Possible locations of the projected 40-tube overbore facility at the C Reactor are discussed from the standpoint of obtaining conversion ratio data applicable to a full-reactor overbore program.

The purpose of this document is to assembly certain job elements which may become part of the Advanced Engineerng Subsection programs, so that those individuals who may be requested to participate in such programs may be aware of the nature and form of Advanced Engineering planning.

Goats under Nembutal and mice were exposed in a shock tube modified to give longer-duration overpressures and equipped with ports for photography. Except for ear damage, displacement still seemed to be the major cause of injury in goats in the 4-foot section of the tube. However, it was found that mice were killed, apparently by pure blast, in a particular position in a particular type of side chamber attached to the higher-pressure, smaller-diameter, section of the tube. The relation between maximum velocity of displacement and the distance animals were thrown was fairly regular. The probability of injury over different terrains is discussed. (auth)

Annual report submitted by the Girl Scouts of the United States of America to Congress describing highlights from 1960, activities, finance, statistics, organizational leadership, and other information about scouting programs.

The 60-in. scattering chamber used with the external beam of the Argonne 60-in. cyclotron is described. The scattering chamber permits operation over an angular range from 4 deg to 176 deg with an accuracy of plus or minus 3 min. of arc. The geometrical factors involved in the measurement of cross sections are known to plus or minus 0.1% or better. The angular positions of the detectors, the target changer, and an absorber foil system in front of the detection units are operated by remote control so as to permit continuous operation of the cyclotron when these parameters are varied. It is possible to operate several detectors simultaneously; and in order to permit angular correlation studies, the angular position of one detector can be varied by remote control with respect to the other detector units. A summary of some of the experimental work performed with this instrument is given. (auth)

Report presenting a large number of measurements of natural environmental radiation in various parts of the United States using a 20-liter air filled polyethylene-walled ionization chamber at atmospheric pressure. The ionization current was measured with a vibrating reed electrometer connected as a continuously reading voltmeter driving a pen recorder" (p. 1).

The effect of extracted zirconium and nitric acid upon the chemical stability of tributyl phosphate was investigated using gas-liquid chromatography. Tributyl phosphate was degraded approximately 1000 times faster by the tributyl phosphate-zirconium reaction than by the tributyl phosphatenitric acid reaction. Normal butyl nitrate was the major volatile product for both systems studied; with extracted zirconium a solid complex corresponding to the formula Zr(NO/sub 3/ )/sub 2/(DBP)/sub 2/ was also obtained. (auth)

Report presenting more than 500 references to the field of temperature measurement. These references were collected from two general sources: Scientific and technical literature and government reports. The period covered is from 1953 to June 1960, with some from earlier dates. References are divided into a number of categories based on the type of instrument used. Some references to calibration of instruments and to scientific theories upon which temperature measurement is based are also presented.

The current interest in the subject of fiber optics has brought about, among its many achievements, the development of a new technique for measuring refractive index. An instrument designed as a light-pipe refractometer or rod photorefractometer has been described by Kapany and Pike. these authors have presented both a theoretical study of the phenomenon and experimental results arising from a prototype apparatus. The range of applicability of such a device is limited, however, by the availability of rod materials having suitable refractive indices. In particular, the available solid material which has the lowest refractive index and which is also transparent is fused quartz (n{sub D} = 1.458). For reasons inherent in the geometry of the photorefractometer optics, the use of quartz rods does not permit high sensitivity of measurement on liquids having refractive index values less than 1.44. Aqueous solutions, therefore, are beyond the range of study of a system using solid rods. Kapany and Pike suggested the possibility of replacing the solid rod with a hollow cylindrical glass tube filled with a standard liquid. In this manner the effective refractive index of the light pipe is that of the reference liquid and can be varied over the complete range …

Report issued by the Brookhaven National Laboratory discussing the work conducted by the lab during the fiscal year of 1960. As stated in the introduction, "the progress and trends of the research program are presented together with a description of the operational, service, and administrative activities of the Laboratory" (p. vii). This report includes tables, illustrations, and photographs.

The oxidation of graphite in the Hanford reactors is of consequence since graphite burnout affects the strength of the moderator. As a means for indication of any highly oxidizing condition within the stack, containers or boats of small weighed samples of reactor-grade graphite are positioned along the length of an empty process channel in each reactor. The rate of oxidation of the monitoring samples, referred to as the burnout rate, is reported as percent weight lose per 1000 operating days (%/KOD). Currently the burnout rate limit is 2%/KOD. This document presents recent burnout data at the C-reactor.

Report discussing variations in comparative tests of portland cements that could lead to the rejection of a material fully conforming to specification requirements, or the acceptance of a material with undesirable chemical or physical properties. Many of the causes for variation in chemical analyses and physical test results are listed in this discussion, and remedies for some of the more frequently encountered deficiencies in apparatus and methods are suggested.

Abstract: A 12,000 curie cesium-137 research irradiator has been designed and installed on the Georgia Tech campus. The evaluation of the physical characteristics of the irradiator has been completed.

This report for March 1961, from the Chemical Processing Department at HAPO, discusses the following: Production operation; Purex and Redox operation; Finished products operation; maintenance: Financial operations; facilities engineering; research; and employee relations.

Graphic pamphlet about Federal employee position classifications, which determines the pay of a Federal employee.

S>Surface ionization results for natural boron isotopic analysis are in agreement with other recent investigations indicating a B/sup 11//B/sup 10/ atom ratio nesrer to 4.00 than the more commonly accepted value of 4.31 based on BF/ sub 3/ analysis. (auth)

The preliminary design is described of equipment to carry out experiments on boiling burnout in which the average coolant density as a function of coolant channel length as well as local coolant densities may be measured. It appears that by use of the equipment, average densities can be accomplished in a few seconds, while determination of a complete density map (with 5% error) across a plane of the assembly requires approximately one hour. (J.R.D.)

