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A Microdetermination of Uranium by Ferric Sulfate Titration (open access)

A Microdetermination of Uranium by Ferric Sulfate Titration

Abstract: "Following nitrate removal by means of a three-stage hydrochloric acid digestion, uranium was reduced with chromous sulfate reagent. In an inert atmosphere, the quadrivalent uranium was titrated at 80-95[degrees] with standard ferric sulfate solution. The end point was obtained with a potentiometric cell including a platinum in-titrant reference electrode and a platinum indicator electrode. Application was made to various low leverl uranium solutions. For samples containing 1 - 12 milligrams or uranium, less than one percent error may be expected. Iron and chromium do not interfere."
Date: February 16, 1949
Creator: Christopherson, E. W.
System: The UNT Digital Library
Corrosion Tests on Tantalum, Hastelloy C and Duriron in 234-5 Project Solutions (open access)

Corrosion Tests on Tantalum, Hastelloy C and Duriron in 234-5 Project Solutions

Introduction: "Room temperature and elevated temperature, static immersion and vapor suspicion, corrosion tests were conducted with Duriron, Hastelloy C, and tantalum in hydriotic acid and 234-5 project process supernatant solution (synthetic environments. The data relevant to these tests are contained herein."
Date: February 25, 1949
Creator: Work, J. B. & Koenig, W. W.
System: The UNT Digital Library
The Surface Preparation of Uranium for X-Ray Diffraction Studies by the Spectrometer Technique (open access)

The Surface Preparation of Uranium for X-Ray Diffraction Studies by the Spectrometer Technique

A report which describes a number of experiments conducted to compare the effects of different methods of surface preparation on x-ray diffraction patterns of uranium obtained by the spectrometer technique.
Date: March 24, 1949
Creator: Bach, J. H. & Burnham, J. B.
System: The UNT Digital Library
The solvent-extraction performance of small scale redox IA columns using Fenske helix packing, ammonium nitrate salting agent, and unirradiated uranium (open access)

The solvent-extraction performance of small scale redox IA columns using Fenske helix packing, ammonium nitrate salting agent, and unirradiated uranium

A report which deals with the Redox IA Column studies made in small-scale columns packed with 3/16-in. Fenske helices and using NH4NO3 salting agent.
Date: April 13, 1949
Creator: Woodfield, F. W.; Bradley, J. G.; Switzer, W. O. & Merrill, E. T.
System: The UNT Digital Library
Corrosion Tests on Carboloy in Redox Process Solutions (open access)

Corrosion Tests on Carboloy in Redox Process Solutions

Introduction: Static, total immersion corrosion tests were carried out at room temperatures with Carboloy grades 44-A, 78, 907, X-3119-A and X-3119-B in Redox process solutions (ANL, June 1, 1949 Flowsheet) 1AX, 1AF, and 1AS.
Date: April 6, 1949
Creator: Koenig, W. W.
System: The UNT Digital Library
Optical Instruments for the Atomic Industry (open access)

Optical Instruments for the Atomic Industry

The following report presents some points of interest obtained from the use of optical equipment at the Hanford Works; however, this report does not give complete descriptions of the instruments or theories. Full descriptions can be found in the Instrument Division Manual, Section IV.
Date: 1949
Creator: Holeman, J. M.
System: The UNT Digital Library
The Critical Mass of a Spherical Reactor with Variable Intrinsic Buckling (open access)

The Critical Mass of a Spherical Reactor with Variable Intrinsic Buckling

Abstract: "The critical mass both of an untamped and water-tamped sphere with parabolic radial variation of the intrinsic buckling is calculated by a perturbation method. The result is applied to finding the minimum critical mass of plutonium in water suspension with infinite water temper; the calculations show that the minimum critical mass at constant concentration may be reduced by an amount of the order of 7.6% when the concentration of plutonium is permitted to vary throughout the suspension."
Date: April 28, 1949
Creator: Muller, G. M.
System: The UNT Digital Library
Determination of Organic Acids in Process Solutions (open access)

Determination of Organic Acids in Process Solutions

Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated potentiometrically with standard potassium hydroxide solution. Since nitric acid and organic acids are present, two end points are observed. The potassium hydroxide added between these end points is equivalent to the organic acids. In the titration, CO2 from the atmosphere or in the potassium hydroxide is a source of error. The former was avoided and correction was made for the latter."
Date: June 29, 1949
Creator: Brouns, R. J. & Pollock, C. W.
System: The UNT Digital Library
Parian and Teflon in 1A Redox Solutions (open access)

Parian and Teflon in 1A Redox Solutions

This report analyzes Parian and Teflon that were exposed to solutions of 1AX, 1AS, and 1AF, ANL June 1, 1948 Flowsheet, under conditions described in the following report.
Date: May 9, 1949
Creator: Koenig, W. W.
System: The UNT Digital Library
The Coulometric Titration of 8-Hydroxyquinoline (open access)

