The work described was undertaken to provide data for nuclear safety studies concerning NPF reprocessing equipment. The original objective was to determine the uranium density and water (hydrogen) content of UO2-H2O mixtures ranging from compact centrifuge cakes to dilute slurries. The scope was later expanded to include mixtures of UO2 with hydrocarbon oil and mixtures of UO3-H2O.

Report documenting the Halogen Collector Test program, which was undertaken to provide "methods of removing trace quantities of radioactive iodine from an air stream" (p. 1). The report includes designs of the program and the test facility, test results, analysis of these results, and encountered problems. Appendices begin on page 38.

Report describing the performance, fission product tolerance, design, and costs of the DR-1 Gas Loop, which is an in-reactor test facility.

A report which describes a number of experiments conducted to compare the effects of different methods of surface preparation on x-ray diffraction patterns of uranium obtained by the spectrometer technique.

Space has been reserved near the southeast corner of the 100-N Area for the 122-N Decontamination Facility. Previous correspondence between Burns and Roe, Inc and General Electric bae discussed various facilities which might be needed in the building. The concepts of the decontamination processes are under active development by research groups at Hanford. At present, there are several workable processes known; each one has one or more fairly serious drawbacks.

The use of a reactor charged with silver nitrate coated packing for removal of radio-iodine from the waste gases of Hanford chemical processing plants has been successful in removing approximately 99.5 percent of this activity. Studies by the Radiological Sciences Department indicated the desirability of further reducing the amount of radio-iodine released to the atmosphere. Therefore, this study was undertaken with the objectives of better understanding the inherent limitations to iodine removal by reaction with silver nitrate, and improving the efficiency of removal of iodine.

Photographic observations of the behavior of uranium dioxide at high temperatures are of great value in designing and evaluating fuel elements. This paper reports the growth of uranium dioxide crystals by vapor deposition during out-of-reactor and in-reactor experiments.

A process for hot-press canning of unplated thorium cores in aluminum jackets was developed using wafers of thorium and aluminum for diffusion and bonding studies.

The feasibility of removing and recovering cesium-137 from various HAPO process solutions by precipitation of Cs2ZnFe(CN)6 has been demonstrated previously. Pilot plant studies of calcination and steam hydrolysis of non-radioactive Cs2ZnFe(CN)6 precipitates by members of the Process Equipment Development Operation are currently in progress. In support of these pilot plant studies, experiments were performed to determine the extent, if any, to which cesium volatilizes during calcination and hydrolysis of Cs2ZnFe(CN)6 precipitates containing cesium-137. Experimental procedures and results are presented in this report.

Well-type scintillation counters have found use in many radiochemical laboratories. A gamma scintillation well counter has been used to measure the gamma activity of liquid samples in the 325 Building counting room for about a year. This well counter has been built and calibrated so that gamma activity measurements made with it can be easily compared with measurements made with the gamma scintillation counter (GSC). The well counter is electronically identical to the present GSC and differs only in the shape of the crystal used and the physical arrangement of the lead shield. The crystal contains a well which allows a tube containing the sample to be inserted in the crystal. The physical arrangement of the detector greatly simplifies the preparation of liquid samples for activity measurement. The 325 Building well counter and its application to chemical research and plant process analysis will be discussed in the following paragraphs. An operating procedure is also included.

This study was initiated to determine the minimum safety requirements for safe anchorage of electric pole lines. The objectives were to investigate the suitability of manufactured concrete pole line anchors for use at the Hanford Atomic Products Operation, to design a concrete anchor slug of optimum shape and size for manufacture, to determine by field tests the resistance pullout of the concrete anchor when buried at various depths under the most favorable condition, and to develop a safe design load for the anchors at various depths of burial and angle of pull based on test results.

This report discusses properties of the Redox process. Density, apparent molar volumes and viscosity are all described.

The fabrication processes applied to nuclear fuels are subject to severe limitations because of the conditions imposed by the reactor environment. The combined problems of neutrons fluxes, high heat fluxes, corrosion by the coolant , and embrittlement by hydriding or similar reactions may be minimized through establishing rigorous materials and fabrication specifications for fuel and cladding.

