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The Higher Fluorides of Plutonium (open access)

The Higher Fluorides of Plutonium

A systematic set of thermodynamic data for most of the known compounds of plutonium is presented. From earlier data present, it is now possible to extend the tabulation of data for the compounds of plutonium to include PuF(4), PuF(5), and PuF(6).
Date: March 20, 1950
Creator: Brewer, Leo, 1919-2005; Bromley, LeRoy A.; Gilles, Paul W. & Lofgren, Norman L.
System: The UNT Digital Library
The Gasometric Determination of Nitrite and Sulfamate (open access)

The Gasometric Determination of Nitrite and Sulfamate

This report covers an investigation made to develop a gasometric determination that can determine 1.2 x 10-(-5) g. of nitrite with a precision (99% limits) of +/- 8%, and discusses how this procedure works.
Date: March 6, 1950
Creator: Carson, W. N.
System: The UNT Digital Library
The Coulometric Determination of Acid (open access)

The Coulometric Determination of Acid

Introduction: "The need for a method of acid determination which could be used for small samples and easily adapted to remote control led to the investigation of the use of electrolytically generated base for the titration of acid in certain solutions. The use of electrolytically generated base for the titration of acetic acid in the presence of nitric acid has been reported (1)."
Date: March 1, 1950
Creator: Carson, W. N. & Ko, Roy
System: The UNT Digital Library
Solubility relationships of acidified stored metal wastes (open access)

Solubility relationships of acidified stored metal wastes

The reports aims to determine the solubility limitation of concentrations of uranium in the food preparation step of the tributyl phosphate waste metal recovery process, and the subsequent solubilities in the RA column.
Date: March 24, 1950
Creator: Curtis, M. H.
System: The UNT Digital Library
Preparation of Ductile Zirconium: Progress Report for February 1950 (open access)

Preparation of Ductile Zirconium: Progress Report for February 1950

Abstract: A tungsten tipped electrode has been used in the continuous casting arc furnace for a 25 minute period during which a 12 inch length of ingot was made. Thermocouple junctions within the mold wall have been improved to give mold zone temperature. A total of 10 iodide dissociation runs have been conducted using feed rates of .62-22.7 lbs ZrIâ‚„ per hour with attendant conversion efficiencies of 97.7-16.4% and zirconium yields of 255-41.2 grams per hour. A curve expressing these data for an arbitrarily selected set of conditions is presented.
Date: March 10, 1950
Creator: DiPietro, W. O.; Findlay, G. R. & Moore, J. H.
System: The UNT Digital Library
Protactinium Chemistry (open access)

Protactinium Chemistry

Report discussing protactinium, including the element's history and the results of various experiments.
Date: March 15, 1950
Creator: Elson, R. E.; Sullivan, J. C.; Studier, N. H. & Sullens, P. A.
System: The UNT Digital Library
Preliminary Report on Thermal and Electrical Conductivities of Some Plutonium-Aluminum Alloys (open access)

Preliminary Report on Thermal and Electrical Conductivities of Some Plutonium-Aluminum Alloys

Abstract: "The thermal and electrical conductivities of a series of Pu-Al alloys have been determined in the range 0.12 atomic percent Pu. The conductivities are approximately proportional to the volume of free aluminum."
Date: March 15, 1950
Creator: Gibney, Robert B. & Sandenaw, Thomas A.
System: The UNT Digital Library
Statistical evaluation of calibrartion data-infrared method for determination of % TBP (open access)

Statistical evaluation of calibrartion data-infrared method for determination of % TBP

A report which discusses the data submitted for evaluation. This data is about optical densities from infrared spectrometer readings on eight standard samples, ranging in percent TBP from 6.71 to 17.85.
Date: March 21, 1950
Creator: Healy, W. C.
System: The UNT Digital Library
Corrosion of Stellite in MJ-1 Streams (open access)

Corrosion of Stellite in MJ-1 Streams

The following report provides data from completed tests for corrosion testing of stellite-T347 stainless steel test cylinders.
Date: March 8, 1950
Creator: Koenig, W. W.
System: The UNT Digital Library
Summary of the Research Progress Meeting of March 9, 1950 (open access)

