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Polarographic Analysis of UNH in the IAW Stream (open access)

Polarographic Analysis of UNH in the IAW Stream

The following report describes two rapid, micro methods for the determination of UNH in Redox waste samples that had been developed fir the concentration range 0.2 to 100 g/l.
Date: January 17, 1949
Creator: Alkire, G. J. & Carson, W. N.
System: The UNT Digital Library
Polarographic Determination of Hexone (open access)

Polarographic Determination of Hexone

The following report describes polarographic methods that determine saturated aliphatic carbonyl compounds.
Date: November 10, 1949
Creator: Alkire, George J.
System: The UNT Digital Library
Limits of Inflammability and Ignition Temperatures of Hexone in Air and in Other Gaseous Atmospheres (open access)

Limits of Inflammability and Ignition Temperatures of Hexone in Air and in Other Gaseous Atmospheres

The following report summarizes the data taken from a series of measurements on the combustion and ignition properties of hexone. The experiments were taken at the Bureau of Mines Central Experiment Station by their personnel, and the samples were given to them by KAPL and Hanford.
Date: September 9, 1949
Creator: Alter, H. Ward
System: The UNT Digital Library
Fabrication of Uranium Wire (open access)

Fabrication of Uranium Wire

From abstract: "The present report describes experimental work performed to establish a procedure for the production of uranium metal wire. In all cases, the size of the initial rod was 1/2 inch diameter. Three materials were used: hot extruded tuballoy rod, high purity cast tuballoy rod, and cast U-235 rod."
Date: October 25, 1949
Creator: Anderson, R. E.; Taub, J. M. & Doll, D. T.
System: The UNT Digital Library
The Machinability of Beryllium (open access)

The Machinability of Beryllium

The following report investigates the isolation of the cause of the unusual tool-wear rates found in machining beryllium as attributed to an inherent characteristic of beryllium, or an effect of inclusions in beryllium, as well as the evaluation of the comparative machinability of the various types of beryllium.
Date: April 30, 1949
Creator: Armstrong, E. T.; Dayton, Russell Wendt & Dawes, R. C.
System: The UNT Digital Library
Bare Beryllium Extrusion Using Graphite Introductory Cones (open access)

Bare Beryllium Extrusion Using Graphite Introductory Cones

The following document describes the process of rare beryllium extrusion using graphite introductory cones with the purpose of finding a lubricant which would decrease excessive friction between the billet and prose parts.
Date: June 28, 1949
Creator: Arnold, Samuel V.
System: The UNT Digital Library
Extrusion at Revere Copper and Brass Inc., March 1, 1949 (open access)

Extrusion at Revere Copper and Brass Inc., March 1, 1949

The following report discusses the process of several sections of beryllium where 3.018" squares 40" in length can be machined, and six sound 8.0" diameter billets and three trial billets containing casting defects can be extruded.
Date: 1949
Creator: Arnold, Samuel V.
System: The UNT Digital Library
Equilibria in the Oxide Systems of Praseodymium and Americium (open access)

Equilibria in the Oxide Systems of Praseodymium and Americium

The thermal decomposition of the higher oxides of praseodymium and americium have been investigated.
Date: April 14, 1949
Creator: Asprey, L. B. & Cunningham, Burris Bell, 1912-1971
System: The UNT Digital Library
The Surface Preparation of Uranium for X-Ray Diffraction Studies by the Spectrometer Technique (open access)

The Surface Preparation of Uranium for X-Ray Diffraction Studies by the Spectrometer Technique

A report which describes a number of experiments conducted to compare the effects of different methods of surface preparation on x-ray diffraction patterns of uranium obtained by the spectrometer technique.
Date: March 24, 1949
Creator: Bach, J. H. & Burnham, J. B.
System: The UNT Digital Library
Fast Neutron Sensitivity of the CP Meter (open access)

