Quarterly report discussing fuel cell research and development work at Argonne National Laboratory (ANL). These efforts have been directed toward seeking alternative cathode materials to NiO for molten carbonate fuel cells. Particular emphasis has been placed on studying the relationship between synthesis conditions and the resistivity of doped and undoped LiFeO2 and Li2 MnO3 and on achieving a better understanding of the crystalline defect structures of the thermodynamically stable phases.