Preignition-limited performance data were obtained on a supercharged CFR engine at two sets of operating conditions over a wide range of fuel-air ratios to determine the preignition characteristics for the following five fuels: s-3 reference fuel, s-3 plus 4 ml. tel per gallon, afd-33(140-p), benzene, and diisobutylene. Maximum thermal-plug temperatures at constant intake-air pressures were also determined to correlate the preignition characteristics of each fuel with its ability to increase general engine-temperature levels. Additional runs were made to compare the preignition-limited performance of triptane, triptane plus 4 ml. tel per gallon, and an-f-28r fuel.