Aid in redesign of the calibration facility in order to: 1. Reduce the rate of exposure for calibration personnel below 1 mr/hr; 2. Reduce the rate of exposure outside of the 3745 Building; 3. Reduce the risk of breaking radium sources; 4. Improve the efficiency of calibration procedures by: a. Allowing calibration to be done faster; b. Providing several calibration ranges which can operate simultaneously in the present space allowed; c. Allowing instrument survey work to proceed while calibration work is done. A well-type calibration installation is proposed and a brief description of the required shielding is included.

The first step in a proposed processing method for recovery of uranium from graphite-uranium fuels consists of oxidation of the fuel by oxygen to volatilize the carbon. Residue ash from the combustion step can be treated in a variety of ways to recover and purify the uranium. The combustion step may be caried out by contacting the solid fuel in a fixed or moving bed with a stream of oxygen-bearing gas in a tubular or annular reactor. Oxidizing gas may be introduced to the reactor at several points up the reactor and there may be continuous or intermittent addition of fresh fuel and removal of residue ash.

The first man-made nuclear reactor -- or "pile" as it was then called -- was rather hurriedly improvised and operated in a crowded space under the athletic bleachers of Stagg Field at the University of Chicago on December 2, 1942. Just prior to this time, there began the assembly of a group of physicists with an unusual assignment. They were determined that radiation hazards of unprecedented proportions must be coped with successfully in the conduct of reactor programs as planned. Since these physicists were to be concerned with the health of radiation workers, they were called health physicists. There was no formal instruction available to this first group of health physicists and they perforce received training as they felt their way by firsthand experience and by trial and error. Health physics at Oak Ridge National Laboratory from the very beginning has been organized into three principal areas: applied activities, education and training and research.

The thermophysical properties of Armco iron such as thermal conductivity, electrical resistivity, and Seebeck coefficient have been extensively investigated and reviewed up to 1000 degrees C. Few investigations of such properties have been made on high purity iron. If such a study is made using the same apparatus to determine the properties of two purity levels of iron, then several significant intercomparisons can be made which add meaning to data on a single material. The systemic errors for a single apparatus are the same, therefore comparison of a property of two similar materials is more significant. A comparison of the property changes with temperature and purity can show the effects of impurities on the mechanisms contributing to a property and allows prediction of the properties of iron as a function of purity. For these reasons a study was initiated on the high-purity iron for comparison to Armco iron.

The experimental details, mathematical models, and typical data for a rapid comparative method for thermal conductivity measurements are presented. The method consists of measuring the temperature change of a small silver sphere after it is brought in contact with a small disk-shaped specimen which was initially at ta higher temperature. This temperature change was calibrated in the range of 50 to 400 degrees C by making measurements on samples of know thermal conductivity. The accuracy of this technique was shown to be between than +-10% with a reproducibility of at least +-2.5%. Using known transport mechanisms for heat conduction in solids and the temperature dependency of the electrical conductivity, a means to judiciously extrapolate thermal conductivity data obtained between 50 and 400 degree C to high temperature is presented.

Grade CGB graphite is a nuclear graphite which is basically an extruded petroleum coke bonded with coal tar pitch. No carbon blacks are used and the low-permeation graphite is finished through a series of impregnations and heat treatments with a final heat treatment of all components to 2800 degrees C. A listing of the results obtained is given in Table 1. The results at 51 degrees C are considered questionable. There was a slight contamination of the 90% Pt 10% Rh-Pt thermocouples at 910 degrees C but it was not sufficient to doubt the validity of the 910 degrees C results. However, the results obtained at 1015 degrees C should be disregarded because of severe thermocouple instabilities. In addition, the electrical resistance of the core heater at 603 degrees C indicated the thermocouples had a -10 to -15 degree error which is sufficient justification to disregard the 605 degrees C data.

