Abstract: "This report describes work done to improve the casting characteristics of methyl methacrylete resin under CMR-6-18 authorization. The experimental program was initiated with the objectives of decreasing casting time, bubble formation and shrinkage. It has been found that by use of a common solvent for monomer and polymer concentration in monomer can be attained greater than any previously reported in preparation of a methacrylate casting resign. Incorporation of this greater amount of polymer has produced the desired effects. A bibliography of relevant literature is included to which reference is made in the text."

The following report describes two rapid, micro methods for the determination of UNH in Redox waste samples that had been developed fir the concentration range 0.2 to 100 g/l.

This report is a progress report detailing operations and ongoing projects at the Brookhaven National Laboratory. The report describes new developments with buildings and progress regarding ongoing experiments. The report includes photographs showing progress in the construction of the reactor and other images and figures that accompany the descriptions of projects.

Abstract. thorium can be precipitated as a salt of p-dimethylaminoazophenylarsonic acid at a pH of about 1.5. the precipitate, collected on a sintered glass filter is washed with dilute ammonium hydroxide to dissolve the dye. the amount of thorium is determined by measuring the concentration of the dye spectrophotometrically at a wavelength of 450 millimicrons. Zirconium, which interferes, can be separated and determined using the same reagent in strong hydrochloric. the behavior of thorium metal upon treatment with various acids and upon fusion withKHSO4 is described. three satisfactory procedures are given for dissolving the metal with sulfuric acid, phosphoric acid, and by a potassium hydrogen sulfate fusion. The laboratory was presented with the problem of analyzing for a large number of elements in O2 metal. the results of a systematic study of methods for effecting solution of the metal are offered here since they may be of some interest and use to other laboratories. The four methods which effected complete solution of the metal are (1) Sulfuric acid method; (2) Fusion method; (3) Phosphoric acid method; and (4) Nitric acid-hydrofluoric acid method.

Abstract. Experimental work was carried out to improve material conversion efficiency and to reduce handling costs inherent in the present process for production of high purity calcium. Charges up to 54 pounds were handled successfully in the equipment available. Material losses were reduced and more complete removal of alkali and alkaline earth metals was effected by controlled pressures of inert gas and by melting under positive pressure of Argon.

Technical report. Numerous application of various column adsorption techniques to inorganic analytical chemistry have appear in the literature. The comparatively recent introduction of ion exchange resins has resulted in the development of efficient, simple, and rapid column adsorption methods. the principal service of column adsorption methods to analytical chemistry is that of providing a relatively simple means of separating an element in a sufficiently pure state so that a direct precipitation, ignition, and weighting, for example, will suffice to complete the quantitative analysis. Systems involving uranyl nitrate will naturally be emphasized in this report but information will be included concerning the separation of the individual members of a series from one another, such as in the alkaline earths and the rare earths.

The critical mass of 94-239 and the corresponding critical dimensions of homogeneous mixtures of 94-239 with various moderating media been calculated as a function of the concentration of 94. A simple transformation makes the figures applicated to92-235. the results are in essential agreement with the preliminary estimated made independently by Oppenheimer and Serber. The problem of the stability of a chain reaction in solution and questions of protection are discussed.

Abstract. Some rather idealized considerations are given regarding the depth a warped rod presses into the ribs at the places of contact. It appears that this distance may, under some conditions, be of the order of 70 times greater than for a straight rod resting uniformly on the ribs.

Abstract. the Laplacian of a beryllium metal lattice with 3.3 kg of uranium metal per cell and a volume ratio of 17.2 was measured in the removable region of the CP-2 machine. the sandwich effect with different moderators made interpretation of the observations very uncertain. The best result found was Be = 407 x 10(-6) cm(-2).

Historical: This process is based on experimental work done in Jackson Laboratory, Send Works, Blue Products, and East Area. It supersedes the Tentative Chambers Works Process for the Manufacture of Fluorine Using Carbon Anode Units, dated December 2, 1943.

Report discussing the results of an investigation of a test for statistical consistency of counter-scaler units.

Introduction: This report embodies the results of an investigation as to the possibility of removing the bulk of the iron from gunk solutions of various concentrations by precipitation of the iron with phthallic acid and subsequent precipitation of tuballoy. The method consists of dissolving the phthallic acid in the gunk solution and then adding NH₃ to a suitable pH, precipitating the iron, and leaving the tuballoy in solution.

Abstract: Solid ferric chloride reacts with solid uranium tetrachloride to form a complex iron-uranium chloride compound at approximately 263°C. The vapor pressure of this compound is nearer to that of uranium tetrachloride than to the vapor pressure of ferric chloride.

This report discusses two methods used for experimental determination of the interfacial tension of an immisible aqueous-organic system where the density of the organic phase is less than that of the aqueous phase. The methods discussed are the falling drop method and the Donnan modification/rising drop method.

Abstract: Twenty-two metallic oxides were refluxed with hexachloropropylene. The anhydrous chlorides or other products formed are described for each oxide. The reactions were particularly vigorous with higher valent oxides of the fifth and sixth group elements.

From abstract: "A comparison has been made of methods for producing Fe59 of higher specific activity than that obtainable by irradiating natural iron in the Clinton pile. Five processes have been considered, (1) irradiation of natural iron in the Hanford piles, (2) irradiation of enriched F58 in the Clinton and Hanford piles, (3) Szilard-Chalmers enrichment using ferrocyanides in the Clinton pile, (4) collection of recoils in a phase separable from the bulk of the iron, and (5) the Co59 (n,p) Fe59 reaction in the Clinton and Hanford piles."

This report for January, 1947 discusses progress regarding ore dressing studies, pyrometallurgical work, chemical work, chemical and spectrographic analysis, and physical methods of analysis.

From introduction: "The purpose of this report is to summarize some of the information obtained to date on the distribution of the uranium in the mineral phases of the phosphate rocks and shale."

Abstract: This discussion concerns the operation, construction, and servicing of an alpha rate meter of medium sensitivity (30,000 alpha particles full scale per minute) and good stability. The instrument is equipped with an oscillator which increases both in frequency and loudness as the alpha activity is increased. The oscillator circuit includes an anticipator which causes a change in frequency depending directly upon the rate of change of alpha activity. Maximum sensitivity is approximately 100 millivolts full scale. Grid current varies from 1 to 5 x 10^-14 amperes. A general discussion of time constants and accuracy is included. Tables of stopping power, ionization and alpha activity are appended.

The following report analyzes and calculates the accuracy of a procedure that processes independent source neutron cards in the Monte Carlo method.

This report follows investigations of fission fragments, as they contain charged nuclear high energy and contain a high excess of neutrons.

This report follows a test made to determine the effect of temperature on the distribution of nitric acid between "carbitol" and gunk, extracting a number of samples of aqueous copper nitrate with samples of "carbitol" of various acidities. The data obtained is covered in Table 1.

Inroduction: "A study of the literature, particularly the work done by R. Strubl, I.W. Kolthoff and S.B. Smith, indicated that a polargraphic method for the estimation of T could be devised which would not sacrifice reasonable accuracy for rapidity. Work was begun with the intention of developing such a method."

Abstract: "For defects between interior and coating, or between successive layers of coating, a simple, fairly accurate formula is established. The temperature rise at the edge of the defect is briefly discussed."