. A pattern transfer is made to a castable ceramic, typically alumina or fused silica (Figure 1). This is followed by spray forming a thick deposit of a tooling alloy on the pattern to capture the desired shape, surface texture, and detail. The resultant metal block is cooled to room temperature and separated from the pattern. The deposit's exterior walls are machined square, allowing it to be used as an insert in a standard mold base. The overall turnaround time for tooling is about 3 to 5 days, starting with a master. Molds and dies produced in this way have been used in high volume production runs in plastic injection molding and die casting. A Cooperative Research and Development Agreement (CRADA) between the Idaho National Engineering and Environmental Laboratory (INEEL) and Grupo Vitro has been established to evaluate the feasibility of using RSP Tooling technology for producing …
Date: November 20, 2001
Creator: unknown
Object Type: Report
System: The UNT Digital Library
Design of an RF Antenna for a Large0Bore, High Power, Steady State Plasma Processing Chamber for Material Separation (open access)

Design of an RF Antenna for a Large0Bore, High Power, Steady State Plasma Processing Chamber for Material Separation

The purpose of this Cooperative Research and Development Agreement (CRADA) between UT-Battelle, LLC, (Contractor), and Archimedes Technology Group, (Participant) is to evaluate the design of an RF antenna for a large-bore, high power, steady state plasma processing chamber for material separation. Criteria for optimization will be to maximize the power deposition in the plasma while operating at acceptable voltages and currents in the antenna structure. The project objectives are to evaluate the design of an RF antenna for a large-bore, high power, steady state plasma processing chamber for material separation. Criteria for optimization will be to maximize the power deposition in the plasma while operating at acceptable voltages and currents in the antenna structure.
Date: November 7, 2001
Creator: Rasmussen, D.A. & Freeman, R.L.
Object Type: Report
System: The UNT Digital Library
Field Investigation to Determine the Extent of Sediment Recontamination at the United Heckathorn Superfund Site, Richmond, California (open access)

Field Investigation to Determine the Extent of Sediment Recontamination at the United Heckathorn Superfund Site, Richmond, California

This field investigation was undertaken to determine the present condition of sediment in Lauritzen Channel and Parr Canal approximately 2 years after completion of sediment remedial actions at the United Heckathorn Superfund site. The study was designed to supplement the post-remediation monitoring program by determining the extent and identifying potential sources of observed pesticide contamination in marine sediments near the site. Core samples collected from Lauritzen Channel and Parr Canal in July 1999 were described geologically, and samples were prepared from different sediment types, such as younger bay mud or older bay mud. Sediment samples were analyzed for grain size, organic carbon, and DDT compounds. Only minor changes have occurred in Parr Canal since remedial actions were taken in 1996-1997, but in Lauritzen Channel, DDT concentrations exceed the remedial goal of 590 ug/kg dry weight in nearly all the unconsolidated sediment (younger bay mud, sand, and disturbed older bay mud). The source of contaminated sediment could not be confirmed by this study; there was no clear correlation between high DDT concentrations and sediment remaining between the pilings, as was originally suspected. There also was no correlation between high DDT concentrations in sediment and the locations of outfalls, although some of …
Date: November 16, 2001
Creator: Kohn, Nancy P. & Gilmore, Tyler J.
Object Type: Report
System: The UNT Digital Library
A Dictionary for Transparency (open access)

A Dictionary for Transparency

There are many terms that are used in association with the U.S. Defense Threat Reduction Agency (DTRA) Transparency Project associated with the Mayak Fissile Materials Storage Facility. This is a collection of proposed definitions of these terms.
Date: November 15, 2001
Creator: Kouzes, Richard T.
Object Type: Report
System: The UNT Digital Library
Federal Agency Site-Level Energy Data (open access)

Federal Agency Site-Level Energy Data

This document provides information that will be useful to FEMP in targeting and identifying Federal sites for energy efficiency project potential. The document consolidates Federal energy data into a single source reference from which FEMP can work to more efficiently target opportunities.
Date: November 30, 2001
Creator: McMordie-Stoughton, Katherine L. & Koehler, Theresa M.
Object Type: Report
System: The UNT Digital Library
Highlighting High Performance: Four Times Square (open access)

