Polarographic Determination of Uranium in Dust Samples (open access)

Polarographic Determination of Uranium in Dust Samples

Abstract: "Samples of dust are collected from the atmosphere with a Mine Safety Appliance Co. electrostatic precipitator and analyzed for uranium by means of a dropping mercury electrode apparatus. Two to three micrograms of uranium can be detected in a cell solution volume of 1 ml. Iron, nickel and chromium present in shop dusts do not interfere. Copper may interfere if present in excess but may be removed by a sulfide precipitation. Directions for preparation of cell solution and operation of the Polarograph are given. The polarographic method described may be used for determination of uranium in samples other than atmospheric dusts."
Date: August 30, 1943
Creator: Smith, Stanton B.
System: The UNT Digital Library
Distribution Coefficient of D₂O Between Triethylamine and Water (open access)

Distribution Coefficient of D₂O Between Triethylamine and Water

Summary: "Water containing 1.8% D2O was distributed between the two liquid phases formed with triethylamine at 20 and 35 C. The triethylamine was removed from each phase by aseotropic distillation with benzene before analyzing the water by determining its density with a quartz float. The ratios of the concentrations of the D2O in the water layer to that in the amino layer were 1.007 and 1.004 at 20 and 35, respectfully. The differences from unity are about the same as the errors of analysis."
Date: August 31, 1943
Creator: Carlson, H. C.
System: The UNT Digital Library