The purpose of this study was to investigate mathematically the concentration decrease due to particle deposition phenomena in highly concentrated monodispersed aerosols (mean particle size less than 1.0 mu) flowing through ventilation ducts. It was found that, from the standpoint of removal, the decrease in concentration due to deposition on duct walls was insignificant; but, when considering contamination on duct walls, the amount deposited, even though small when compared with the amount in the bulk stream, should not be overlooked.

Summary: The use of dimensionless-parameter frequency response diagrams to determine accuracies of lumped-parameter approximations is demonstrated by two examples: calculation of the heat flux at the surface of a semi-infinite solid due to temperature fluctuations of an adjacent fluid; and the response of a counterflow heat exchanger to inlet fluid temperature perturbations. Dimensionless system parameters make it possible to use general-purpose plots to find the error in particular approximations as a function of the frequency of perturbation. Such plots are directly applicable to control-system stability problems, where the highest frequency of interest is usually apparent.

Abstract. Some diffusion parameters of water are computed with various thermal-neutron scattering laws. It is found that the diffusion cooling coefficient, in particular, is reasonably sensitive to the scattering law, but that the diffusion cooling coefficients predicted by the Radkowsky and Nelkin kernels are in fortuitious agreement. The coefficients computed for the Nelkin kernel, when treated in a manner consistent with the way in which experimental data are treated, are in reasonable agreement with the results of a recent experiment.

Abstract: (1) Grain growth in UO2 pellets was studies between 100 C and 2600 C. The pellets were encapsulated in small vacuum-tight tungsten containers in an argon atmosphere. (2) The grain size-time relationship could be expressed by an equation. A low exponent, m>_ 1/3, was found in those experiments and is related to the type of UO2 investigated. An activation energy of 65 kcal/mole was obtained for the grain growth process. The time exponent, m, increased with increasing temperature if the pellets were not contained in closed capsules bu heated under an argon pressure of 1.5 atm. (3) An interaction between tungsten and UO2 could be observed at a a temperature of 2600 C after prolonged heat treatment.

From introduction: "This is the sixteenth in a series of quarterly reports which cover the progress and results from the conceptual designs, economic evaluations and research and development work performed by the General Electric Company as part of Contract AT(01-3)-189, Project Agreement No. 13."

FLOSS III is a third-generation version of a digital computer program which solves a one-dimensional difference representation of the momentum, energy, continuity, and state equations for turbulent, compressible gas flow in equivalent hydraulic channels. Extensive use of this program has been employed in the design and performance analyses of Pluto-type nuclear heat exchangers, and in the specific case of the Tory II-A test series, agreement was obtained to better than 5% for all experimentally measured parameters. The NOMAC and DASH-N programs combine the effects of up to thirty varieties of channels with the dependent boundary conditions imposed by a common inlet diffuser and exit nozzle. The resulting calculations yield performance information for blow-down facility and ramjet flight condition application of the heat exchanger.

Modifications to the A.A.E.C.'s Siemens Diffractometer are described which enable precision lattice parameter determinations on single crystals. Analysis of the errors and consideration of results suggest that accuracies of about 1--2 parts in 10/sup 5/ are obtained on small beryllium oxide crystals. Details of alignment and measurement procedure are included.

The results of unclassified experiments on the irradiation behaviour of BeO fueled with UO2 and (U,Th)O2 are summarized and discussed. The overall picture is still somewhat confused owing to the different experimental conditions used by different workers. A serious deficiency in most of the work is the failure to quote the energies of the irradiation neutrons and it is not clear whether the observed changes are due to fission fragment or fast neutron bombardment. The irradiation behaviour, in general, appears to be good up to fission doses of at least 5 x 10(20) fissions cm-3 of dispersion.

