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A Microdetermination of Uranium by Ferric Sulfate Titration (open access)

A Microdetermination of Uranium by Ferric Sulfate Titration

Abstract: "Following nitrate removal by means of a three-stage hydrochloric acid digestion, uranium was reduced with chromous sulfate reagent. In an inert atmosphere, the quadrivalent uranium was titrated at 80-95[degrees] with standard ferric sulfate solution. The end point was obtained with a potentiometric cell including a platinum in-titrant reference electrode and a platinum indicator electrode. Application was made to various low leverl uranium solutions. For samples containing 1 - 12 milligrams or uranium, less than one percent error may be expected. Iron and chromium do not interfere."
Date: February 16, 1949
Creator: Christopherson, E. W.
System: The UNT Digital Library
The Coulometric Titration of 8-Hydroxyquinoline (open access)

The Coulometric Titration of 8-Hydroxyquinoline

Abstract: "A new method of determining 8-hydroxyquinoline by titration with electrolytucally-generated bromine has been developed. Results show good precision in the range 0.4 mg. to 1.6 mg. total 8-hydroxyquinoline, with 99% confidence limits of less than +/- 2%. An electronically-regulated constant current source, required by the method, is described. A new indicator system with high sensitivity to free bromine is discussed."
Date: June 16, 1949
Creator: Carson, W. N.
System: The UNT Digital Library
The Coulometric Determination of Acetic Acid (open access)

The Coulometric Determination of Acetic Acid

Abstract: "Small amounts of acetic acid, equivalent to 400 ul. of 0.3 to 0.13 g/L. can be titrated coulonatrically in the presence of a 10 to 25-fold excess of HN03 in 70%, isopropanol. An accuracy of +/- 0.1% and a precision of +/- 8.5% (99% limite) are obtained.
Date: August 16, 1949
Creator: Carson, W. N. & Ko, Roy
System: The UNT Digital Library
The Spectrochemical Analysis of Hafnium and Zirconium (open access)

The Spectrochemical Analysis of Hafnium and Zirconium

Abstract: "The analysis of hafnium and zirconium by the copper spark technique is presented for solutions of HCl, HF, and HClO4 acids. The special techniques of electrode protection and vacuum drying of perchloric acid samples are outlined. Also given are the working curves and deviations of both elements."
Date: March 16, 1949
Creator: Conway, John G. & Moore, Milton F.
System: The UNT Digital Library
Power Recovery at Brookhaven ; Report No. 1 (open access)

Power Recovery at Brookhaven ; Report No. 1

From introduction: "This is the first report on the study made of the possible power recovery without excessive cost, from the operation of the Brookhaven reactor."
Date: June 16, 1949
Creator: Lucke, Charles Edward
System: The UNT Digital Library
Preparation of Ductile Zirconium: Summary of Thermodynamic Data (open access)

Preparation of Ductile Zirconium: Summary of Thermodynamic Data

Abstract: A summary of thermodynamic calculations for zirconium halides is given. Data indicates that the iodide is the most promising of the halides for arc dissociation and that good recoveries of zirconium should be obtainable provided dissociation is carried out at reduced pressure.
Date: September 16, 1949
Creator: Findlay, G. R.
System: The UNT Digital Library
Procedures in Magnetic Measurements at the University of California Radiation Laboratory, Berkeley:  Fields Which are Constant or Vary Slowly with Time (open access)

Procedures in Magnetic Measurements at the University of California Radiation Laboratory, Berkeley: Fields Which are Constant or Vary Slowly with Time

The flux standard is a device which will give a known flux-linkage change to be used as a calibration. At the Radiation Laboratory, two types of flux standards are used, a stationary type and a portable type.
Date: August 16, 1949
Creator: Richardson, Robert E.
System: The UNT Digital Library