Highlighting High Performance: Four Times Square

4 Times Square is a 48-story environmentally responsible building in New York City. Developed by the Durst Organization, the building is the first project of its size to adopt standards for energy efficiency, indoor ecology, sustainable materials, and responsible construction, operations, and maintenance procedures. Designers used a whole-building approach--considering how the building's systems can work together most efficiently--and educated tenants on the benefits of the design.
Date: November 1, 2001
Creator: unknown
Object Type: Text
System: The UNT Digital Library
RPM-SIM-Based Analysis of Power Converter Applications in Renewable Energy Systems: Preprint (open access)

RPM-SIM-Based Analysis of Power Converter Applications in Renewable Energy Systems: Preprint

This paper briefly presents the RPM-SIM simulator and, in particular, its abilities to simulate and analyze renewable energy systems with power converters. This modular simulation system is used to study applications and cost-effective performance of renewable energy systems, analyze both static and dynamic performance, develop control strategies, and simulate autonomous renewable energy systems under different generation and load conditions (such as different wind speeds, temperature, insolation conditions, and load profiles).
Date: November 1, 2001
Creator: Bialasiewicz, J. T.; Muljadi, E. & Nix, R. G.
Object Type: Article
System: The UNT Digital Library
Science & Technology Review November 2001 (open access)

Science & Technology Review November 2001

None
Date: November 1, 2001
Creator: Quong, A
Object Type: Report
System: The UNT Digital Library
International Workshop of the Physics of Compressible Turbulent Mixing (open access)

International Workshop of the Physics of Compressible Turbulent Mixing

None
Date: November 28, 2001
Creator: Schilling, O
Object Type: Report
System: The UNT Digital Library
Status and Recent Results for EMSP Project No.70108 Effects of Fluid Distribution on Measured Geophysical Properties for Partially Saturated, Shallow Subsurface Conditions (open access)

Status and Recent Results for EMSP Project No.70108 Effects of Fluid Distribution on Measured Geophysical Properties for Partially Saturated, Shallow Subsurface Conditions

The objective of this report is to improve geophysical imaging of the vadose zone by developing improved methods for interpreting geophysical field data. The purpose of this EMSP project is to develop relationships between laboratory measured geophysical properties and porosity, saturation, soil composition, and fluid distribution, for partially saturated soils. Algorithms for relationships between soil composition, fluids, and geophysical measurements can provide new methods to interpret geophysical field data collected in the vadose zone at sites such as Hanford, WA.
Date: November 1, 2001
Creator: Berge, P. A.; Bonner, B. P.; Roberts, J. J.; Wildenschild, D.; Berryman, J. G. & Bertete-Aquirre, H.
Object Type: Article
System: The UNT Digital Library
State Renewable Energy News -- Vol. 10, No. 3, Fall 2001 (Newsletter) (open access)

State Renewable Energy News -- Vol. 10, No. 3, Fall 2001 (Newsletter)

This newsletter is prepared for the NARUC Renewable and Distributed Resources Subcommittee to promote information sharing on state-level renewable electric activities. It is sponsored by the Office of Power Technologies of the U.S. Department of Energy.
Date: November 1, 2001
Creator: unknown
Object Type: Journal/Magazine/Newsletter
System: The UNT Digital Library
Progress in Infrared Pyrometry Measurements of Shocked Solids (open access)

