Report issued by the Oak Ridge National Laboratory discussing quarterly progress made by the Homogeneous Reactor Program. Descriptions of progress and studies conducted are presented. This report includes tables, illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing quarterly progress of the Homogeneous Reactor Project. Progress of operations, design, development, and analysis is presented. This report includes tables, illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing quarterly progress of the Homogeneous Reactor Project. Progress of operations, design, development, and analysis is presented. This report includes tables, illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing quarterly progress made by the Homogeneous Reactor Program. Descriptions of progress and studies conducted are presented. This report includes tables, illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing semiannual progress made by the Instrumentation and Controls Division. Descriptions of progress and studies conducted are presented. This report includes illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing semiannual progress made by the Physics Division. Descriptions of progress and studies conducted are presented. This report includes tables, and illustrations.

Report issued by the Oak Ridge National Laboratory discussing annual progress made by the Solid State Division. Work and research progress made during 1957 is presented. This report includes tables, illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing progress made by the Stable Isotopes Division. Descriptions of of the progress and studies made are presented. This report includes tables, illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing the vibrational analysis of the molecular spectrum of polonium. Experimental procedures, results, and analysis are presented. This report includes tables, illustrations, and photographs.

Report issued by the Oak Ridge National Laboratory discussing the Research Reactor (ORR). General descriptions of the ORR are presented. This report includes tables, and illustrations.

Report issued by the Oak Ridge National Laboratory discussing the aging characteristics of the alloy Hastelloy B. Materials, equipment, experimental procedures, and results used to determine the characteristics of the alloy are presented. This report includes tables, illustrations, and photographs.

From abstract: "On the 86-inch cyclotron a 41-kw beam has been calorimetered at a net ion loading efficiency of 40%; the average proton current was 1.85 ma at 22.5 Mev. Practical specific yields have been determined for (p,2n) reactions on zinc and bismuth. The investigation of products of proton-induced fission of uranium has been continued and new techniques are being used in measuring angular distribution of reaction products. The 63-inch heavy particle cyclotron is now in operation; N+++ particles have been accelerated to ~25 Mev. In preliminary tests, induced activities have been detected in carbon, nitrogen, and oxygen targets. A hot-cathode ion source is ready for test operation. The 22-inch cyclotron is being used in an investigation of the problems associated with the use of rf and dc electrodes for the acceleration of protons from the ion source into the dees. Radiation-induced corrosion in Inconel tubing containing #21 eutectic (ANP) has been produced by proton irradiation in the 86-inch cylclotron; it is shown that the corrosion was not due to thermal effects. Approximately 150 grams of highly purified U 238 (< 5 ppm U 235) have been prepared, and two grams of thorium 230 (ionium) has been enriched to 90.6%."

An inconel loop circulating fluoride fuel (62 1/2 make [unintelligible] NaF, 12 1/2 make [unintelligible] ZrF4, 25 make [unintelligible] UF4, 92 [unintelligible] enriched) was operated at 1485°F with a temperature difference of about 35°F in the Low Intensity Test Reactor for 645 hr. For 475 hr of this time the reactor was at full power, and fission power generation in the loop was 2.7 kw, with a max length power density of 0.4 kw/cc. The total volume of fuel was 1290 cc (5.o kg [unintelligible] and the the flow through the irradiated section was 8.6 fps (Reynolds number 5500). The loop has been disassembled and has been examined by chemical and metallographic analyses. Ne acceleration of corrosion of decomposition of fuel by irradiation was noted, although deposition of fission-product ruthenium was absorbed. Ne mass transfer of Inconel was formed, and the corrosive [unintelligible] was general and relatively light. The average corrosive generation, in the usual form of subsurface yields, was 0.5 [unintelligible], the maximum penetration was 2 to 3 miles.

