A series of measurements was performed to investigate the gamma ray spectra, in the region from about 100 kev to about 3 Mev, resulting from the capture of thermal neutrons in a number of elements. The purpose of the experiment was to supplement the high energy capture gamma ray data in order to remove some of the ambiguities from the proposed energy level schemes and to obtain information for the Shielding Group of Brookhaven National Laboratory on elements normally found in reactors.