Progress in Infrared Pyrometry Measurements of Shocked Solids

Temperature measurement is one of the grand challenges still facing experimental shock physics. A shock experiment fundamentally measures E({sigma}{sub x}, {var_epsilon}{sub 11}) which is an incomplete equation of state since temperature (or entropy) remains unspecified. Ideally, one would like to experimentally determine a free energy F(T, {var_epsilon}{sub ij}) from which all other thermo-mechanical properties might be derived. In practice, temperature measurement would allow direct comparison with theory/simulation since T and {var_epsilon}{sub 11} are in most theories the underlying variables. Temperature is a sensitive measure of energy partitioning, knowledge of which would increase our understanding phase boundaries and thermally activated processes (such as chemical reactivity (including dissociation and ionization)). Temperature measurement would also allow a thermodynamically consistent coupling of hydrodynamic equations of state to the material's constitutive (deformation) behavior. The measurement of the temperature of a material that has undergone severe strains at small time-scales is extremely difficult, and we are developing a method using infrared reflectance and pyrometry. The emitted power from a warm surface is measured over a range of wavelengths using a multi-channel IR detector with a response time of {approx}0.1 {micro}s. Each channel of the detector passes the radiation from a selected wavelength interval into a detector. …
Date: November 5, 2001
Creator: Cazamias, J U; Hare, D E & Poulsen, P
Object Type: Article
System: The UNT Digital Library
Factors Affecting the Fuel Consumption of Plug-In Hybrid Electric Vehicles (open access)

Factors Affecting the Fuel Consumption of Plug-In Hybrid Electric Vehicles

Primary Factors that Impact the Fuel Consumption of Plug-In Hybrid Electric Vehicles RICHARD ‘BARNEY’ CARLSON, MATTHEW G. SHIRK Idaho National Laboratory 2525 N. Fremont Ave., Idaho Falls, ID 83415, USA richard.carlson@inl.gov Abstract Plug-in Hybrid Electric Vehicles (PHEV) have proven to significantly reduce petroleum consumption as compared to conventional internal combustion engine vehicles (ICE) by utilizing electrical energy for propulsion. Through extensive testing of PHEV’s, analysis has shown that the fuel consumption of PHEV’s is more significantly affected than conventional vehicles by either the driver’s input or by the environmental inputs around the vehicle. Six primary factors have been identified that significantly affect the fuel consumption of PHEV’s. In this paper, these primary factors are analyzed from on-road driving and charging data from over 200 PHEV’s throughout North America that include Hymotion Prius conversions and Hybrids Plus Escape conversions. The Idaho National Laboratory (INL) tests plug-in hybrid electric (PHEV) vehicles as part of its conduct of DOE’s Advanced Vehicle Testing Activity (AVTA). In collaboration with its 75 testing partners located in 23 states and Canada, INL has collected data on 191 PHEVs, comprised of 12 different PHEV models (by battery manufacturer). With more than 1 million PHEV test miles accumulated to …
Date: November 1, 2001
Creator: Carlson, Richard "Barney"; Shirk, Matthew G. & Geller, Benjamin M.
Object Type: Article
System: The UNT Digital Library
CHANGES IN MOISTURE, CARBON, NITROGEN, SULPHUR, VOLATILES, AND CALORIFIC VALUE OF MISCANTHUS DURING TORREFACTION (open access)

CHANGES IN MOISTURE, CARBON, NITROGEN, SULPHUR, VOLATILES, AND CALORIFIC VALUE OF MISCANTHUS DURING TORREFACTION

Torrefaction tests were carried out on miscanthus samples in order to understand the changes in chemical composition at temperatures of 250–350°C and residence times of 30–120 minutes. The raw material chemical composition was moisture content 7.97%, moisture-free carbon (C) 47.73%, hydrogen (H) 5.85%, nitrogen (N) 0.28%, sulphur (S) 0.02%, volatiles (V) 83.29% for volatiles, and moisture and ash-free (MAF) calorific value (CV) 8423 BTU/lb (19.59 MJ/kg). Torrefaction at temperatures of 250°C and residence time of 30 minutes resulted in a significant decrease in moisture by about 82.68%, but the other components, C, H, N, S, and V changed only marginally. Increasing the torrefaction temperature to 350°C and residence time to 120 minutes further reduced the moisture to a final value of 0.54% (a 93.2% reduction compared to original) and also resulted in a significant decrease in the other components, H, N, and V by 58.29%, 14.28%, and 70.45%, respectively. The carbon content at 350°C and 120 minutes increased by about 4% and sulfur values were below detection limits. The calorific values increased by about 5.59% at 250°C and 30 minutes, whereas at 350°C and 120 minutes, the increase was much greater (about 75.61%) and resulted in a maximum degree of …
Date: November 1, 2001
Creator: Tumuluru, Jaya Shankar; Boardman, Richard; Wright, Christopher & Heintzelman, John
Object Type: Article
System: The UNT Digital Library
Review of Methods Related to Assessing Human Performance in Nuclear Power Plant Control Room Simulations (open access)