The Coulometric Titration of 8-Hydroxyquinoline

Abstract: "A new method of determining 8-hydroxyquinoline by titration with electrolytucally-generated bromine has been developed. Results show good precision in the range 0.4 mg. to 1.6 mg. total 8-hydroxyquinoline, with 99% confidence limits of less than +/- 2%. An electronically-regulated constant current source, required by the method, is described. A new indicator system with high sensitivity to free bromine is discussed."
Date: June 16, 1949
Creator: Carson, W. N.
System: The UNT Digital Library
The Coulometric Determination of Acetic Acid (open access)

The Coulometric Determination of Acetic Acid

Abstract: "Small amounts of acetic acid, equivalent to 400 ul. of 0.3 to 0.13 g/L. can be titrated coulonatrically in the presence of a 10 to 25-fold excess of HN03 in 70%, isopropanol. An accuracy of +/- 0.1% and a precision of +/- 8.5% (99% limite) are obtained.
Date: August 16, 1949
Creator: Carson, W. N. & Ko, Roy
System: The UNT Digital Library
Redox : Analytical Research Group Report [for] March and April 1949 (open access)

Redox : Analytical Research Group Report [for] March and April 1949

Report discussing the results of research conducted by the Hanford Works Analytical Research Group during the period from March 1949 to April 1949.
Date: June 21, 1949
Creator: Schmidt, H. R.
System: The UNT Digital Library
Investigations Relating to the Extension of Laminar Flow by Means of Boundary-Layer Suction Through Slots (open access)

Investigations Relating to the Extension of Laminar Flow by Means of Boundary-Layer Suction Through Slots

Note presenting experimental investigations of boundary-layer suction through slots as a means of increasing the extent of laminar flow on airfoil sections. The results show that, with the use of suitable slots, substantial increases in the extent of laminar flow can be achieved by boundary-layer control with only a small expenditure of power. Results regarding slot geometry and arrangement, suction slots in an unfavorable pressure gradient, suction slots in a favorable pressure gradient, and determinations of the relations controlling the distribution of suction slots are provided.
Date: October 1949
Creator: Loftin, Laurence K., Jr. & Burrows, Dale L.
System: The UNT Digital Library
Quantitative Study of Variations in Concentration of Glycerol and Aerosol OT on Foaming Volume of Oil at Room Temperature (open access)

Quantitative Study of Variations in Concentration of Glycerol and Aerosol OT on Foaming Volume of Oil at Room Temperature

"The amount of foam that can be formed in the presence of certain pure chemical agents was investigated by a new method. The effect of variations in concentration and proportion of Aerosol OT and glycerol was studied and the effects of various other mixtures have been given for comparison. Both Gulf Agent and Aerosol-OT - glycerol mixtures, when present in comparable amounts, prohibited the formation of the normal volumes of foam to the same extent and in the optimum cases reduced it to only one-tenth of its normal value" (p. 1).
Date: April 1949
Creator: McBain, J. W. & Ross, Sydney
System: The UNT Digital Library
Effect of Various Compounds in Use With Airplane Engines Upon Foaming of Aircraft Lubricating Oil (open access)

Effect of Various Compounds in Use With Airplane Engines Upon Foaming of Aircraft Lubricating Oil

Report presenting an investigation of aircraft lubricating oil that is contaminated with various materials used in connection with airplane engines or contained in the fuel. Over 60 of the materials have been tested to determine their influence on the foaming of an aircraft lubricating oil. All but 13 of the compounds were found to have a small or negligible effect, but the other 13 were found to be strong foaming agents.
Date: April 1949
Creator: McBain, J. W. & Woods, W. W.
System: The UNT Digital Library
The Buckling of Parallel Simply Supported Tension and Compression Members Connected by Elastic Deflectional Springs (open access)

The Buckling of Parallel Simply Supported Tension and Compression Members Connected by Elastic Deflectional Springs

Note presenting an investigation of the problem of the buckling of parallel simply supported tension and compression members connected by equally stiff and equally spaced elastic deflection springs as an approximation to the problem of the effect of finite stiffness of ribs and tension surface on the buckling load of the compression surface of a wing. Charts relating compressive buckling load, deflectional spring stiffness, and the ratio of the flexural stiffness of the members are given for tension and compression members with various numbers of spans.
Date: February 1949
Creator: Seide, Paul & Eppler, John F.
System: The UNT Digital Library
Compressive Buckling of Simply Supported Plates With Longitudinal Stiffeners (open access)

Compressive Buckling of Simply Supported Plates With Longitudinal Stiffeners

"Charts are presented for the analysis of the stability under compression of simply supported rectangular plates with one, two, three, and an infinite number of identical equally spaced longitudinal stiffeners that have zero torsional stiffness" (p. 1).
Date: March 1949
Creator: Seide, Paul & Stein, Manuel
System: The UNT Digital Library
Linear theory of boundary effects in open wind tunnels with finite jet lengths (open access)

