The following report is based on the observations made during a visit to the Oak Ride National Laboratories of their Redox Pilot Plant equipment.

Introduction: In order to determine the relative corrosion resistance of welded mild and stainless steels in Redox Stream IAW neutralized to pH 0, 2, and 10 a test program, described below, has been carried out.

From summary: "On the basis of the tests described herein, the corrosion characteristics of T-347 welded stainless steel are found not to be affected by the magnetic properties of the welds even though these properties are likely the result of the presence of the ferritic structure."

Introduction: Static, total immersion corrosion tests were carried out at room temperatures with Carboloy grades 44-A, 78, 907, X-3119-A and X-3119-B in Redox process solutions (ANL, June 1, 1949 Flowsheet) 1AX, 1AF, and 1AS.

Introduction: "Room temperature and elevated temperature, static immersion and vapor suspicion, corrosion tests were conducted with Duriron, Hastelloy C, and tantalum in hydriotic acid and 234-5 project process supernatant solution (synthetic environments. The data relevant to these tests are contained herein."

Abstract: "Small amounts of acetic acid, equivalent to 400 ul. of 0.3 to 0.13 g/L. can be titrated coulonatrically in the presence of a 10 to 25-fold excess of HN03 in 70%, isopropanol. An accuracy of +/- 0.1% and a precision of +/- 8.5% (99% limite) are obtained.

Abstract: "A new method of determining 8-hydroxyquinoline by titration with electrolytucally-generated bromine has been developed. Results show good precision in the range 0.4 mg. to 1.6 mg. total 8-hydroxyquinoline, with 99% confidence limits of less than +/- 2%. An electronically-regulated constant current source, required by the method, is described. A new indicator system with high sensitivity to free bromine is discussed."

Abstract: "The critical mass both of an untamped and water-tamped sphere with parabolic radial variation of the intrinsic buckling is calculated by a perturbation method. The result is applied to finding the minimum critical mass of plutonium in water suspension with infinite water temper; the calculations show that the minimum critical mass at constant concentration may be reduced by an amount of the order of 7.6% when the concentration of plutonium is permitted to vary throughout the suspension."

From introduction: "This report examines the hazard which would result in the extremely unlikely event that all of the safety devices failed to operate either by accident or sabotage."

The following report discusses the presentation of preliminary density and viscosity data which may explain whether higher viscosities of the Deo Base-TBP systems, and a change in density differences between the two phases will lead to unsatisfactory column operation.

The following report describes the developmental process of the determination of free nitric acid in solutions containing uranyl nitrate, aluminum nitrate and sodium dichromate.

Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated potentiometrically with standard potassium hydroxide solution. Since nitric acid and organic acids are present, two end points are observed. The potassium hydroxide added between these end points is equivalent to the organic acids. In the titration, CO2 from the atmosphere or in the potassium hydroxide is a source of error. The former was avoided and correction was made for the latter."

Summary: "This report investigates photographic methods of measuring beta radiation and includes a study of temperature effects on these measurements. Experimental data are submitted to show that an increase in film temperature before and during beta irradiation causes a definite increase in density for the same dosage. Recommendations drawn from experience gained in the experimental works are offered."

Abstract: "The sensitivity to fast neutrons of a CP Meter ionization chamber of the type used for health physics beta and gamma survey measurements has been investigated."

Abstract: "A method is described for the identification and quantitative determination of trace amounts of rare earths in graphite by measurement of the energies and decays of the activities induced by neutron irradiation. The specific rare earth elements identified are europium and samarium. During the development of this method, the half-lives of Eu-152 and Sm-153 were determined. These are reported as 9.32 +/- 0.04 hours and 46.34 +/- 0.23 respectively."

This report is a document summarizing all information available on life aspects of various measures proposed to reduce or eliminate corrosion of Van Stone flanger.

Abstract: "Following nitrate removal by means of a three-stage hydrochloric acid digestion, uranium was reduced with chromous sulfate reagent. In an inert atmosphere, the quadrivalent uranium was titrated at 80-95[degrees] with standard ferric sulfate solution. The end point was obtained with a potentiometric cell including a platinum in-titrant reference electrode and a platinum indicator electrode. Application was made to various low leverl uranium solutions. For samples containing 1 - 12 milligrams or uranium, less than one percent error may be expected. Iron and chromium do not interfere."

The following report presents some points of interest obtained from the use of optical equipment at the Hanford Works; however, this report does not give complete descriptions of the instruments or theories. Full descriptions can be found in the Instrument Division Manual, Section IV.

This report analyzes Parian and Teflon that were exposed to solutions of 1AX, 1AS, and 1AF, ANL June 1, 1948 Flowsheet, under conditions described in the following report.

The following report describes two rapid, micro methods for the determination of UNH in Redox waste samples that had been developed fir the concentration range 0.2 to 100 g/l.

The following report describes polarographic methods that determine saturated aliphatic carbonyl compounds.

This report discusses methods of producing aluminum nitrate for the Redox process. Large amounts of aluminum nitrate are consumed during the Redox process, so this report explores preparation of this material through the dissolution of hydrated aluminum oxide in nitric acid.

This report discusses properties of the Redox process. Density, apparent molar volumes and viscosity are all described.

Report discussing experiments and developments in purification of graphite starting from March, 1949.