Review of Methods Related to Assessing Human Performance in Nuclear Power Plant Control Room Simulations

With the increased use of digital systems in Nuclear Power Plant (NPP) control rooms comes a need to thoroughly understand the human performance issues associated with digital systems. A common way to evaluate human performance is to test operators and crews in NPP control room simulators. However, it is often challenging to characterize human performance in meaningful ways when measuring performance in NPP control room simulations. A review of the literature in NPP simulator studies reveals a variety of ways to measure human performance in NPP control room simulations including direct observation, automated computer logging, recordings from physiological equipment, self-report techniques, protocol analysis and structured debriefs, and application of model-based evaluation. These methods and the particular measures used are summarized and evaluated.
Date: November 1, 2001
Creator: Blanc, Katya L Le; Boring, Ronald L & Gertman, David I
Object Type: Article
System: The UNT Digital Library
Hot Wire Needle Probe for In-Pile Thermal Conductivity Detection (open access)

Hot Wire Needle Probe for In-Pile Thermal Conductivity Detection

Thermal conductivity is a key property of interest for both nuclear fuel and structural materials, and must be known for proper design, test, and application of new fuels and structural materials in nuclear reactors. Thermal conductivity is highly dependent on the physical structure, chemical composition, and the state of the material. Typically, thermal conductivity changes that occur during irradiation are measured out-of-pile by Post Irradiated Examination (PIE) using a “cook and look” approach in hot-cells. Repeatedly removing samples from a test reactor to make out-of-pile measurements is expensive, has the potential to disturb phenomena of interest, and only provides understanding of the sample's end state at the time each measurement is made. There are also limited thermophysical property data for advanced fuels. Such data are needed for simulation design codes, the development of next generation reactors, and advanced fuels for existing nuclear plants. Being able to quickly characterize fuel thermal conductivity during irradiation can improve the fidelity of data, reduce costs of post-irradiation examinations, increase understanding of how fuels behave under irradiation, and confirm or improve existing thermal conductivity measurement techniques. This paper discusses advancements from Idaho National Laboratory (INL) / Utah State University (USU) examinations, including background information, governing …
Date: November 1, 2001
Creator: Daw, Joshua; Rempe, Joy; Condie, Keith; Knudson, Darrell; Wilkins, S. Curtis; Fox, Brandon S. et al.
Object Type: Article
System: The UNT Digital Library
Vadose Zone Transport Field Study: Status Report (open access)

Vadose Zone Transport Field Study: Status Report

Studies were initiated at the Hanford Site to evaluate the process controlling the transport of fluids in the vadose zone and to develop a reliable database upon which vadose-zone transport models can be calibrated. These models are needed to evaluate contaminant migration through the vadose zone to underlying groundwaters at Hanford. A study site that had previously been extensively characterized using geophysical monitoring techniques was selected in the 200 E Area. Techniques used previously included neutron probe for water content, spectral gamma logging for radionuclide tracers, and gamma scattering for wet bulk density. Building on the characterization efforts of the past 20 years, the site was instrumented to facilitate the comparison of nine vadose-zone characterization methods: advanced tensiometers, neutron probe, electrical resistance tomography (ERT), high-resolution resistivity (HRR), electromagnetic induction imaging (EMI), cross-borehole radar (XBR), and cross-borehole seismic (XBS). Soil coring was used to obtain soil samples for analyzing ionic and isotopic tracers.
Date: November 30, 2001
Creator: Gee, Glendon W. & Ward, Anderson L.
Object Type: Report
System: The UNT Digital Library
The Status of Radiation Damage Experiments (open access)