Linear theory of boundary effects in open wind tunnels with finite jet lengths

Report in two parts: one examines the boundary conditions for an open wind tunnel with special references to the effects of the closed entrance and exit sections, while the other derives solutions of four types of two-dimensional open tunnels, including one in which the pressures on the two free surfaces are not equal.
Date: March 1949
Creator: Katzoff, Samuel; Gardner, Clifford S.; Diesendruck, Leo & Eisenstadt, Bertram J.
System: The UNT Digital Library
Matrix Methods for Calculating Cantilever-Beam Deflections (open access)

Matrix Methods for Calculating Cantilever-Beam Deflections

Note presenting the method of numerical integration for calculation of beam deflection in matrix form to give it the advantages which are inherent in an influence-coefficient method. Examples are presented to show that the use of weighted matrices reduces the calculation time required to obtain a desired degree of accuracy.
Date: March 1949
Creator: Benscoter, Stanley U. & Gossard, Myron L.
System: The UNT Digital Library
Effect of forebody warp on the hydrodynamic qualities of a hypothetical flying boat having a hull length-beam ratio of 15 (open access)

Effect of forebody warp on the hydrodynamic qualities of a hypothetical flying boat having a hull length-beam ratio of 15

Report of an investigation of the effect of forebody warp on the hydrodynamic qualities of a hypothetical flying boat with a hull length-beam ratio of 15 in smooth water and in waves. Warping the forebody planing bottom was found to appreciably increase the range of stable trim between the lower and upper trim limits of stability, although the center-of-gravity limits of stability were reduced.
Date: March 1949
Creator: Carter, Arthur W. & Weinstein, Irving
System: The UNT Digital Library
Data on the Compressive Strength of 75S-T6 Aluminum-Alloy Flat Panels with Longitudinal Extruded Z-Section Stiffeners (open access)

Data on the Compressive Strength of 75S-T6 Aluminum-Alloy Flat Panels with Longitudinal Extruded Z-Section Stiffeners

"The experimental results are presented for a part of an investigation of the compressive strength of 75S-T6 aluminum-alloy flat panels with longitudinal extruded Z-section stiffeners. This part of the investigation is concerned with panels in which the ratio of the thickness of the stiffener material to the skin material varies from 0.4 to 1.0 and the ratio of stiffener spacing to skin thickness varies from 15 to 40" (p. 1).
Date: March 1949
Creator: Hickman, William A. & Dow, Norris F.
System: The UNT Digital Library
Corrosion tests of a heated wing utilizing an exhaust-gas-air mixture for ice prevention (open access)

Corrosion tests of a heated wing utilizing an exhaust-gas-air mixture for ice prevention

Report presenting an investigation of the exhaust of corrosive attack in an aluminum alloy wing employing an exhaust-gas-air mixture as a heating medium for ice prevention. There were no cases of structurally serious corrosion on either painted or plain specimens removed from the wing for detailed microscopic and metallurgic examination.
Date: January 1949
Creator: Holdaway, George H.
System: The UNT Digital Library
Study by the Prandtl-Glauert method of compressibility effects and critical Mach number for ellipsoids of various aspect ratios and thickness ratios (open access)

Study by the Prandtl-Glauert method of compressibility effects and critical Mach number for ellipsoids of various aspect ratios and thickness ratios

From Summary: "By the use of a form of the Prandtl-Glauert method that is valid for three-dimensional flow problems, the value of the maximum incremental velocity for compressible flow about thin ellipsoids at zero angle of attack is calculated as a function of the Mach number for various aspect ratios and thickness ratios. The critical Mach numbers (within the accuracy of the Prandtl-Glauert method) of the various ellipsoids are also determined. The results indicate an increase in critical Mach number with decrease in aspect ratio which is large enough to explain experimental results on low-aspect-ratio wings at zero lift."
Date: January 1949
Creator: Hess, Robert V. & Gardner, Clifford S.
System: The UNT Digital Library
Investigation of Meteorological Conditions Associated with Aircraft Icing in Layer-Type Clouds for 1947-48 Winter (open access)

Investigation of Meteorological Conditions Associated with Aircraft Icing in Layer-Type Clouds for 1947-48 Winter

Rotating-cylinder measurements of the icing conditions encountered in flight during the winter of 1947-48 are presented. Liquid water content, drop size, and temperature data are shown to be consistent with previously measured conditions and with proposed maximum icing conditions in supercooled layer-type clouds. Cumulative frequency graphs of meteorological parameters indicate the frequency with which various icing conditions have been encountered in the Great Lakes area and surrounding states.
Date: January 1949
Creator: Kline, Dwight B.
System: The UNT Digital Library