Fast Neutron Sensitivity of the CP Meter

Abstract: "The sensitivity to fast neutrons of a CP Meter ionization chamber of the type used for health physics beta and gamma survey measurements has been investigated."
Date: June 10, 1949
Creator: Baker, E. E.; Gydesen, F. R. & Whipple, G. H., Jr.
System: The UNT Digital Library
Direct Current Electromagnetic Pumps (open access)

Direct Current Electromagnetic Pumps

Abstract: "A number of direct current conduction type electromagnetic pumps for liquid metals were constructed. Pumping capacities of over 400 gpm and efficiencies of over 50 percent were obtained. NaK alloy at temperatures up to 400 C was used in the test. The large currents required were obtained from rectifiers or from a homopolar generator constructed for the purpose."
Date: October 25, 1949
Creator: Barnes, A. H.; Smith, F. A. & Whitham, G. K.
System: The UNT Digital Library
Life of Van Stone Corrective Measures (open access)

Life of Van Stone Corrective Measures

This report is a document summarizing all information available on life aspects of various measures proposed to reduce or eliminate corrosion of Van Stone flanger.
Date: September 12, 1949
Creator: Botsford, C. W. & Eschbach, E. A.
System: The UNT Digital Library
Lectures on Nuclear Science and Engineering, November 16, 1948 to February 1, 1949 (open access)

Lectures on Nuclear Science and Engineering, November 16, 1948 to February 1, 1949

Technical report including multiple lectures on nuclear science and engineering, planned to survey the theories, designs, operations, and experimental facilities of the Brookhaven Nuclear Reactor.
Date: 1949
Creator: Brookhaven National Laboratory
System: The UNT Digital Library
Determination of Organic Acids in Process Solutions (open access)

Determination of Organic Acids in Process Solutions

Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated potentiometrically with standard potassium hydroxide solution. Since nitric acid and organic acids are present, two end points are observed. The potassium hydroxide added between these end points is equivalent to the organic acids. In the titration, CO2 from the atmosphere or in the potassium hydroxide is a source of error. The former was avoided and correction was made for the latter."
Date: June 29, 1949
Creator: Brouns, R. J. & Pollock, C. W.
System: The UNT Digital Library
Supplemental Technical Report on an Improved Process for the Manufacture of High Purity Calcium, Period Covered November 10, 1948 to January 31, 1949 (open access)

Supplemental Technical Report on an Improved Process for the Manufacture of High Purity Calcium, Period Covered November 10, 1948 to January 31, 1949

Abstract. Experimental work was carried out to improve material conversion efficiency and to reduce handling costs inherent in the present process for production of high purity calcium. Charges up to 54 pounds were handled successfully in the equipment available. Material losses were reduced and more complete removal of alkali and alkaline earth metals was effected by controlled pressures of inert gas and by melting under positive pressure of Argon.
Date: January 31, 1949
Creator: Brown, H. & Woodberry, P.
System: The UNT Digital Library
Progress Report on Carnotite Studies; Carbonate Process : July 1949 (open access)

Progress Report on Carnotite Studies; Carbonate Process : July 1949

This report for the month of July, 1949 discusses progress regarding work on the carbonate process and the recovery of uranium and vanadium from carbonate liquors.
Date: August 8, 1949
Creator: Brown, K. B. & Coleman, C. F.
System: The UNT Digital Library
Progress Report on Carnotite Studies; Carbonate Processes: September 1949 (open access)

Progress Report on Carnotite Studies; Carbonate Processes: September 1949

This is a progress report on the carbonate process, compiled by the chemical development department of the Carbide and Carbon Chemicals Corporation's Y-12 plant, covering the month of September, 1949. In the previous month, the problem of immediate interest to the Monticello operation were listed. Projects that were left incomplete during that time were continued during this month, as well as a brief investigation of the process in which raw ore is leached with sodium carbonate, the sands and slime separated, the sands leached with acid, and the slimes roasted in a pellitized form.
Date: October 6, 1949
Creator: Brown, K. B. & Coleman, C. F.
System: The UNT Digital Library
Progress Report on Carnotite Studies; Carbonate Processes : August 1949 (open access)