This report is the result of a study to develop heat-resistant fin materials possessing a high thermal conductivity for air radiators. Since an economical and commercially feasible product was desired, the investigation was restricted primarily to a study of electroplated copper, clad copper, and copper alloys. Sheet material 0.008 to 0.010 in. thick was evaluated for fabricability and for metallurgical stability and thermal conductivity at 1500°F. From the results of the rests it was concluded that: (1) electroplates were unsatisfactory; (2) clad-copper fins possessing a thermal conductivity of 50% of that of copper are commercially feasible; (3) copper-aluminum alloys possessing a thermal conductivity approaching that of copper at 1500°F are possible. Service tests of clad copper and the copper-aluminum alloys indicate that the choice of materials will be dictated by the requirements of the radiator, since each presents some unique problems.

Techniques are described for determining U-235 abundance by measurement of the intensity of 0.18 Mev gamma radiation. One method involves measurement of the ratio of the intensity of 0.18-Mev radiation to that of 0.1 Mev radiation. The preferred technique consists of chemical separation of uranium followed by direct counting of 0.18-Mev photons. Application has been made in analysis of uranium samples of abundances in the range of 0.05% to 93%. Accuracy appears to be better than 3% if the abundance is between 0.7% and 100%. Findings in the self-absorption of 0.18 Mev radiation in uranium oxide are presented.

This technical report is the second of a series which concerns the separation of ions by solvent extraction with trialkyl phosphine oxides (TOPO). This investigation has consisted in the extraction of various ions from acidic solutions with extractants that are representative of these ore specific phosphine oxides - triphenylphosphine oxide (THPO) and tris-2-ethylhexylphosihine oxides (TEHPO). In general it is observed that: (a) the order of increasing capacity of extraction is THPO > TOPO >TEHPO. (b) No ion is extracted by THPO or TEHPO that is not extracted by TOPO under certain conditions. (c) The effect of hydrogen ion concentration is greater in TEHPO systems than it is in the other two, which indicated greater selectivity of extraction with TEHPO.

Twenty-five hundred psi ring-type flanges, ring gaskets, bolts, and special connectors were tested for adaptability to the aqueous homogenous reactor. High pressure line closures were studied to obtain empirical data pertinent to the selection or design of a connector capable of withstanding sustained thermal cycling and high pressures encountered in the aqueous homogenous reactor. Specialized stress-strain measurement techniques yielded information concerning flange deformation, ring type gaskets, bolts, and special connectors. The results indicated that no totally acceptable connector is currently available. Most promising of the combination of components tested during this period was a 2500 psi ring type flange with an accurately machined octagonal gasket and Grade B-7 bolts.

Resistance of carbon steel to corrosion in oxygenated high-temperature (250C) water was unexpectedly good at high oxygen concentration. Pertinent literature, critically examined, and toroid experiments indicted that at low oxygen concentration attack did increase with concentration, but as oxygen concentration was sufficiently increased, more protective films were formed on the metal. Some corrosion factors in the application of carbon steel to nuclear reactors systems are discussed.

The HRT refrigeration system was designed to use Freon-11 (CCI3F) as the refrigerant material in the secondary loop. A Van de Graaff irradiation of this material indicated that serious corrosion problems were probable if Freon were used in the proposed metal system. A survey was made of candidate refrigerants, and Amsco 125-82 and triethyl phosphate were selected for irradiation and physical-property determinations.

In order to evaluate the behavior of an APPR type absorber rod, an irradiation test program has been established. Approximately 21 more samples are planned for testing under this request. The request proposes testing a full size APPR-1 type control rod in the MTR. The objective of the test is to better evaluate the neutron absorbing material proposed for the APPR-1 control rod.

A method was developed for calculating shield induced gamma radiation escaping through openings in a biological shield. The method was applied to the HRT and the results indicated that the contribution to the dose from induced activity in the HRT shield was around 0.1 r/hr and was insignificant in comparison to to other mechanisms contributing to the escape of gamma rays through shield openings.

A new type of continuous density meter, applicable for use with ThO2 slurry in high temperature-pressure systems, was tested successfully in a low temperature slurry loop.

The results of an examination of "O" ring gaskets remove from the HRT following a discovery that the water in the leak detector system contained 1000 ppm chloride are presented.

A six-inch diameter "O" ring from the HRT Mockup was examined metallographically after 2452 hours exposure to uranyl sulfate solution at 300C. surface defects, except for cold work defects were found only in areas exposed to uranyl sulfates. Defects found were pits, transgranular cracks, surface cracks, and grain attacks.