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Determination of Rare Earths in Refined Uranium : Topical Report (open access)

Determination of Rare Earths in Refined Uranium : Topical Report

Abstract: "Rare-earth analyses were performed on several samples of refined uranium oxide and nitrate, using a modified cellulose column procedure. Rare earths were not detectable in samples of 0.03 shotgun of less. Detection limits were from 0.0005 to 0.015 ppm. Negligible quantities of low-cross-section rare earths were found in less pure uranium samples, obtained during start-up operations of the pilot plant at the Feed Materials Production Center, primarily those rare earths of greater than average abundance in nature. No correlation was found between rare-earth content and shotgun values. Rare earths do not appear to be contributing significantly to the neutron absorption of refined uranium. A modified cellulose column procedure, which includes a preconcentration solvent-extraction step, is described. Radioactive tracer tests indicating rare-earth recoveries by the method of >98 per cent are reported."
Date: June 30, 1953
Creator: Ewing, R. A. & Bearse, A. E.
System: The UNT Digital Library