The addition of a surface active agent to an aqeous-organic interface produced a resistance to mass transfer equivalent to slightly more than 1 cm of water. Five semicontinuous Druhm runs were made with 1/2in. thick MgO liners and terminated due to either failures of the UFe nozzle or a top gasket leak. In preliminary scale-up tests of the flame calcination equipment, a maximum feed rate equivalent to 720 g oxides/hr was achieved using a 3-in. i.d. magnesia reflector with an outside wall temperature of 1500°C.

Uranium extractions from carbonate solutions were effective and phase separation rates were rapid using a new commercial quaternary extractant, Alamine 336. Extraction coefficients were approximately proportional to the quaternary concentration. Addition of -0.5 mole tridecanol/mole quaternary to the solvent gave optimum extraction efficiency and phase separation rates.