The Valve Actuated Pulse Column Design (open access)

The Valve Actuated Pulse Column Design

Abstract: "The valve-actuated pulse column is employed to give phase separation on each half cycle in the countercurrent flow cycle and provides independent control over each step in the cycle. The dependence on temperature of operation, on pulse frequency and amplitude, and on plate design and spacing has been studied for extraction and stripping of uranium with tributyl phosphate in a hydrocarbon diluent. It is found that the efficiency increases quite significantly as the temperature is raised regardless of the direction of transfer and this increased efficiency is accompanied by greater operational freedom. A decrease in hole size, decrease in plate separation and increase in frequency all lead to higher efficiency in agreement with the concept that small drops continually formed coalesced and reformed, lead to maximum interphase transfer. The high extraction efficiency of the column is probably aided further by the relatively sharp pulse produced."
Date: February 16, 1953
Creator: Burger, L. L. & Clark, L. H.
System: The UNT Digital Library
Production Test 235-5 Plant Process Evaluation Reduction of Plutonium Tetrafluoride With Calcium and Sulfur (open access)

Production Test 235-5 Plant Process Evaluation Reduction of Plutonium Tetrafluoride With Calcium and Sulfur

This report discusses the production of plutonium metal through the reduction of plutonium tetra fluoride with calcium metal and sulfur. It elaborates that iodine, which was originally used instead of calcium metal, presented several practical problems, but reductions completed with calcium were unsatisfactory.
Date: February 10, 1953
Creator: Kerr, W. B.
System: The UNT Digital Library
Reactivity Effects of Very Inhomogeneous Enriched Loadings (open access)

Reactivity Effects of Very Inhomogeneous Enriched Loadings

From abstract: "The reactivity effects of one and of two highly enriched fuel rods placed into a natural uranium lattice thermal pile are investigated according to the small source model."
Date: February 24, 1953
Creator: Neumann, H.
System: The UNT Digital Library
Preliminary Results of the Ratio of PU²³⁹ Fission Cross Section to U²³⁵ Fission Cross Section (open access)

Preliminary Results of the Ratio of PU²³⁹ Fission Cross Section to U²³⁵ Fission Cross Section

This report presents the final results from the investigation of the ratio of Pu-239 fission cross section to U-235 fission cross section. Three sets of plutonium and uranium foils were prepared at KAPL and were investigated to acquire the final results.
Date: February 20, 1953
Creator: Leonard, B. R.
System: The UNT Digital Library
Hanford Works Analytical Manual for Reactor Process Water (open access)

Hanford Works Analytical Manual for Reactor Process Water

Purpose: "The Hanford Works Analytical Manual for Process Water is designed to specify the analytical methods to be applied for control purposes in the Reactor Section, Process Sub-Section laboratories. The procedures are in general form and serve as references rather than outlined laboratory instructions. The manual us designed to replace the "Hanford Works Manual," HW-12862."
Date: February 13, 1953
Creator: Hanford Works
System: The UNT Digital Library
Thermogalvanic Effects Between Aluminum Slug Jackets (open access)

Thermogalvanic Effects Between Aluminum Slug Jackets

Report discussing an experiment testing the severity of attack of an aluminum slug jacket containing one or more spots hotter than the rest of the jacket. These conditions match those likely to exist in a poorly bonded slug.
Date: February 2, 1953
Creator: Katayama, Y. B.
System: The UNT Digital Library
Transformation and Magnetic Phenomena Occuring in Boron Stainless Steel Vertical Safety Rods (open access)

Transformation and Magnetic Phenomena Occuring in Boron Stainless Steel Vertical Safety Rods

Summary: "The low carbon 18-8 stainless steels containing approximately 1.7 per cent boron used for vertical safety rods at Hanford were found to be structurally stable in the temperature range 0-450 C. The addition of boron decreases the stability of this metastable austenitic alloy. Sufficient ferrite formation is induced by sub-zero temperature treatments to result in dimensional changes and a magnetic alloy. The difficulties encountered in machining this material are believed to be due primarily to segregation in the castings resulting in small areas of the hard intermetallic compound, FeB."
Date: February 6, 1953
Creator: Hueschen, R. E.
System: The UNT Digital Library
Neutron Diffusion and Random Walk (open access)

Neutron Diffusion and Random Walk

The following report analyzes random walks and whether or not they can be used to shed any light on problems of neutron diffusion.
Date: February 5, 1953
Creator: Duvall, G. E.
System: The UNT Digital Library
A Method for the Analysis of Radionuclide Mixture Using a Gamma-Beta Scintillation Spectrometer (open access)

A Method for the Analysis of Radionuclide Mixture Using a Gamma-Beta Scintillation Spectrometer

The following report describes a beta and gamma scintillation detector similar to what was used in previous decay studies, yet was modified to make it suitable for the analysis of mixtures of radio-nuclides.
Date: February 27, 1953
Creator: Leboeuf, M. B. & Connally, R. E.
System: The UNT Digital Library
The Analysis of TBP Process Streams for Calcium with the Flame Photometer (open access)

The Analysis of TBP Process Streams for Calcium with the Flame Photometer

Summary: A method was found for determining calcium concentrations in TBP process streams in spite of serious interferences bysodium, ferrous, uranyl, sulfate, phosphate, and sulfamate ions as well as by TBP. The precision attainable varied from sample to sample, depending upon its composition. In general, errors of 20% or greater occurred. The smallest determinable amount of calcium was about 10 mg/1.
Date: February 20, 1953
Creator: Brite, D. W.
System: The UNT Digital Library