Tests were conducted to obtain data on the dynamic response of the plant to various power range control rod withdrawal transients. The Reactor plant responded generally as expected. Comparison of data with simulator studies revealed that transients were more severe and had less measurable differences between the 20, 40, and 60% power runs than those transients predicted. (J.R.D.)

Reported DSN calculations of reactivity worths of heterogeneities in ZPR- III fast critical assemblies, caused by use of various fuel plate and diluent thicknesses, have shown the necessity for high-order approximations to obtain convergence of flux shape and eigenvalue. Convergence properties of solutions for a simplified two-region, oneenergy-group, repetitive slab cell having regional thicknesses and regional cross sections representative of those encountered in some energy -groups of the previous threegroup study are compared for DSN (N = 2, 4, 8, 16), singlespherical harmonics, PN (N = 1, 3,...., 11, 13), and double spherical harmonics, DPN (N = 1, 2, 3, 4, 5), solutions for the case of a spatially constant unit source density in the alternate regions of the cell. Analogous uncollided flux solutions and an integral transport solution for uncollided flux showing effects of contributions of sources in neighboring cells upon the solution are obtained. As the angular width of the anisotropic flux component occurs predominantly in the region about mu = 0, the "shape" of the spatial flux is largely determined by at most a few nearestneighbor source regions, and the anisotropic component is largely the anisotropic component of the uncollided flux. Use of either a discrete ordinate …

Report presenting a table of corrected optical pyrometer readings which enables optical pyrometer users to convert observed temperature immediately to the true temperature, if the effective emissivity of the material being observed is known. The table gives observed temperatures from 1,000 to 3,000ºK in increments of 5 degrees, from 3,000 to 5,000ºK in increments of 10 degrees, from 5,000 to 10,000ºK in increments of 50 degrees, and from 10,000 to 39,900ºK in increments of 100 degrees. For these, true temperatures are tabulated for 49 emissivities ranging from 0.02 to 0.98 in increments of 0.02.

Corrosion studies were conducted on stainless steel types 347 and Carpenter-20, Monel, titanium 55A, and tsntalum in decontamination solutions. These solutions are: 10% nitric acid, 10% citric acid, 10% sodium hydroxide--2.5% tartaric acid, 10% oxalic acid, 0.003M periodic acid in 0.05M nitric acid, 3% sodium fluoride --20% nitric acid, Turco 4501 and Turco 4502, and 0.25M phosphoric acid. Boron stainless steel type 304L was studied in 10% sodium hydroxide--2.5% tartaric acid, 10 and 60% nitric acids, Turco 4501 and Turco 4502. The two austenitic stainless steels were found to be acceptable construction materials for handling each of the decontamination solutions except 3% sodium fluoride--20% nitric acid. Special limitations are defined for Monel, titanium 55A, and tantalum when exposed to decontamination reagents. (auth)

The corrosion behavior of pure aluminum and some of its alloys in superheated steam was found to depend markedly on the method of starting the corrosion test. Pure aluminum samples survived only in tests that were brought to temperature and pressure very rapidly. Resistant Al-- Ni-- Fe alloys performed well only if a relatively slow starting procedure was used, suffering extensive blistering or complete disintegration in a test started rapidly. Over the range of temperature and pressure investigated, 400 to 540 deg C and 150 to 600 psig, with optimum starting conditions both pure aluminum and resistant Al-- Ni-- Fe alloy samples quickly formed a very protective oxide film. Interference colors were noted for exposures of several weeks. Samples surviving a 260-day test at 540 deg C and 600 psig had less than 1-mg/cm/sup 2/ weight gain. Nonresistant alloys disintegrated in short corrosion exposures. A penetrating attack, initiated in only a few spots, rapidly destroyed the samples. The effects of composition, dispersion of second-phsse compounds, hydrogen porosity, and pretreatments were investigated for 5.6% Ni--0.3% Fe-0.1% Ti in 540 deg C, 600-psig steam. It was concluded that porosity produced by corrosion product hydrogen was a major factor in the survival of …

Corrosion tests in dilute phosphoric acid (pH 3.5) at elevated temperature are described for X8001 aluminum, 18-8 stainless steels, aluminized carbon steel, and Zircaloy. In a 307-day dynamic test at 18 ft/sec and 315 deg C, X8001 aluminum corroded at a rate of 1/2 mdd for the first 240 days. In subsequent exposures, the corrosion rate increased, but the total average penetration at 307 days was only 0.0005 inch. At 200 days, the total corrosion in this test was one-fiftieth that in distilled water. Static tests at 225 deg C gave corrosion rates too low to measure (<0.2 mdd). Of several different 18-8 stainless steels tested in this solution at 315 deg C, only sensitized type 316 suffered intergranular attack. General attack rates of the other samples, of the order of 1/4 mdd, were obtained for the period from 94 to 186 days. Although this is much larger than the rate in distilled water, it represents a penetration rate of only about 5 x 10/sup -//sup 5/ inch/year. Aluminized carbon steel did not suffer rapid corrosion in this solution at 315 deg C, even when large areas of the carbon steel were exposed. There was a tendency for corrosion to …

The proposal to reduce P{sub 32} in reactor effluent by increasing aluminum sulphate and bauxite feed to 18 ppm while maintaining 7.0 pH water is estimated to cost $1,368,000. This represents an increase of $507,000 over FY 1962 budgeted cost for aluminum sulphate, bauxite and sulphuric acid. The basis for the cost estimate is provided, and detail calculations are given.