Abstract: The use of a high energy proton or electron beam, directed vertically to act as a probe for the study of atmospheric processes is proposed. An outstanding feature of such an atmospheric probe is its capability to ionize a column of air repeatedly in a few microseconds and in approximately the same place. Characteristics of a vertical proton beam which may be generated by the Zero Gradient Synchrotron at the Argonne National Laboratory are discussed and calculations are presented to provide an estimate of the ion concentration as a function of height in the atmosphere. The potential uses of an atmospheric ionized column for meteorological research are discussed such investigations include the artificial initiation of lightning, the production of atmospheric ozone resulting from lightning, and the line spectra associated wit the lightning channel. Also presented is a method whereby a combination of the igh energy particle beam and infrared techniques may be used to determine the air circulation within a thunderstorm. Brief mention is made of the possible uses of a high energy particle beam for aerospace sciences, such as the study of whistlers and elecro-magnetic radiation phenomenon associated with the aurora and airglow.

Introduction: The purpose of this technical report is to review the water chemistry methods and equipment developed for use with the Maritime Loop Irradiation Program conducted in the General Electric Test Reactor (GETR) from December 2, 1960 to July 19, 1962. Special emphasis is given to areas having general application to other high purity water systems. The Appendix includes a discussion of specific conductivity and pH in high purity water systems. A major section of this report is devoted to a review of gross activity levels on coupons of two different surface finishes exposed in the loop coolant system for various time intervals. A major objective of the chemistry program was to select or develop analytical methods such that the analyses could be performed at the loop location by technical personnel who normally operate the loop. By this means, frequent samples were obtained and analyzed directly thus providing close monitoring and control of the loop water chemistry at minimum expense.

Summary: The Mixed Spectrum Superheater (MSSR) is an integral superheater reactor in which boiling occurs in an annular Boiling Water Reactor section and steam in superheated in an unmoderated fast section in the center. A Mixed Spectrum Critical Assembly (MSCA) to be operated at the Vallecitos Atomic Laboratory has been designed to mock up a 75-150 MWe prototype MSSR. The principal experimental measurements aimed at proving the feasibility of the MSSR concept include power distribution, Doppler effect, flooding effects, distribution of reactivity, control rod worths, and the effect of the control system on the power distribution.

Abstract. A brief review of the development of the subject of lattice defects in solids is given. The relation of this problem to field theory methodology is discussed; the defect is regarded as a particle imbedded in the phonon field. One may then discuss scattering states in the field, or “dressed” states of the particle. Specific application is then made to a defect in a simple cubic crystal including interactions between the defect site and its six nearest neighbors. Scattering solutions and scattering cross-sections are calculated and show that vacancies can cause strong resonant scattering, or pseudo-localized modes, at frequencies well below the Debye frequency. Applications to thermal conductivity and other experiments are discussed briefly.

A summary of the available literature on the development of the various processes for the separation of uranium and thorium from aqueous nitrate solutions is presented. Flowsheets are given corresponding to the various stages in the development of the Thorex processes.

This manual gives a description, operating instructions, circuit diagram and parts list of Transistorised Temperature Controller type 30 designed in the laboratories of the Australian Atomic Energy Commission.

Technical report. From Abstract : "Magnetic moment measurements have been made on single crystals of terbium (hcp) with fields of 50 to 18,000 oe applied along the <1120> (a-axis), <1010> (b-axis), and <0001> (c-axis) directions. The temperature range covered was 1.4 to 500°K."

Technical report. From Abstract : "The thallium-rich region of the thallium-indium phase diagram was determined from atmospheric pressure to 5.5 kbars primary from electrical resistivity data obtained as a function of composition, temperature, and pressure."

Technical report. From Abstract : "The reactions of VCl2. VCl3, and VCl3-VBr3 mixtures with bromine vapor at 350 to 450°C led to vaporization of the halides and deposition of mixed halides of vanadium (III) at lower temperatures."

Technical report. From Abstract : "The vapor pressures of crystalline VCl2, VBr2, VCl3 and VBr3 have been measured by the Knudsen effusion method using pyrex and Vycor effusion cells. ... During the measurements on VCl3 and VBr3 dissociation and disproportionation of the samples occurred simultaneously with the simple vaporization. However, because the product of each of these processes was collected separately during an experiment, the vapor pressure due to sublimation was obtained without difficulty."