The Status of Radiation Damage Experiments

Experiments have been on-going for about two years to determine the effects that radiation damage have on the physical and chemical properties of candidate titanate ceramics for the immobilization of plutonium. We summarize the results of these experiments in this document.
Date: November 20, 2001
Creator: Strachan, Denis M.; Scheele, Randall D.; Icenhower, Jonathan P.; Kozelisky, Anne E.; Sell, Richard L.; Legore, Virginia L. et al.
Object Type: Report
System: The UNT Digital Library
Selection of Sampling Pumps Used for Groundwater Monitoring at the Hanford Site (open access)

Selection of Sampling Pumps Used for Groundwater Monitoring at the Hanford Site

The variable frequency drive centrifugal submersible pump, Redi-Flo2a made by Grundfosa, was selected for universal application for Hanford Site groundwater monitoring. Specifications for the selected pump and five other pumps were evaluated against current and future Hanford groundwater monitoring performance requirements, and the Redi-Flo2 was selected as the most versatile and applicable for the range of monitoring conditions. The Redi-Flo2 pump distinguished itself from the other pumps considered because of its wide range in output flow rate and its comparatively moderate maintenance and low capital costs. The Redi-Flo2 pump is able to purge a well at a high flow rate and then supply water for sampling at a low flow rate. Groundwater sampling using a low-volume-purging technique (e.g., low flow, minimal purge, no purge, or micropurgea) is planned in the future, eliminating the need for the pump to supply a high-output flow rate. Under those conditions, the Well Wizard bladder pump, manufactured by QED Environmental Systems, Inc., may be the preferred pump because of the lower capital cost.
Date: November 5, 2001
Creator: Schalla, Ronald; Webber, William D. & Smith, Ronald M.
Object Type: Report
System: The UNT Digital Library
Evaluation of Effect of Fuel Assembly Loading Patterns on Thermal and Shielding Performance of a Spent Fuel Storage/Transportation Cask (open access)

Evaluation of Effect of Fuel Assembly Loading Patterns on Thermal and Shielding Performance of a Spent Fuel Storage/Transportation Cask

The licensing of spent fuel storage casks is generally based on conservative analyses that assume a storage system being uniformly loaded with design basis fuel. The design basis fuel typically assumes a maximum assembly enrichment, maximum burn up, and minimum cooling time. These conditions set the maximum decay heat loads and radioactive source terms for the design. Recognizing that reactor spent fuel pools hold spent fuel with an array of initial enrichments, burners, and cooling times, this study was performed to evaluate the effect of load pattern on peak cladding temperature and cask surface dose rate. Based on the analysis, the authors concluded that load patterns could be used to reduce peak cladding temperatures in a cask without adversely impacting the surface dose rates.
Date: November 20, 2001
Creator: Cuta, Judith M.; Jenquin, Urban P. & McKinnon, Mikal A.
Object Type: Report
System: The UNT Digital Library
Annual Hanford Seismic Report For Fiscal Year 2001 (open access)

Annual Hanford Seismic Report For Fiscal Year 2001

This report summarizes the earthquake activity on the Hanford Site for the Fiscal year 2001
Date: November 30, 2001
Creator: Hartshorn, Donald C.; Reidel, Stephen P.; Rohay, Alan C. & Valenta, Michelle M.
Object Type: Report
System: The UNT Digital Library
Total Sky Imager Model 880 Status and Testing Results (open access)

Total Sky Imager Model 880 Status and Testing Results

The Total Sky Imager (TSI) is manufactured by Yankee Environmental Systems (YES) Incorporated, based in Turner Falls, Massachusetts. (For more information about YES, see http://www.yesinc.com/.) The TSI is a commercialized version of the Hemispheric Sky Imager prototype (Long et al. 1998). YES has now produced a more sophisticated (compared to the original model 440) model 880 of the TSI (see Figure 1). The first YES TSI 880 was deployed at the Blackwell Tonkawa Airport (BTA) as part of the Department of Energy (DOE) Atmospheric Radiation Measurement (ARM) Program 2000 Cloud intensive operational period (IOP). This TSI 880 collected data from March 2, 2000 through April 6, 2000. This report gives an assessment of the TSI based on the BTA and Southern Great Plane (SGP) Central Facility (CF) data collected to date.
Date: November 1, 2001
Creator: Long, CN; Slater, DW & Tooman, T
Object Type: Report
System: The UNT Digital Library