Processing and mechanical properties of silicon nitride formed by robocasting aqueous slurries (open access)

Processing and mechanical properties of silicon nitride formed by robocasting aqueous slurries

Robocasting is a new freeform fabrication technique for dense ceramics. It uses robotics to control deposition of ceramic slurries through an orifice. The optimization of concentrated aqueous Si{sub 3}N{sub 4} slurry properties to achieve high green density robocast bodies and subsequent high sintered densities was investigated. The effects of pH, electrolyte, additives and solids loading on the dispersion and rheological properties of Si{sub 3}N{sub 4} slurries were determined. The mechanical behavior of sintered robocast bars was determined and compared to conventionally produced silicon nitride ceramics.
Date: January 26, 2000
Creator: He, Guoping; Hirschfeld, Deidre A. & Cesarano, Joseph, III
System: The UNT Digital Library
The ''Radiation continuity Checker'', an Instrument for Monitoring Nuclear Disarmament Treaty Compliance (open access)

The ''Radiation continuity Checker'', an Instrument for Monitoring Nuclear Disarmament Treaty Compliance

We describe the design, construction and performance of an instrument designed to monitor compliance with future arms control treaties. By monitoring changes in the gamma-ray spectrum emitted by a stored nuclear weapon, our device is able to sense perturbations in the contents of a weapon storage container that would indicate treaty non-compliance. Our instrument (dubbed the Radiation Continuity Checker or RCC) is designed to detect significant perturbations in the gamma-ray spectra (indicative of tampering) while storing no classified information about the weapon, and having a negligible ''false alarm rate''. In this paper we describe the technical details of two prototype instruments and describe the strategies we have adopted to perform signal processing in these instruments. Our first instrument prototype uses a scintillation spectrometer and a massive tungsten alloy collimator to reject the gamma-ray background. Our second prototype instrument makes use of an active collimation scheme employing a multiple detector Compton scatter approach to reject background radiation. The signal processing method we employ uses linear algorithms applied pulse by pulse. This eliminates the need for storage of pulse height spectra, which are in many cases classified.
Date: October 1, 2000
Creator: Bernstein, A.; Brunett, B. A.; Hilton, N. R.; Lund, J. C. & van Scyoc, J. M.
System: The UNT Digital Library
Mechanical properties and shear failure surfaces of two alumina powders in triaxial compression (open access)

Mechanical properties and shear failure surfaces of two alumina powders in triaxial compression

In the manufacture of ceramic components, near-net-shape parts are commonly formed by uniaxially pressing granulated powders in rigid dies. Density gradients that are introduced into a powder compact during press-forming often increase the cost of manufacturing, and can degrade the performance and reliability of the finished part. Finite element method (FEM) modeling can be used to predict powder compaction response, and can provide insight into the causes of density gradients in green powder compacts; however, accurate numerical simulations require accurate material properties and realistic constitutive laws. To support an effort to implement an advanced cap plasticity model within the finite element framework to realistically simulate powder compaction, the authors have undertaken a project to directly measure as many of the requisite powder properties for modeling as possible. A soil mechanics approach has been refined and used to measure the pressure dependent properties of ceramic powders up to 68.9 MPa (10,000 psi). Due to the large strains associated with compacting low bulk density ceramic powders, a two-stage process was developed to accurately determine the pressure-density relationship of a ceramic powder in hydrostatic compression, and the properties of that same powder compact under deviatoric loading at the same specific pressures. Using this …
Date: April 24, 2000
Creator: Zeuch, David H.; Grazier, J. Mark; Arguello, Jose G., Jr. & Ewsuk, Kevin G.
System: The UNT Digital Library
Near Infrared (NIR) Imaging Techniques Using Lasers and Nonlinear Crystal Optical Parametric Oscillator/Amplifier (OPO/OPA) Imaging and Transferred Electron (TE) Photocathode Image Intensifiers (open access)

Near Infrared (NIR) Imaging Techniques Using Lasers and Nonlinear Crystal Optical Parametric Oscillator/Amplifier (OPO/OPA) Imaging and Transferred Electron (TE) Photocathode Image Intensifiers

Laboratory experiments utilizing different near-infrared (NIR) sensitive imaging techniques for LADAR range gated imaging at eye-safe wavelengths are presented. An OPO/OPA configuration incorporating a nonlinear crystal for wavelength conversion of 1.56 micron probe or broadcast laser light to 807 nm light by utilizing a second pump laser at 532 nm for gating and gain, was evaluated for sensitivity, resolution, and general image quality. These data are presented with similar test results obtained from an image intensifier based upon a transferred electron (TE) photocathode with high quantum efficiency (QE) in the 1-2 micron range, with a P-20 phosphor output screen. Data presented include range-gated imaging performance in a cloud chamber with varying optical attenuation of laser reflectance images.
Date: December 20, 2000
Creator: Yates, George J.; Mcdonald, Thomas E., Jr.; Bliss, David E.; Cameron, Stewart M.; Greives, Kenneth H. & Zutavern, Fred J.
System: The UNT Digital Library
Range-Gated LADAR Coherent Imaging Using Parametric Up-Conversion of IR and NIR Light for Imaging with a Visible-Range Fast-Shuttered Intensified Digital CCD Camera (open access)

Range-Gated LADAR Coherent Imaging Using Parametric Up-Conversion of IR and NIR Light for Imaging with a Visible-Range Fast-Shuttered Intensified Digital CCD Camera

Research is presented on infrared (IR) and near infrared (NIR) sensitive sensor technologies for use in a high speed shuttered/intensified digital video camera system for range-gated imaging at ''eye-safe'' wavelengths in the region of 1.5 microns. The study is based upon nonlinear crystals used for second harmonic generation (SHG) in optical parametric oscillators (OPOS) for conversion of NIR and IR laser light to visible range light for detection with generic S-20 photocathodes. The intensifiers are ''stripline'' geometry 18-mm diameter microchannel plate intensifiers (MCPIIS), designed by Los Alamos National Laboratory and manufactured by Philips Photonics. The MCPIIS are designed for fast optical shattering with exposures in the 100-200 ps range, and are coupled to a fast readout CCD camera. Conversion efficiency and resolution for the wavelength conversion process are reported. Experimental set-ups for the wavelength shifting and the optical configurations for producing and transporting laser reflectance images are discussed.
Date: December 20, 2000
Creator: Yates, George J.; Mcdonald, Thomas E., Jr.; Bliss, David E.; Cameron, Stewart M. & Zutavern, Fred J.
System: The UNT Digital Library
The Impact of Emerging MEMS-Based Microsystems on US Defense Applications (open access)

The Impact of Emerging MEMS-Based Microsystems on US Defense Applications

This paper examines the impact of inserting Micro-Electro-Mechanical Systems (MEMS) into US defense applications. As specific examples, the impacts of micro Inertial Measurement Units (IMUs), radio frequency MEMS (RF MEMS), and Micro-Opto-Electro-Mechanical Systems (MOEMS) to provide integrated intelligence, communication, and control to the defense infrastructure with increased affordability, functionality, and performance are highlighted.
Date: January 20, 2000
Creator: Staple, Bevan D. & Jakubczak, Jerome F., II
System: The UNT Digital Library