The purpose of this report is to show the impedance of an approximate equivalent circuit on a complex plan for various constant frequencies and different metals. The equivalent circuit represents a testing coil driven with an AC voltage and a network to represent the impedance of the metal.

This report covers an investigation made to develop a gasometric determination that can determine 1.2 x 10-(-5) g. of nitrite with a precision (99% limits) of +/- 8%, and discusses how this procedure works.

Introduction: "The need for a method of acid determination which could be used for small samples and easily adapted to remote control led to the investigation of the use of electrolytically generated base for the titration of acid in certain solutions. The use of electrolytically generated base for the titration of acetic acid in the presence of nitric acid has been reported (1)."

The amount of dry air or inert gas supplied to a "one pass" glove box ventilation system is proportional to the glove box inleakage. Most glove boxes in the 234r5 Building are equipped with sundry attachments, each contributing to the inleakage. No individual leak rate date is available for these auxiliary components in the "as installed" condition. Nor is the effect of time upon the leak rates known. Knowledge of these values, or at least an indication of the order of magnitude of the leakage attributable to each item, would provide a basis for analyzing glove box ventilation problems and for establishing criteria for new glove box designs.

This report summarizes the research and development work carried out during June, July, and August, 1959, for Budget Activity 2790- Separations Development for Non-Production Reactors. The effort on Activity 2790 - Separations Development for Non-Production Reactors. The effort on Activity 2790 will enable Hanford to begin reprocessing in January, 1962, the fuel elements from power reactors which employ depleted or slightly enriched uranium fuels.

A knowledge of the preferred orientation of the crystal aggregates in pile structural materials is of basic importance in the attempt to understand their behavior under operating conditions. The effect of a preferential alignment of crystallites in enisotropic materials is to create a directional variation in physical and mechanical properties. In most applications directional effects are undesirable and efforts are usually made during fabrication to avoid the conditions which cause the orientation or, if possible, to alleviate the condition by proper heat treatments after the forming process if the orientation persists. Some of the variables that affect the type and degree of preferred orientation is metals during the forming process include working temperature, per cent reduction, the nature of the applied forces used, the crystal structure, and the inherent deformation mechanisms of the metal.

The reports aims to determine the solubility limitation of concentrations of uranium in the food preparation step of the tributyl phosphate waste metal recovery process, and the subsequent solubilities in the RA column.

A coolant line rupture during operation of a high temperature gas cooled graphite moderated reactor would present a serious hazard. The reactor would immediately depressurize and a great deal of air would be introduced into the coolant stream. As the air passed over the graphite moderator a runaway oxidation reaction would probably ensue unless an adequate safety system were available. This investigation was designed to evaluate chlorine as a reactor safeguard to be used to control a runaway reaction. Throughout this study, a small amount of chlorine in an air stream has demonstrated the ability to substantially reduce the oxidation rate of graphite. This has been the case even where the principal oxidizing agent was molecular oxygen or ozone.

Water treatment systems for preparing and maintaining high purity water in out-of-reactor or in-reactor test oops are becoming increasingly important. In out0of-reactor experiments the presence of ionic impurities in the water has a marked influence on film formation and corrosion rates. It is therefore , imperative that these impurities be maintained at the lower practical concentration.

The purpose of this report is to present a HAPO proposal for the design and construction of a high-temperature, high-pressure light water recirculation test facility for the Westinghouse Electric Corporation, Atomic Power Division This report does not attempt to justify the feasibility of site location nor does it attempt to elaborate on such technical considerations as permissible test specimen heat generation and enrichment requirements which have been covered in an earlier document. Instead, detail information is developed on the proposed design with major emphasis on detail descriptions of the proposed loop and auxiliaries, design and construction scheduling and costs, and operating costs.

Report discussing the procedures and experimental data of various plutonium waste recovery methods. The report elaborates on the different methods of collection necessary for different wastes.