Progress Report on Carnotite Studies; Carbonate Processes : August 1949

This is a progress report compiled by the chemical development department of the Carbide and Carbon Chemicals Corporation's Y-12 plant, discussing work on the carbonate (Monticello) process, as well as the recovery of uranium and vanadium from carbonate liquors.
Date: September 8, 1949
Creator: Brown, K. B.; Coleman, C. F. & Grimes, W. R.
System: The UNT Digital Library
Density and Viscosity of Solutions in the Tributyl Phosphate Process for Uranium Recovery (open access)

Density and Viscosity of Solutions in the Tributyl Phosphate Process for Uranium Recovery

The following report discusses the presentation of preliminary density and viscosity data which may explain whether higher viscosities of the Deo Base-TBP systems, and a change in density differences between the two phases will lead to unsatisfactory column operation.
Date: November 29, 1949
Creator: Burger, L. L. & Slansky, C. M.
System: The UNT Digital Library
Properties of the System: Uranyl Nitrate-Aluminum Nitrate - Nitric Acid (or Sodium Hydroxide) - Sodium Nitrate - Water - Hexone (open access)

Properties of the System: Uranyl Nitrate-Aluminum Nitrate - Nitric Acid (or Sodium Hydroxide) - Sodium Nitrate - Water - Hexone

This report discusses properties of the Redox process. Density, apparent molar volumes and viscosity are all described.
Date: March 22, 1949
Creator: Burger, L. L.; Rehn, I. M.; Schmidt, H. R. & Slansky, C. M.
System: The UNT Digital Library
Stepwise Calculation for the Determination of the Number of Transfer Units in Countercurrent Extraction Columns (open access)

Stepwise Calculation for the Determination of the Number of Transfer Units in Countercurrent Extraction Columns

Report discussing a method for the stepwise calculation of the number of transfer units utilized in a given solvent extraction operation. "Use of the method results in a very appreciable saving in time of calculation with an error of 1.5% for the runs tested. The error tends to become smaller with increasing total numbers of transfer units involved."
Date: September 12, 1949
Creator: Burns, W. A. & Eschbach, E. A.
System: The UNT Digital Library
Dissolution of Uranium Tetrafluoride (open access)

Dissolution of Uranium Tetrafluoride

"Five new dissolution processes for uranium tetrafluoride are discussed-the NH4OH-H2O2 method, the H2SC4 - (NH4)2S2O8 method, the AlCl3 method, the NaAlcl method, and the Al (NO3)3.9E2O method. It is concluded that NaAlCl4 and Al(NO3)3.9H2O are preferable to the other agents, especially with regard to rate of dissolution and ease of manipulation."
Date: 1949
Creator: Calkins, V. P. & Susano, C. D.
System: The UNT Digital Library
Special Irradiation of Temperature-Indicating Liquid: Final Report--Production Test 105-266-P (open access)

Special Irradiation of Temperature-Indicating Liquid: Final Report--Production Test 105-266-P

A report discussing an experiment conducted to determine the effect of radiation on the melting point of Tempilaq, a commercially available, temperature-indicating liquid.
Date: August 18, 1949
Creator: Carbon, M. W.
System: The UNT Digital Library
The Coulometric Titration of 8-Hydroxyquinoline (open access)

The Coulometric Titration of 8-Hydroxyquinoline

Abstract: "A new method of determining 8-hydroxyquinoline by titration with electrolytucally-generated bromine has been developed. Results show good precision in the range 0.4 mg. to 1.6 mg. total 8-hydroxyquinoline, with 99% confidence limits of less than +/- 2%. An electronically-regulated constant current source, required by the method, is described. A new indicator system with high sensitivity to free bromine is discussed."
Date: June 16, 1949
Creator: Carson, W. N.
System: The UNT Digital Library