Purpose: "The Hanford Works Analytical Manual for Process Water is designed to specify the analytical methods to be applied for control purposes in the Reactor Section, Process Sub-Section laboratories. The procedures are in general form and serve as references rather than outlined laboratory instructions. The manual us designed to replace the "Hanford Works Manual," HW-12862."

Report discussing the distribution of mass in the spontaneous fission of Cm²⁴², which was investigated by a radiochemical determination of the fission yields of twenty-one nuclides ranging in mass from 91 to 140. "Corrections for absorption, scattering, geometry, decay, and fractional saturation were applied to obtain saturation disintegration rates, which, with the known fission rate of the source, give the fission yields."

Gamma plutonium is found to be orthorhombic with eight atoms in a unit cell of dimension (1t 235 degree C) [formula]. The calculated density is [formula]. The space group is Fddd and the positions of the eight atoms are: [formula]. Each plutonium atom is bonded to ten others at an aver distance of [formula], four being at [formula], two at [formula] and found at [formula]. The mean linear coefficients of thermal expansion are found to be [formula].

A method for monitoring radiation damage irradiations using the change of the electrical conductivity of graphite is described. Results of monitoring operations in a number of locations are given. An attempt is made to explain the damage rate found in the converter at CP-3. An estimate of the flux spectrum in VT-4 and the converter of CP-3 is made and the damage rate is computed according to theories of Seitz and James. It is found that the experimental results are more in accord with the predictions of Seitz. A number of corrections to James' report, ORNL-307, are noted in an appendix. It is shown that some information about the fast flux spectrum can be inferred from the radiation damage rate.

Experiments are described in which the pile-induced changes in electrical resistivity and elastic modulus of graphite were investigated as functions of the sample temperature during bombardment and the amount of bombardment. The data are for relatively low bombardment times (up to ca. 20 L-units) and temperatures (up to 340*C) and are not sufficiently extensive to permit unequivocal conclusions.

The following documents are quarterly progress reports recorded in the chemistry division of the University of California's radiation laboratory.

In the past year, exploratory data have been taken to determine the relative solubilities of hydrogen and deuterium in various solvents in the vicinity of room temperature and atmospheric pressure. This investigation is one phase of a program to determine the feasibility of separating deuterium from hydrogen by means of rectified absorption.