Summary of the Research Progress Meeting of March 9, 1950

The design of the present time of light mass spectrograph is similar to that of the isotron devised some time ago for isotope separation. The spectrograph will employ the time of flight principle only for the isotopic analysis of small samples.
Date: March 23, 1950
Creator: Kramer, Henry P.
System: The UNT Digital Library
Experimental Breeder Project: Report for the Period March 1, 1949 Through January 31, 1950 (open access)

Experimental Breeder Project: Report for the Period March 1, 1949 Through January 31, 1950

Report discussing the progress made on the Experimental Breeder Project during the period from March 1, 1949 to January 31, 1950.
Date: March 13, 1950
Creator: Lichtenberger, H. V.
System: The UNT Digital Library
Preparation of Anhydrous Vanadium Trifluoride (open access)

Preparation of Anhydrous Vanadium Trifluoride

Report discussing a procedure for the preparation of anhydrous vanadium trifluoride. From abstract: "By selecting proper operating conditions and equipment, a method of preparation was devised such that anhydrous vanadium trifluoride of high purity was produced reliably in five pound batches." The method of preparation involves manipulating the starting material, vanadium pentoxide.
Date: March 13, 1950
Creator: Mackey, T. S. & Johnsson, K. O.
System: The UNT Digital Library
The Oxidation of Plutonium to the Plutonyl State (open access)

The Oxidation of Plutonium to the Plutonyl State

This report follows the study of the oxidation of plutonium III and IV to the plutonyl state.
Date: March 22, 1950
Creator: Miller, H. W. & Brouns, R. J.
System: The UNT Digital Library
The Preparation of Thin Films of Plutonium by Electrodeposition (open access)

The Preparation of Thin Films of Plutonium by Electrodeposition

This report discusses methods for preparing thin films of plutonium on metallic disks, which are used for alpha energy analysis, fission counting, and preparation of geometry standards in ordinary counting. Various methods of preparation were tested and analyzed, but electrodeposition was the most effective method. Deposition was then tested, but the yields were "somewhat erratic".
Date: March 22, 1950
Creator: Miller, H. W. & Brouns, R. J.
System: The UNT Digital Library
The Determination of Tributyl Phosphate in Deodorized Shell Base with the Infrared Spectrometer (open access)

The Determination of Tributyl Phosphate in Deodorized Shell Base with the Infrared Spectrometer

The following report describes methods used to determine tributylphosphate in a deodorized shell base. An infrared absorption method is developed to emphasize toward determination of TBP in RCW streams, the organic waste streams.
Date: March 10, 1950
Creator: Moore, R. H.
System: The UNT Digital Library
Infrared Absorption Measurements Indicating Intermolecular Association of Water and Hexone (open access)

Infrared Absorption Measurements Indicating Intermolecular Association of Water and Hexone

This report analyzes infrared absorption measurements that were made in the regions of carbonyl band and hydroxyl band absorptions on solutions of water in hexone and water in acetone, confirming intermolecular association of water and hexone.
Date: March 8, 1950
Creator: Moore, R. H.
System: The UNT Digital Library
P-10 Chemical Equilibria (open access)

P-10 Chemical Equilibria

This report studies tritium oxides and tritium in water vapor, a product of P-10.
Date: March 23, 1950
Creator: Roesch, William C.
System: The UNT Digital Library
The Development of Plutonium Electrodeposition Methods : Interim Report (open access)

The Development of Plutonium Electrodeposition Methods : Interim Report

From introduction: "The following report presents a body of information obtained in the Health Instrument Development Laboratory from September, 1948, to the present, and is intended to be a preliminary review of [the study of electrodeposition of plutonium]. Many improvements in technique and methods and investigations along lines not explored are suggested by the present work. These will be undertaken as time permits, and reported at a later time."
Date: March 1, 1950
Creator: Schwendiman, L. C.
System: The UNT Digital Library